Research output: Contribution to journal › Article › peer-review
Synthesis of highly dispersed vanadium diboride with the use of nanofibrous carbon. / Krutskii, Yu L.; Maksimovskii, E. A.; Krutskaya, T. M. et al.
In: Russian Journal of Applied Chemistry, Vol. 90, No. 9, 01.09.2017, p. 1379-1385.Research output: Contribution to journal › Article › peer-review
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TY - JOUR
T1 - Synthesis of highly dispersed vanadium diboride with the use of nanofibrous carbon
AU - Krutskii, Yu L.
AU - Maksimovskii, E. A.
AU - Krutskaya, T. M.
AU - Popov, M. V.
AU - Netskina, O. V.
AU - Nikulina, A. A.
AU - Cherkasova, N. Yu
AU - Kvashina, T. S.
N1 - Publisher Copyright: © 2017, Pleiades Publishing, Ltd.
PY - 2017/9/1
Y1 - 2017/9/1
N2 - Reduction of vanadium(III) oxide with boron carbide and nanofibrous carbon in an induction furnace in argon was used to obtain a highly dispersed vanadium diboride powder. The characteristics of vanadium diboride powders were studied by various analytical methods. It was found that the material obtained contains only a single phase, vanadium diboride, with powder particles mostly aggregated, the average size of particles and aggregates being 9.8 μm at a wide particle size distribution. The optimal synthesis parameters were determined: V2O3: B4C: C ratio corresponding to the stoichiometry, temperature 1700°C, and keeping time 20 min.
AB - Reduction of vanadium(III) oxide with boron carbide and nanofibrous carbon in an induction furnace in argon was used to obtain a highly dispersed vanadium diboride powder. The characteristics of vanadium diboride powders were studied by various analytical methods. It was found that the material obtained contains only a single phase, vanadium diboride, with powder particles mostly aggregated, the average size of particles and aggregates being 9.8 μm at a wide particle size distribution. The optimal synthesis parameters were determined: V2O3: B4C: C ratio corresponding to the stoichiometry, temperature 1700°C, and keeping time 20 min.
KW - IRON BORIDE BATTERY
KW - MOLECULAR-OXYGEN
KW - METAL BORIDES
KW - HIGH-CAPACITY
KW - OXIDATION
UR - http://www.scopus.com/inward/record.url?scp=85040126140&partnerID=8YFLogxK
U2 - 10.1134/S1070427217090014
DO - 10.1134/S1070427217090014
M3 - Article
AN - SCOPUS:85040126140
VL - 90
SP - 1379
EP - 1385
JO - Russian Journal of Applied Chemistry
JF - Russian Journal of Applied Chemistry
SN - 1070-4272
IS - 9
ER -
ID: 9060373