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Synthesis of fine dispersed titanium diboride from nanofibrous carbon. / Krutskii, Yu L.; Bannov, A. G.; Antonova, E. V. et al.

In: Ceramics International, Vol. 43, No. 3, 15.02.2017, p. 3212-3217.

Research output: Contribution to journal › Article › peer-review

Harvard

Krutskii, YL, Bannov, AG, Antonova, EV, Sokolov, VV, Pichugin, AY, Maksimovskii, EA, Krutskaya, TM, Netskina, OV & Bataev, IA 2017, 'Synthesis of fine dispersed titanium diboride from nanofibrous carbon', Ceramics International, vol. 43, no. 3, pp. 3212-3217. https://doi.org/10.1016/j.ceramint.2016.11.146

APA

Krutskii, Y. L., Bannov, A. G., Antonova, E. V., Sokolov, V. V., Pichugin, A. Y., Maksimovskii, E. A., Krutskaya, T. M., Netskina, O. V., & Bataev, I. A. (2017). Synthesis of fine dispersed titanium diboride from nanofibrous carbon. Ceramics International, 43(3), 3212-3217. https://doi.org/10.1016/j.ceramint.2016.11.146

Vancouver

Krutskii YL, Bannov AG, Antonova EV, Sokolov VV, Pichugin AY, Maksimovskii EA et al. Synthesis of fine dispersed titanium diboride from nanofibrous carbon. Ceramics International. 2017 Feb 15;43(3):3212-3217. doi: 10.1016/j.ceramint.2016.11.146

Author

Krutskii, Yu L. ; Bannov, A. G. ; Antonova, E. V. et al. / Synthesis of fine dispersed titanium diboride from nanofibrous carbon. In: Ceramics International. 2017 ; Vol. 43, No. 3. pp. 3212-3217.

BibTeX

@article{d3eeb371db7f4968b8a121b617d7ee46,
title = "Synthesis of fine dispersed titanium diboride from nanofibrous carbon",
abstract = "This paper presents the experimental data on the synthesis of titanium diboride (TiB2) fine dispersed powder carried out in laboratory scale. TiB2 powder was prepared by the reduction of titanium dioxide with boron carbide and nanofibrous carbon in an argon atmosphere. The powders of TiB2 were characterized by X-ray diffraction (XRD), elemental analyses, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), low-temperature nitrogen adsorption, particle size analysis, simultaneous thermogravimetry and differential scanning calorimetry (TG-DSC). The resulting material contains a single phase – titanium diboride. The particles of the powder were predominantly aggregated. The average size of the particles and the aggregates were 7.4–8.0 µm with a wide size of distribution. The specific surface values of samples obtained were 2.4–5.8 m2/g. The oxidation of titanium diboride began from the temperature of 450 °C. In this work, the optimal synthesis conditions were estimated: the molar ratio was TiO2:B4C:C=2:1:3 (according to stoichiometry), the temperature was 1600 °C, the process duration was 20–30 min.",
keywords = "Borides, Carbon nanofibers, Chemical preparation, Chemical properties, Powders, Spectroscopy, MECHANOCHEMICAL SYNTHESIS, MECHANICAL-PROPERTIES, TIB2-SIC CERAMIC COMPOSITES, POWDERS, CARBIDE, REDUCTION, BORIDE, MICROSTRUCTURE, SHS",
author = "Krutskii, {Yu L.} and Bannov, {A. G.} and Antonova, {E. V.} and Sokolov, {V. V.} and Pichugin, {A. Yu} and Maksimovskii, {E. A.} and Krutskaya, {T. M.} and Netskina, {O. V.} and Bataev, {I. A.}",
year = "2017",
month = feb,
day = "15",
doi = "10.1016/j.ceramint.2016.11.146",
language = "English",
volume = "43",
pages = "3212--3217",
journal = "Ceramics International",
issn = "0272-8842",
publisher = "Elsevier",
number = "3",

}

RIS

TY - JOUR

T1 - Synthesis of fine dispersed titanium diboride from nanofibrous carbon

AU - Krutskii, Yu L.

AU - Bannov, A. G.

AU - Antonova, E. V.

AU - Sokolov, V. V.

AU - Pichugin, A. Yu

AU - Maksimovskii, E. A.

AU - Krutskaya, T. M.

AU - Netskina, O. V.

AU - Bataev, I. A.

PY - 2017/2/15

Y1 - 2017/2/15

N2 - This paper presents the experimental data on the synthesis of titanium diboride (TiB2) fine dispersed powder carried out in laboratory scale. TiB2 powder was prepared by the reduction of titanium dioxide with boron carbide and nanofibrous carbon in an argon atmosphere. The powders of TiB2 were characterized by X-ray diffraction (XRD), elemental analyses, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), low-temperature nitrogen adsorption, particle size analysis, simultaneous thermogravimetry and differential scanning calorimetry (TG-DSC). The resulting material contains a single phase – titanium diboride. The particles of the powder were predominantly aggregated. The average size of the particles and the aggregates were 7.4–8.0 µm with a wide size of distribution. The specific surface values of samples obtained were 2.4–5.8 m2/g. The oxidation of titanium diboride began from the temperature of 450 °C. In this work, the optimal synthesis conditions were estimated: the molar ratio was TiO2:B4C:C=2:1:3 (according to stoichiometry), the temperature was 1600 °C, the process duration was 20–30 min.

AB - This paper presents the experimental data on the synthesis of titanium diboride (TiB2) fine dispersed powder carried out in laboratory scale. TiB2 powder was prepared by the reduction of titanium dioxide with boron carbide and nanofibrous carbon in an argon atmosphere. The powders of TiB2 were characterized by X-ray diffraction (XRD), elemental analyses, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), low-temperature nitrogen adsorption, particle size analysis, simultaneous thermogravimetry and differential scanning calorimetry (TG-DSC). The resulting material contains a single phase – titanium diboride. The particles of the powder were predominantly aggregated. The average size of the particles and the aggregates were 7.4–8.0 µm with a wide size of distribution. The specific surface values of samples obtained were 2.4–5.8 m2/g. The oxidation of titanium diboride began from the temperature of 450 °C. In this work, the optimal synthesis conditions were estimated: the molar ratio was TiO2:B4C:C=2:1:3 (according to stoichiometry), the temperature was 1600 °C, the process duration was 20–30 min.

KW - Borides

KW - Carbon nanofibers

KW - Chemical preparation

KW - Chemical properties

KW - Powders

KW - Spectroscopy

KW - MECHANOCHEMICAL SYNTHESIS

KW - MECHANICAL-PROPERTIES

KW - TIB2-SIC CERAMIC COMPOSITES

KW - POWDERS

KW - CARBIDE

KW - REDUCTION

KW - BORIDE

KW - MICROSTRUCTURE

KW - SHS

UR - http://www.scopus.com/inward/record.url?scp=85006364625&partnerID=8YFLogxK

U2 - 10.1016/j.ceramint.2016.11.146

DO - 10.1016/j.ceramint.2016.11.146

M3 - Article

AN - SCOPUS:85006364625

VL - 43

SP - 3212

EP - 3217

JO - Ceramics International

JF - Ceramics International

SN - 0272-8842

IS - 3

ER -

ID: 10351789