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A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products. / Petrov, P. A.; Filippova, E. A.; Kompankov, N. B. et al.

In: Journal of Structural Chemistry, Vol. 63, No. 3, 9, 03.2022, p. 470-475.

Research output: Contribution to journal › Article › peer-review

Harvard

Petrov, PA, Filippova, EA, Kompankov, NB, Sukhikh, TS & Sokolov, MN 2022, 'A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products', Journal of Structural Chemistry, vol. 63, no. 3, 9, pp. 470-475. https://doi.org/10.1134/S0022476622030131

APA

Petrov, P. A., Filippova, E. A., Kompankov, N. B., Sukhikh, T. S., & Sokolov, M. N. (2022). A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products. Journal of Structural Chemistry, 63(3), 470-475. [9]. https://doi.org/10.1134/S0022476622030131

Vancouver

Petrov PA, Filippova EA, Kompankov NB, Sukhikh TS, Sokolov MN. A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products. Journal of Structural Chemistry. 2022 Mar;63(3):470-475. 9. doi: 10.1134/S0022476622030131

Author

Petrov, P. A. ; Filippova, E. A. ; Kompankov, N. B. et al. / A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products. In: Journal of Structural Chemistry. 2022 ; Vol. 63, No. 3. pp. 470-475.

BibTeX

@article{23a6ab7ce1d34426bb4466e9cf4f1389,
title = "A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products",
abstract = "A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex is synthesized and characterized by single crystal X-ray diffraction (XRD). Its recrystallization from the CH2Cl2/ROH (R = Me, Et) mixture is found to result in the formation of the [ReVOCl2(OR)(PPh3)2] – its oxidation product. The crystal structure of the new [ReOCl2(OEt)(PPh3)2] polymorph is determined by single crystal XRD.",
keywords = "phosphines, rhenium, single crystal X-ray diffraction analysis",
author = "Petrov, {P. A.} and Filippova, {E. A.} and Kompankov, {N. B.} and Sukhikh, {T. S.} and Sokolov, {M. N.}",
note = "Funding Information: The work was supported by the Ministry of Science and Higher Education of the Russian Federation within the State Assignment for the Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences (project No. 121031700313-8). Publisher Copyright: {\textcopyright} 2022, Pleiades Publishing, Ltd.",
year = "2022",
month = mar,
doi = "10.1134/S0022476622030131",
language = "English",
volume = "63",
pages = "470--475",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "3",

}

RIS

TY - JOUR

T1 - A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex and its oxidation products

AU - Petrov, P. A.

AU - Filippova, E. A.

AU - Kompankov, N. B.

AU - Sukhikh, T. S.

AU - Sokolov, M. N.

N1 - Funding Information: The work was supported by the Ministry of Science and Higher Education of the Russian Federation within the State Assignment for the Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences (project No. 121031700313-8). Publisher Copyright: © 2022, Pleiades Publishing, Ltd.

PY - 2022/3

Y1 - 2022/3

N2 - A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex is synthesized and characterized by single crystal X-ray diffraction (XRD). Its recrystallization from the CH2Cl2/ROH (R = Me, Et) mixture is found to result in the formation of the [ReVOCl2(OR)(PPh3)2] – its oxidation product. The crystal structure of the new [ReOCl2(OEt)(PPh3)2] polymorph is determined by single crystal XRD.

AB - A new polymorph of the [ReCl3(MeCN)(PPh3)2] complex is synthesized and characterized by single crystal X-ray diffraction (XRD). Its recrystallization from the CH2Cl2/ROH (R = Me, Et) mixture is found to result in the formation of the [ReVOCl2(OR)(PPh3)2] – its oxidation product. The crystal structure of the new [ReOCl2(OEt)(PPh3)2] polymorph is determined by single crystal XRD.

KW - phosphines

KW - rhenium

KW - single crystal X-ray diffraction analysis

UR - http://www.scopus.com/inward/record.url?scp=85131764663&partnerID=8YFLogxK

UR - https://www.elibrary.ru/item.asp?id=48721085

UR - https://www.mendeley.com/catalogue/5ba46c5a-77e5-3a0b-8a8d-115e67589bda/

U2 - 10.1134/S0022476622030131

DO - 10.1134/S0022476622030131

M3 - Article

AN - SCOPUS:85131764663

VL - 63

SP - 470

EP - 475

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 3

M1 - 9

ER -

ID: 36434605