Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products. / Petrov, P. A.; Filippova, E. A.; Kompankov, N. B. и др.
в: Journal of Structural Chemistry, Том 63, № 3, 9, 03.2022, стр. 470-475.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products
AU - Petrov, P. A.
AU - Filippova, E. A.
AU - Kompankov, N. B.
AU - Sukhikh, T. S.
AU - Sokolov, M. N.
N1 - Funding Information: The work was supported by the Ministry of Science and Higher Education of the Russian Federation within the State Assignment for the Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences (project No. 121031700313-8). Publisher Copyright: © 2022, Pleiades Publishing, Ltd.
PY - 2022/3
Y1 - 2022/3
N2 - A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex is synthesized and characterized by single crystal X-ray diffraction (XRD). Its recrystallization from the CH2Cl2/ROH (R = Me, Et) mixture is found to result in the formation of the [ReVOCl2(OR)(PPh3)2] – its oxidation product. The crystal structure of the new [ReOCl2(OEt)(PPh3)2] polymorph is determined by single crystal XRD.
AB - A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex is synthesized and characterized by single crystal X-ray diffraction (XRD). Its recrystallization from the CH2Cl2/ROH (R = Me, Et) mixture is found to result in the formation of the [ReVOCl2(OR)(PPh3)2] – its oxidation product. The crystal structure of the new [ReOCl2(OEt)(PPh3)2] polymorph is determined by single crystal XRD.
KW - phosphines
KW - rhenium
KW - single crystal X-ray diffraction analysis
UR - http://www.scopus.com/inward/record.url?scp=85131764663&partnerID=8YFLogxK
UR - https://www.elibrary.ru/item.asp?id=48721085
UR - https://www.mendeley.com/catalogue/5ba46c5a-77e5-3a0b-8a8d-115e67589bda/
U2 - 10.1134/S0022476622030131
DO - 10.1134/S0022476622030131
M3 - Article
AN - SCOPUS:85131764663
VL - 63
SP - 470
EP - 475
JO - Journal of Structural Chemistry
JF - Journal of Structural Chemistry
SN - 0022-4766
IS - 3
M1 - 9
ER -
ID: 36434605