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New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range. / Panchenko, A. V.; Serebrennikova, P. S.; Komarov, V. Yu et al.

In: Journal of Structural Chemistry, Vol. 64, No. 8, 08.2023, p. 1399-1411.

Research output: Contribution to journal › Article › peer-review

Harvard

Panchenko, AV, Serebrennikova, PS, Komarov, VY & Gromilov, SA 2023, 'New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range', Journal of Structural Chemistry, vol. 64, no. 8, pp. 1399-1411. https://doi.org/10.1134/S002247662308005X

APA

Panchenko, A. V., Serebrennikova, P. S., Komarov, V. Y., & Gromilov, S. A. (2023). New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range. Journal of Structural Chemistry, 64(8), 1399-1411. https://doi.org/10.1134/S002247662308005X

Vancouver

Panchenko AV, Serebrennikova PS, Komarov VY, Gromilov SA. New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range. Journal of Structural Chemistry. 2023 Aug;64(8):1399-1411. doi: 10.1134/S002247662308005X

Author

Panchenko, A. V. ; Serebrennikova, P. S. ; Komarov, V. Yu et al. / New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range. In: Journal of Structural Chemistry. 2023 ; Vol. 64, No. 8. pp. 1399-1411.

BibTeX

@article{7c4ca3f8905649938af8670b4486a57b,
title = "New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range",
abstract = "New techniques for the calibration of single-crystal diffractometers equipped with a 2D detector are proposed to improve the accuracy of measuring the unit cell parameters. According to these methods, reflection profiles are processed using the original SearchXY-2θ program, and the detector position is refined by recording an external reference. Details of the calibration of diffractometers equipped with a three- or four-circle goniometer are discussed. The use of reflections with 2θ ≈ 100° when refining the unit cell parameters of a test InSb single crystal allowed measuring parameter a of the cubic unit cell with a relative error of 7·10–5. The possibilities of the techniques are also demonstrated on the measurements of the a(T) dependence for InSb in the range of 90-490 K.",
keywords = "2D detector, InSb single crystal, accuracy of measuring unit cell parameters, diffraction data processing, goniometer calibration, high-temperature X-ray diffraction, single-crystal diffractometer",
author = "Panchenko, {A. V.} and Serebrennikova, {P. S.} and Komarov, {V. Yu} and Gromilov, {S. A.}",
note = "This work was funded by the Ministry of Science and Higher Education of the Russian Federation (project No. 21031700313-8) and by the Priority–2030 program.",
year = "2023",
month = aug,
doi = "10.1134/S002247662308005X",
language = "English",
volume = "64",
pages = "1399--1411",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "8",

}

RIS

TY - JOUR

T1 - New Approaches to the Diffractometer Calibration. Study of InSb in the 90-490 K Temperature Range

AU - Panchenko, A. V.

AU - Serebrennikova, P. S.

AU - Komarov, V. Yu

AU - Gromilov, S. A.

N1 - This work was funded by the Ministry of Science and Higher Education of the Russian Federation (project No. 21031700313-8) and by the Priority–2030 program.

PY - 2023/8

Y1 - 2023/8

N2 - New techniques for the calibration of single-crystal diffractometers equipped with a 2D detector are proposed to improve the accuracy of measuring the unit cell parameters. According to these methods, reflection profiles are processed using the original SearchXY-2θ program, and the detector position is refined by recording an external reference. Details of the calibration of diffractometers equipped with a three- or four-circle goniometer are discussed. The use of reflections with 2θ ≈ 100° when refining the unit cell parameters of a test InSb single crystal allowed measuring parameter a of the cubic unit cell with a relative error of 7·10–5. The possibilities of the techniques are also demonstrated on the measurements of the a(T) dependence for InSb in the range of 90-490 K.

AB - New techniques for the calibration of single-crystal diffractometers equipped with a 2D detector are proposed to improve the accuracy of measuring the unit cell parameters. According to these methods, reflection profiles are processed using the original SearchXY-2θ program, and the detector position is refined by recording an external reference. Details of the calibration of diffractometers equipped with a three- or four-circle goniometer are discussed. The use of reflections with 2θ ≈ 100° when refining the unit cell parameters of a test InSb single crystal allowed measuring parameter a of the cubic unit cell with a relative error of 7·10–5. The possibilities of the techniques are also demonstrated on the measurements of the a(T) dependence for InSb in the range of 90-490 K.

KW - 2D detector

KW - InSb single crystal

KW - accuracy of measuring unit cell parameters

KW - diffraction data processing

KW - goniometer calibration

KW - high-temperature X-ray diffraction

KW - single-crystal diffractometer

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-85169612304&origin=inward&txGid=7c4da0cf84ee80564b06b056f38abe2c

UR - https://www.mendeley.com/catalogue/dd1d9fd4-c5dc-3d84-ae5c-6ac8a23bd23e/

U2 - 10.1134/S002247662308005X

DO - 10.1134/S002247662308005X

M3 - Article

VL - 64

SP - 1399

EP - 1411

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 8

ER -

ID: 59235431