Standard
Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75) : Synthesis, structure, thermal properties. / Makotchenko, E. V.; Plyusnin, P. E.; Shubin, Yu V. et al.
In:
Russian Journal of Inorganic Chemistry, Vol. 62, No. 1, 01.01.2017, p. 12-21.
Research output: Contribution to journal › Article › peer-review
Harvard
Makotchenko, EV
, Plyusnin, PE, Shubin, YV, Baidina, IA, Korol’kov, IV, Sheludyakova, LA
& Korenev, SV 2017, '
Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75): Synthesis, structure, thermal properties',
Russian Journal of Inorganic Chemistry, vol. 62, no. 1, pp. 12-21.
https://doi.org/10.1134/S0036023617010119
APA
Makotchenko, E. V.
, Plyusnin, P. E., Shubin, Y. V., Baidina, I. A., Korol’kov, I. V., Sheludyakova, L. A.
, & Korenev, S. V. (2017).
Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75): Synthesis, structure, thermal properties.
Russian Journal of Inorganic Chemistry,
62(1), 12-21.
https://doi.org/10.1134/S0036023617010119
Vancouver
Makotchenko EV
, Plyusnin PE, Shubin YV, Baidina IA, Korol’kov IV, Sheludyakova LA et al.
Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75): Synthesis, structure, thermal properties.
Russian Journal of Inorganic Chemistry. 2017 Jan 1;62(1):12-21. doi: 10.1134/S0036023617010119
Author
Makotchenko, E. V.
; Plyusnin, P. E. ; Shubin, Yu V. et al. /
Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75) : Synthesis, structure, thermal properties. In:
Russian Journal of Inorganic Chemistry. 2017 ; Vol. 62, No. 1. pp. 12-21.
BibTeX
@article{b2f4bd75cc0c434fa362fa1e3ecb865e,
title = "Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75): Synthesis, structure, thermal properties",
abstract = "The double complex salts [Au(En)2][Ir(NO2)6] • 2H2O (I) and [Au(En)2][Ir(NO2)6] (II) and solid solutions [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O, where x = 0.25, 0.5, 0.75, were prepared and characterized by powder X-ray diffraction, IR spectroscopy, elemental analysis, and DTA. The crystal structures were determined by X-ray diffraction. The thermal behavior of compounds under reducing atmosphere was studied. The final products of thermolysis were found to be two-phase mixtures consisting of nano-sized pure gold particles (~55 nm) and particles of Au–Ir–Rh solid solutions (~3 nm).",
keywords = "CRYSTAL-STRUCTURE, DEPOSITION PRECIPITATION, DECOMPOSITION, CATALYSTS, GOLD(III), GOLD, RH, IR",
author = "Makotchenko, {E. V.} and Plyusnin, {P. E.} and Shubin, {Yu V.} and Baidina, {I. A.} and Korol{\textquoteright}kov, {I. V.} and Sheludyakova, {L. A.} and Korenev, {S. V.}",
year = "2017",
month = jan,
day = "1",
doi = "10.1134/S0036023617010119",
language = "English",
volume = "62",
pages = "12--21",
journal = "Russian Journal of Inorganic Chemistry",
issn = "0036-0236",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "1",
}
RIS
TY - JOUR
T1 - Double complex salts [Au(En)2][Ir(NO2)6] • nH2O (n = 0, 2), [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O (x = 0.25, 0.5, 0.75)
T2 - Synthesis, structure, thermal properties
AU - Makotchenko, E. V.
AU - Plyusnin, P. E.
AU - Shubin, Yu V.
AU - Baidina, I. A.
AU - Korol’kov, I. V.
AU - Sheludyakova, L. A.
AU - Korenev, S. V.
PY - 2017/1/1
Y1 - 2017/1/1
N2 - The double complex salts [Au(En)2][Ir(NO2)6] • 2H2O (I) and [Au(En)2][Ir(NO2)6] (II) and solid solutions [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O, where x = 0.25, 0.5, 0.75, were prepared and characterized by powder X-ray diffraction, IR spectroscopy, elemental analysis, and DTA. The crystal structures were determined by X-ray diffraction. The thermal behavior of compounds under reducing atmosphere was studied. The final products of thermolysis were found to be two-phase mixtures consisting of nano-sized pure gold particles (~55 nm) and particles of Au–Ir–Rh solid solutions (~3 nm).
AB - The double complex salts [Au(En)2][Ir(NO2)6] • 2H2O (I) and [Au(En)2][Ir(NO2)6] (II) and solid solutions [Au(En)2][Ir(NO2)6]x[Rh(NO2)6]1–x • nH2O, where x = 0.25, 0.5, 0.75, were prepared and characterized by powder X-ray diffraction, IR spectroscopy, elemental analysis, and DTA. The crystal structures were determined by X-ray diffraction. The thermal behavior of compounds under reducing atmosphere was studied. The final products of thermolysis were found to be two-phase mixtures consisting of nano-sized pure gold particles (~55 nm) and particles of Au–Ir–Rh solid solutions (~3 nm).
KW - CRYSTAL-STRUCTURE
KW - DEPOSITION PRECIPITATION
KW - DECOMPOSITION
KW - CATALYSTS
KW - GOLD(III)
KW - GOLD
KW - RH
KW - IR
UR - http://www.scopus.com/inward/record.url?scp=85013167780&partnerID=8YFLogxK
U2 - 10.1134/S0036023617010119
DO - 10.1134/S0036023617010119
M3 - Article
AN - SCOPUS:85013167780
VL - 62
SP - 12
EP - 21
JO - Russian Journal of Inorganic Chemistry
JF - Russian Journal of Inorganic Chemistry
SN - 0036-0236
IS - 1
ER -