Standard

Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane). / Bykova, E. A.; Khranenko, S. P.; Gromilov, S. A.

In: Journal of Structural Chemistry, Vol. 59, No. 1, 01.01.2018, p. 172-176.

Research output: Contribution to journal › Article › peer-review

Harvard

Bykova, EA, Khranenko, SP & Gromilov, SA 2018, 'Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane)', Journal of Structural Chemistry, vol. 59, no. 1, pp. 172-176. https://doi.org/10.1134/S0022476618010262

APA

Bykova, E. A., Khranenko, S. P., & Gromilov, S. A. (2018). Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane). Journal of Structural Chemistry, 59(1), 172-176. https://doi.org/10.1134/S0022476618010262

Vancouver

Bykova EA, Khranenko SP, Gromilov SA. Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane). Journal of Structural Chemistry. 2018 Jan 1;59(1):172-176. doi: 10.1134/S0022476618010262

Author

Bykova, E. A. ; Khranenko, S. P. ; Gromilov, S. A. / Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane). In: Journal of Structural Chemistry. 2018 ; Vol. 59, No. 1. pp. 172-176.

BibTeX

@article{19c8f89524d3482ca073ddd25b3e48c6,
title = "Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane)",
abstract = "The crystal structures of [CuL2](ReO4)2 and [NiL2](ReO4)2 (L = 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraaza-cyclotetradecane) are studied. The crystal structural data for [CuL2](ReO4)2, C16H32CuN4O8Re2: a = 13.5523(7) {\AA}, b = 9.3446(4) {\AA}, c = 18.4410(9) {\AA}, V = 2335.38(19) {\AA}3, space group Pbca, Z = 4, dx = 2.402 g/cm3; the copper atom coordination C–N of (2×)1.973(5) {\AA} and (2×)2.008(5) {\AA}, the additional coordination Cu…O of (2×)2.642 {\AA}. The crystal structural data for [NiL2](ReO4)2, C16H32NiN4O8Re2: a = 8.9308(2) {\AA}, b = 14.3479(3) {\AA}, c = 18.6501(4) {\AA}, β = 91.492(1)°, V = 2388.98(9) {\AA}3, space group P21/c, Z = 4, dx = 2.334 g/cm3; the nickel atom coordination Ni–N of 1.889(4)-1.917(3) {\AA}, the additional coordination Ni…O of 2.750(3) {\AA}.",
keywords = "copper, crystal chemistry, macrocyclic ligand, nickel, perrhenate anion, single crystal X-ray diffraction, structural packing, CRYSTAL-STRUCTURE, COORDINATION",
author = "Bykova, {E. A.} and Khranenko, {S. P.} and Gromilov, {S. A.}",
year = "2018",
month = jan,
day = "1",
doi = "10.1134/S0022476618010262",
language = "English",
volume = "59",
pages = "172--176",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "1",

}

RIS

TY - JOUR

T1 - Structural Packing Features of [ML 2](ReO4)2 (M = Cu, Ni; L = 5,5,7,12,12,14-Hexamethyl-1,4,8,11-Tetraaza-Cyclotetradecane)

AU - Bykova, E. A.

AU - Khranenko, S. P.

AU - Gromilov, S. A.

PY - 2018/1/1

Y1 - 2018/1/1

N2 - The crystal structures of [CuL2](ReO4)2 and [NiL2](ReO4)2 (L = 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraaza-cyclotetradecane) are studied. The crystal structural data for [CuL2](ReO4)2, C16H32CuN4O8Re2: a = 13.5523(7) Å, b = 9.3446(4) Å, c = 18.4410(9) Å, V = 2335.38(19) Å3, space group Pbca, Z = 4, dx = 2.402 g/cm3; the copper atom coordination C–N of (2×)1.973(5) Å and (2×)2.008(5) Å, the additional coordination Cu…O of (2×)2.642 Å. The crystal structural data for [NiL2](ReO4)2, C16H32NiN4O8Re2: a = 8.9308(2) Å, b = 14.3479(3) Å, c = 18.6501(4) Å, β = 91.492(1)°, V = 2388.98(9) Å3, space group P21/c, Z = 4, dx = 2.334 g/cm3; the nickel atom coordination Ni–N of 1.889(4)-1.917(3) Å, the additional coordination Ni…O of 2.750(3) Å.

AB - The crystal structures of [CuL2](ReO4)2 and [NiL2](ReO4)2 (L = 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraaza-cyclotetradecane) are studied. The crystal structural data for [CuL2](ReO4)2, C16H32CuN4O8Re2: a = 13.5523(7) Å, b = 9.3446(4) Å, c = 18.4410(9) Å, V = 2335.38(19) Å3, space group Pbca, Z = 4, dx = 2.402 g/cm3; the copper atom coordination C–N of (2×)1.973(5) Å and (2×)2.008(5) Å, the additional coordination Cu…O of (2×)2.642 Å. The crystal structural data for [NiL2](ReO4)2, C16H32NiN4O8Re2: a = 8.9308(2) Å, b = 14.3479(3) Å, c = 18.6501(4) Å, β = 91.492(1)°, V = 2388.98(9) Å3, space group P21/c, Z = 4, dx = 2.334 g/cm3; the nickel atom coordination Ni–N of 1.889(4)-1.917(3) Å, the additional coordination Ni…O of 2.750(3) Å.

KW - copper

KW - crystal chemistry

KW - macrocyclic ligand

KW - nickel

KW - perrhenate anion

KW - single crystal X-ray diffraction

KW - structural packing

KW - CRYSTAL-STRUCTURE

KW - COORDINATION

UR - http://www.scopus.com/inward/record.url?scp=85044083166&partnerID=8YFLogxK

U2 - 10.1134/S0022476618010262

DO - 10.1134/S0022476618010262

M3 - Article

AN - SCOPUS:85044083166

VL - 59

SP - 172

EP - 176

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 1

ER -

ID: 12155390