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Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex. / Shmakova, A. A.; Abramov, P. A.; Sokolov, M. N.

In: Journal of Structural Chemistry, Vol. 60, No. 7, 01.07.2019, p. 1080-1085.

Research output: Contribution to journal › Article › peer-review

Harvard

Shmakova, AA, Abramov, PA & Sokolov, MN 2019, 'Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex', Journal of Structural Chemistry, vol. 60, no. 7, pp. 1080-1085. https://doi.org/10.1134/S0022476619070084

APA

Shmakova, A. A., Abramov, P. A., & Sokolov, M. N. (2019). Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex. Journal of Structural Chemistry, 60(7), 1080-1085. https://doi.org/10.1134/S0022476619070084

Vancouver

Shmakova AA, Abramov PA, Sokolov MN. Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex. Journal of Structural Chemistry. 2019 Jul 1;60(7):1080-1085. doi: 10.1134/S0022476619070084

Author

Shmakova, A. A. ; Abramov, P. A. ; Sokolov, M. N. / Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex. In: Journal of Structural Chemistry. 2019 ; Vol. 60, No. 7. pp. 1080-1085.

BibTeX

@article{0ecb27db6e0f4e7186610a202771d659,
title = "Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex",
abstract = "The bis(oxalate) complex of niobium (NH4)[NbO(C2O4)2(H2O)2]·3H2O can be dissolved in DMF on heating. Ether diffusion into this solution in the presence of Et4NBr leads to the formation of colorless crystals of (Et4N)4[Nb2O2(C2O4)4(μ-C2O4)] (1). The characterization of the obtained compound by single crystal and powder XRD, IR and Raman spectroscopy, and elemental analysis allows to clarify processes occurring with the bis(oxalate) niobium complex in aqueous solutions.",
keywords = "crystal structure, niobium, oxalate complex, ACIDS, CRYSTAL-STRUCTURE, TANTALUM, WATER-SOLUBLE COMPLEXES, NIOBIUM COLUMBIUM",
author = "Shmakova, {A. A.} and Abramov, {P. A.} and Sokolov, {M. N.}",
year = "2019",
month = jul,
day = "1",
doi = "10.1134/S0022476619070084",
language = "English",
volume = "60",
pages = "1080--1085",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "7",

}

RIS

TY - JOUR

T1 - Synthesis, Structure, and Spectral Studies of the (Et4N)4[Nb2O2(C2O4)4(µ-C2O4)] Complex

AU - Shmakova, A. A.

AU - Abramov, P. A.

AU - Sokolov, M. N.

PY - 2019/7/1

Y1 - 2019/7/1

N2 - The bis(oxalate) complex of niobium (NH4)[NbO(C2O4)2(H2O)2]·3H2O can be dissolved in DMF on heating. Ether diffusion into this solution in the presence of Et4NBr leads to the formation of colorless crystals of (Et4N)4[Nb2O2(C2O4)4(μ-C2O4)] (1). The characterization of the obtained compound by single crystal and powder XRD, IR and Raman spectroscopy, and elemental analysis allows to clarify processes occurring with the bis(oxalate) niobium complex in aqueous solutions.

AB - The bis(oxalate) complex of niobium (NH4)[NbO(C2O4)2(H2O)2]·3H2O can be dissolved in DMF on heating. Ether diffusion into this solution in the presence of Et4NBr leads to the formation of colorless crystals of (Et4N)4[Nb2O2(C2O4)4(μ-C2O4)] (1). The characterization of the obtained compound by single crystal and powder XRD, IR and Raman spectroscopy, and elemental analysis allows to clarify processes occurring with the bis(oxalate) niobium complex in aqueous solutions.

KW - crystal structure

KW - niobium

KW - oxalate complex

KW - ACIDS

KW - CRYSTAL-STRUCTURE

KW - TANTALUM

KW - WATER-SOLUBLE COMPLEXES

KW - NIOBIUM COLUMBIUM

UR - http://www.scopus.com/inward/record.url?scp=85070233790&partnerID=8YFLogxK

U2 - 10.1134/S0022476619070084

DO - 10.1134/S0022476619070084

M3 - Article

AN - SCOPUS:85070233790

VL - 60

SP - 1080

EP - 1085

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 7

ER -

ID: 21237789