Research output: Contribution to journal › Conference article › peer-review
Production of nanoscale crystalline materials (Si, SiC) by a highly efficient hyperbaric method. / Ezdin, B. S.; Kalyada, V. V.; Ischenko, A. V. et al.
In: Journal of Physics: Conference Series, Vol. 1128, No. 1, 012100, 07.12.2018.Research output: Contribution to journal › Conference article › peer-review
}
TY - JOUR
T1 - Production of nanoscale crystalline materials (Si, SiC) by a highly efficient hyperbaric method
AU - Ezdin, B. S.
AU - Kalyada, V. V.
AU - Ischenko, A. V.
AU - Zarvin, A. E.
AU - Nikiforov, A. A.
AU - Yatsenko, D. A.
N1 - Publisher Copyright: © 2018 Institute of Physics Publishing. All rights reserved.
PY - 2018/12/7
Y1 - 2018/12/7
N2 - The method of producing nanopowders of Si and SiC by pyrolysis of a silicon-hydrocarbon mixture by compression in a cyclic process in a flow reactor is proposed and implemented. The obtained powders are characterized by X-ray diffraction and transmission electron microscopy. The new design solutions and use of ceramic coatings obtained by applying microarc oxidation for the piston-cylinder assembly - a compression unit of the reactor - allowed avoiding the use of compression rings and lubricants, achieving a high compression ratio and pressure and temperature in the reactor needed for monosilane pyrolysis. Pyrolysis in the flow reactor is convenient, technological and efficient in terms of its use in the production of high purity nanopowders.
AB - The method of producing nanopowders of Si and SiC by pyrolysis of a silicon-hydrocarbon mixture by compression in a cyclic process in a flow reactor is proposed and implemented. The obtained powders are characterized by X-ray diffraction and transmission electron microscopy. The new design solutions and use of ceramic coatings obtained by applying microarc oxidation for the piston-cylinder assembly - a compression unit of the reactor - allowed avoiding the use of compression rings and lubricants, achieving a high compression ratio and pressure and temperature in the reactor needed for monosilane pyrolysis. Pyrolysis in the flow reactor is convenient, technological and efficient in terms of its use in the production of high purity nanopowders.
KW - SILICON-CARBIDE
KW - POWDERS
UR - http://www.scopus.com/inward/record.url?scp=85058637715&partnerID=8YFLogxK
U2 - 10.1088/1742-6596/1128/1/012100
DO - 10.1088/1742-6596/1128/1/012100
M3 - Conference article
AN - SCOPUS:85058637715
VL - 1128
JO - Journal of Physics: Conference Series
JF - Journal of Physics: Conference Series
SN - 1742-6588
IS - 1
M1 - 012100
T2 - 3rd All-Russian Scientific Conference Thermophysics and Physical Hydrodynamics with the School for Young Scientists, TPH 2018
Y2 - 10 September 2018 through 16 September 2018
ER -
ID: 17878491