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Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O. / Petrov, P. A.; Sosnin, G. A.; Naumov, D. Yu et al.

In: Journal of Structural Chemistry, Vol. 56, No. 4, 30.07.2015, p. 765-768.

Research output: Contribution to journal › Article › peer-review

Harvard

Petrov, PA, Sosnin, GA, Naumov, DY & Konchenko, SN 2015, 'Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O', Journal of Structural Chemistry, vol. 56, no. 4, pp. 765-768. https://doi.org/10.1134/S002247661504023X

APA

Petrov, P. A., Sosnin, G. A., Naumov, D. Y., & Konchenko, S. N. (2015). Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O. Journal of Structural Chemistry, 56(4), 765-768. https://doi.org/10.1134/S002247661504023X

Vancouver

Petrov PA, Sosnin GA, Naumov DY, Konchenko SN. Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O. Journal of Structural Chemistry. 2015 Jul 30;56(4):765-768. doi: 10.1134/S002247661504023X

Author

Petrov, P. A. ; Sosnin, G. A. ; Naumov, D. Yu et al. / Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O. In: Journal of Structural Chemistry. 2015 ; Vol. 56, No. 4. pp. 765-768.

BibTeX

@article{7cf4f540900b4a789a7d671f60005ffb,
title = "Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O",
abstract = "The seven-electron neutral cluster complex [Mo3S4(dppe)3Cl3] (dppe = Ph2PCH2CH2PPh2) is obtained by the reduction of the [Mo3S4(dppe)3Cl3]Cl cluster with gallium metal. The molecular and crystal structure of [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O solvate is determined by single crystal XRD. The crystallographic data are as follows: monoclinic crystal symmetry, space group C2/c, a = 41.1775(16) {\AA}, b = 17.7178(7) {\AA}, c = 28.9609(9) {\AA}, β = 110.363(1)°, V = 19808.7(13) {\AA}3, Z = 8, d calc = 1.384 g/cm3.",
keywords = "cluster complexes, molybdenum, single crystal X-ray diffraction study, sulfur",
author = "Petrov, {P. A.} and Sosnin, {G. A.} and Naumov, {D. Yu} and Konchenko, {S. N.}",
year = "2015",
month = jul,
day = "30",
doi = "10.1134/S002247661504023X",
language = "English",
volume = "56",
pages = "765--768",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "4",

}

RIS

TY - JOUR

T1 - Crystal structure of the seven-electron molybdenum cluster [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O

AU - Petrov, P. A.

AU - Sosnin, G. A.

AU - Naumov, D. Yu

AU - Konchenko, S. N.

PY - 2015/7/30

Y1 - 2015/7/30

N2 - The seven-electron neutral cluster complex [Mo3S4(dppe)3Cl3] (dppe = Ph2PCH2CH2PPh2) is obtained by the reduction of the [Mo3S4(dppe)3Cl3]Cl cluster with gallium metal. The molecular and crystal structure of [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O solvate is determined by single crystal XRD. The crystallographic data are as follows: monoclinic crystal symmetry, space group C2/c, a = 41.1775(16) Å, b = 17.7178(7) Å, c = 28.9609(9) Å, β = 110.363(1)°, V = 19808.7(13) Å3, Z = 8, d calc = 1.384 g/cm3.

AB - The seven-electron neutral cluster complex [Mo3S4(dppe)3Cl3] (dppe = Ph2PCH2CH2PPh2) is obtained by the reduction of the [Mo3S4(dppe)3Cl3]Cl cluster with gallium metal. The molecular and crystal structure of [Mo3S4(dppe)3Cl3]3.5C4H8O20.5Et2O solvate is determined by single crystal XRD. The crystallographic data are as follows: monoclinic crystal symmetry, space group C2/c, a = 41.1775(16) Å, b = 17.7178(7) Å, c = 28.9609(9) Å, β = 110.363(1)°, V = 19808.7(13) Å3, Z = 8, d calc = 1.384 g/cm3.

KW - cluster complexes

KW - molybdenum

KW - single crystal X-ray diffraction study

KW - sulfur

UR - http://www.scopus.com/inward/record.url?scp=84942518556&partnerID=8YFLogxK

U2 - 10.1134/S002247661504023X

DO - 10.1134/S002247661504023X

M3 - Article

AN - SCOPUS:84942518556

VL - 56

SP - 765

EP - 768

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 4

ER -

ID: 25415283