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Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions. / Timakova, E. V.; Afonina, L. I.; Bulina, N. V. et al.

In: Russian Journal of Applied Chemistry, Vol. 90, No. 7, 01.07.2017, p. 1040-1046.

Research output: Contribution to journal › Article › peer-review

Harvard

Timakova, EV, Afonina, LI, Bulina, NV, Shatskaya, SS, Yukhin, YM & Volodin, VA 2017, 'Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions', Russian Journal of Applied Chemistry, vol. 90, no. 7, pp. 1040-1046. https://doi.org/10.1134/S1070427217070035

APA

Timakova, E. V., Afonina, L. I., Bulina, N. V., Shatskaya, S. S., Yukhin, Y. M., & Volodin, V. A. (2017). Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions. Russian Journal of Applied Chemistry, 90(7), 1040-1046. https://doi.org/10.1134/S1070427217070035

Vancouver

Timakova EV, Afonina LI, Bulina NV, Shatskaya SS, Yukhin YM, Volodin VA. Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions. Russian Journal of Applied Chemistry. 2017 Jul 1;90(7):1040-1046. doi: 10.1134/S1070427217070035

Author

Timakova, E. V. ; Afonina, L. I. ; Bulina, N. V. et al. / Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions. In: Russian Journal of Applied Chemistry. 2017 ; Vol. 90, No. 7. pp. 1040-1046.

BibTeX

@article{b7b98d054e5344d89410ca86e91bee35,
title = "Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions",
abstract = "Conditions were determined in which basic bismuth oxalate of composition BiC2O4(OH) can be obtained by direct precipitation upon addition of oxalic acid from nitrate solutions used in production of bismuth compounds. The composition of the compound was confirmed by X-ray phase and chemical analyses, IR and Raman spectroscopy, and thermogravimetry. Electron microscopy was used to examine the effect of the composition of the reaction medium and temperature on the morphology of the product being obtained. It was shown that β-Bi2O3 can be obtained in oxidative thermolysis of basic bismuth oxalate, depending on its morphology.",
keywords = "RATE THERMAL-ANALYSIS, TRANSFORMATION, BI2O3",
author = "Timakova, {E. V.} and Afonina, {L. I.} and Bulina, {N. V.} and Shatskaya, {S. S.} and Yukhin, {Yu M.} and Volodin, {V. A.}",
year = "2017",
month = jul,
day = "1",
doi = "10.1134/S1070427217070035",
language = "English",
volume = "90",
pages = "1040--1046",
journal = "Russian Journal of Applied Chemistry",
issn = "1070-4272",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "7",

}

RIS

TY - JOUR

T1 - Synthesis of basic bismuth(III) oxalate by precipitation from nitrate solutions

AU - Timakova, E. V.

AU - Afonina, L. I.

AU - Bulina, N. V.

AU - Shatskaya, S. S.

AU - Yukhin, Yu M.

AU - Volodin, V. A.

PY - 2017/7/1

Y1 - 2017/7/1

N2 - Conditions were determined in which basic bismuth oxalate of composition BiC2O4(OH) can be obtained by direct precipitation upon addition of oxalic acid from nitrate solutions used in production of bismuth compounds. The composition of the compound was confirmed by X-ray phase and chemical analyses, IR and Raman spectroscopy, and thermogravimetry. Electron microscopy was used to examine the effect of the composition of the reaction medium and temperature on the morphology of the product being obtained. It was shown that β-Bi2O3 can be obtained in oxidative thermolysis of basic bismuth oxalate, depending on its morphology.

AB - Conditions were determined in which basic bismuth oxalate of composition BiC2O4(OH) can be obtained by direct precipitation upon addition of oxalic acid from nitrate solutions used in production of bismuth compounds. The composition of the compound was confirmed by X-ray phase and chemical analyses, IR and Raman spectroscopy, and thermogravimetry. Electron microscopy was used to examine the effect of the composition of the reaction medium and temperature on the morphology of the product being obtained. It was shown that β-Bi2O3 can be obtained in oxidative thermolysis of basic bismuth oxalate, depending on its morphology.

KW - RATE THERMAL-ANALYSIS

KW - TRANSFORMATION

KW - BI2O3

UR - http://www.scopus.com/inward/record.url?scp=85034226941&partnerID=8YFLogxK

U2 - 10.1134/S1070427217070035

DO - 10.1134/S1070427217070035

M3 - Article

AN - SCOPUS:85034226941

VL - 90

SP - 1040

EP - 1046

JO - Russian Journal of Applied Chemistry

JF - Russian Journal of Applied Chemistry

SN - 1070-4272

IS - 7

ER -

ID: 9674861