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Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]. / Asanova, Tatyana; Asanov, Igor; Zadesenets, Andrey et al.

In: Journal of Thermal Analysis and Calorimetry, Vol. 123, No. 2, 01.02.2016, p. 1183-1195.

Research output: Contribution to journal › Article › peer-review

Harvard

Asanova, T, Asanov, I, Zadesenets, A, Filatov, E, Plyusnin, P, Gerasimov, E & Korenev, S 2016, 'Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]', Journal of Thermal Analysis and Calorimetry, vol. 123, no. 2, pp. 1183-1195. https://doi.org/10.1007/s10973-015-5002-5

APA

Asanova, T., Asanov, I., Zadesenets, A., Filatov, E., Plyusnin, P., Gerasimov, E., & Korenev, S. (2016). Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]. Journal of Thermal Analysis and Calorimetry, 123(2), 1183-1195. https://doi.org/10.1007/s10973-015-5002-5

Vancouver

Asanova T, Asanov I, Zadesenets A, Filatov E, Plyusnin P, Gerasimov E et al. Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]. Journal of Thermal Analysis and Calorimetry. 2016 Feb 1;123(2):1183-1195. doi: 10.1007/s10973-015-5002-5

Author

Asanova, Tatyana ; Asanov, Igor ; Zadesenets, Andrey et al. / Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]. In: Journal of Thermal Analysis and Calorimetry. 2016 ; Vol. 123, No. 2. pp. 1183-1195.

BibTeX

@article{a96cc0239e6746f7819ea78d37d8cd0a,
title = "Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]",
abstract = "Thermal decomposition of double complex salt [Pd(NH3)4][PtCl6] in a helium atmosphere has been studied by ex situ X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy. Statistical multivariate curve resolution approach to XPS and Auger spectra analysis was applied. This approach was compared with a convenient XPS analysis, demonstrating comparable results and its effectiveness in analysis of sample containing components with various oxidation states, but a little difference in composition. The result obtained allows the complex salt to use as a perspective single-source precursor in one-pot synthesis of PdPt alloy nanoparticles. To examine the precursor, thermal decomposition and shock of [Pd(NH3)4][PtCl6] were performed under various conditions in inert and reduction atmospheres and the final products were studied.",
keywords = "PdPt alloy nanoparticles, Thermal analysis, Thermal decomposition, XPS, XRD, [Pd(NH)][PtCl]",
author = "Tatyana Asanova and Igor Asanov and Andrey Zadesenets and Evgeniy Filatov and Pavel Plyusnin and Evgeniy Gerasimov and Sergey Korenev",
year = "2016",
month = feb,
day = "1",
doi = "10.1007/s10973-015-5002-5",
language = "English",
volume = "123",
pages = "1183--1195",
journal = "Journal of Thermal Analysis and Calorimetry",
issn = "1388-6150",
publisher = "Springer Nature",
number = "2",

}

RIS

TY - JOUR

T1 - Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6]

AU - Asanova, Tatyana

AU - Asanov, Igor

AU - Zadesenets, Andrey

AU - Filatov, Evgeniy

AU - Plyusnin, Pavel

AU - Gerasimov, Evgeniy

AU - Korenev, Sergey

PY - 2016/2/1

Y1 - 2016/2/1

N2 - Thermal decomposition of double complex salt [Pd(NH3)4][PtCl6] in a helium atmosphere has been studied by ex situ X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy. Statistical multivariate curve resolution approach to XPS and Auger spectra analysis was applied. This approach was compared with a convenient XPS analysis, demonstrating comparable results and its effectiveness in analysis of sample containing components with various oxidation states, but a little difference in composition. The result obtained allows the complex salt to use as a perspective single-source precursor in one-pot synthesis of PdPt alloy nanoparticles. To examine the precursor, thermal decomposition and shock of [Pd(NH3)4][PtCl6] were performed under various conditions in inert and reduction atmospheres and the final products were studied.

AB - Thermal decomposition of double complex salt [Pd(NH3)4][PtCl6] in a helium atmosphere has been studied by ex situ X-ray diffraction, X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy. Statistical multivariate curve resolution approach to XPS and Auger spectra analysis was applied. This approach was compared with a convenient XPS analysis, demonstrating comparable results and its effectiveness in analysis of sample containing components with various oxidation states, but a little difference in composition. The result obtained allows the complex salt to use as a perspective single-source precursor in one-pot synthesis of PdPt alloy nanoparticles. To examine the precursor, thermal decomposition and shock of [Pd(NH3)4][PtCl6] were performed under various conditions in inert and reduction atmospheres and the final products were studied.

KW - PdPt alloy nanoparticles

KW - Thermal analysis

KW - Thermal decomposition

KW - XPS

KW - XRD

KW - [Pd(NH)][PtCl]

UR - http://www.scopus.com/inward/record.url?scp=84954286920&partnerID=8YFLogxK

U2 - 10.1007/s10973-015-5002-5

DO - 10.1007/s10973-015-5002-5

M3 - Article

AN - SCOPUS:84954286920

VL - 123

SP - 1183

EP - 1195

JO - Journal of Thermal Analysis and Calorimetry

JF - Journal of Thermal Analysis and Calorimetry

SN - 1388-6150

IS - 2

ER -

ID: 25403025