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Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic. / Krutskii, Yu L.; Maksimovskii, E. A.; Popov, M. V. et al.

In: Russian Journal of Applied Chemistry, Vol. 90, No. 10, 01.10.2017, p. 1579-1585.

Research output: Contribution to journal › Article › peer-review

Harvard

Krutskii, YL, Maksimovskii, EA, Popov, MV, Netskina, OV, Krutskaya, TM, Cherkasova, NY, Kvashina, TS & Drobyaz, EA 2017, 'Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic', Russian Journal of Applied Chemistry, vol. 90, no. 10, pp. 1579-1585. https://doi.org/10.1134/S1070427217100044

APA

Krutskii, Y. L., Maksimovskii, E. A., Popov, M. V., Netskina, O. V., Krutskaya, T. M., Cherkasova, N. Y., Kvashina, T. S., & Drobyaz, E. A. (2017). Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic. Russian Journal of Applied Chemistry, 90(10), 1579-1585. https://doi.org/10.1134/S1070427217100044

Vancouver

Krutskii YL, Maksimovskii EA, Popov MV, Netskina OV, Krutskaya TM, Cherkasova NY et al. Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic. Russian Journal of Applied Chemistry. 2017 Oct 1;90(10):1579-1585. doi: 10.1134/S1070427217100044

Author

Krutskii, Yu L. ; Maksimovskii, E. A. ; Popov, M. V. et al. / Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic. In: Russian Journal of Applied Chemistry. 2017 ; Vol. 90, No. 10. pp. 1579-1585.

BibTeX

@article{ab295ef925e2408097b677d1319c5e7c,
title = "Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic",
abstract = "Reduction of zirconium dioxide with boron carbide and nanofibrous carbon in argon yielded a highly dispersed powder of zirconium diboride. Characteristics of zirconium diboride powders were examined by various analytical methods. The material obtained is represented by a single phase, zirconium diboride. Powder particles are for the most part aggregated. The average size of particles and aggregates is 10.9–12.9 μm with a wide size distribution. The specific surface area of the samples is 1.8–3.6 m2 g–1. The oxidation of zirconium diboride begins at a temperature of 640°C The optimal synthesis parameters were determined: ZrO2: B4C: C molar ratio of 2: 1: 3 (in accordance with stoichiometry), process temperature 1600–1700°C, synthesis duration 20 min.",
keywords = "ZRB2 POWDER, TEMPERATURE SYNTHESIS, BORO/CARBOTHERMAL REDUCTION, BOROTHERMAL REDUCTION, METAL BORIDES, ZRO2, SHS, PRECURSORS, EVOLUTION, TITANIUM",
author = "Krutskii, {Yu L.} and Maksimovskii, {E. A.} and Popov, {M. V.} and Netskina, {O. V.} and Krutskaya, {T. M.} and Cherkasova, {N. Yu} and Kvashina, {T. S.} and Drobyaz, {E. A.}",
note = "Publisher Copyright: {\textcopyright} 2017, Pleiades Publishing, Ltd.",
year = "2017",
month = oct,
day = "1",
doi = "10.1134/S1070427217100044",
language = "English",
volume = "90",
pages = "1579--1585",
journal = "Russian Journal of Applied Chemistry",
issn = "1070-4272",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "10",

}

RIS

TY - JOUR

T1 - Synthesis of Highly Dispersed Zirconium Diboride for Fabrication of Special-Purpose Ceramic

AU - Krutskii, Yu L.

AU - Maksimovskii, E. A.

AU - Popov, M. V.

AU - Netskina, O. V.

AU - Krutskaya, T. M.

AU - Cherkasova, N. Yu

AU - Kvashina, T. S.

AU - Drobyaz, E. A.

N1 - Publisher Copyright: © 2017, Pleiades Publishing, Ltd.

PY - 2017/10/1

Y1 - 2017/10/1

N2 - Reduction of zirconium dioxide with boron carbide and nanofibrous carbon in argon yielded a highly dispersed powder of zirconium diboride. Characteristics of zirconium diboride powders were examined by various analytical methods. The material obtained is represented by a single phase, zirconium diboride. Powder particles are for the most part aggregated. The average size of particles and aggregates is 10.9–12.9 μm with a wide size distribution. The specific surface area of the samples is 1.8–3.6 m2 g–1. The oxidation of zirconium diboride begins at a temperature of 640°C The optimal synthesis parameters were determined: ZrO2: B4C: C molar ratio of 2: 1: 3 (in accordance with stoichiometry), process temperature 1600–1700°C, synthesis duration 20 min.

AB - Reduction of zirconium dioxide with boron carbide and nanofibrous carbon in argon yielded a highly dispersed powder of zirconium diboride. Characteristics of zirconium diboride powders were examined by various analytical methods. The material obtained is represented by a single phase, zirconium diboride. Powder particles are for the most part aggregated. The average size of particles and aggregates is 10.9–12.9 μm with a wide size distribution. The specific surface area of the samples is 1.8–3.6 m2 g–1. The oxidation of zirconium diboride begins at a temperature of 640°C The optimal synthesis parameters were determined: ZrO2: B4C: C molar ratio of 2: 1: 3 (in accordance with stoichiometry), process temperature 1600–1700°C, synthesis duration 20 min.

KW - ZRB2 POWDER

KW - TEMPERATURE SYNTHESIS

KW - BORO/CARBOTHERMAL REDUCTION

KW - BOROTHERMAL REDUCTION

KW - METAL BORIDES

KW - ZRO2

KW - SHS

KW - PRECURSORS

KW - EVOLUTION

KW - TITANIUM

UR - http://www.scopus.com/inward/record.url?scp=85042078053&partnerID=8YFLogxK

U2 - 10.1134/S1070427217100044

DO - 10.1134/S1070427217100044

M3 - Article

AN - SCOPUS:85042078053

VL - 90

SP - 1579

EP - 1585

JO - Russian Journal of Applied Chemistry

JF - Russian Journal of Applied Chemistry

SN - 1070-4272

IS - 10

ER -

ID: 9961521