Small angle X-ray scattering study for supported catalysts: From solids to sols

Standard

Small angle X-ray scattering study for supported catalysts: From solids to sols. / Larichev, Yu V.

In: Nano-Structures and Nano-Objects, Vol. 25, 100647, 02.2021.

Research output: Contribution to journal › Article › peer-review

Harvard

Larichev, YV 2021, 'Small angle X-ray scattering study for supported catalysts: From solids to sols', Nano-Structures and Nano-Objects, vol. 25, 100647. https://doi.org/10.1016/j.nanoso.2020.100647

APA

Larichev, Y. V. (2021). Small angle X-ray scattering study for supported catalysts: From solids to sols. Nano-Structures and Nano-Objects, 25, [100647]. https://doi.org/10.1016/j.nanoso.2020.100647

Vancouver

Larichev YV. Small angle X-ray scattering study for supported catalysts: From solids to sols. Nano-Structures and Nano-Objects. 2021 Feb;25:100647. doi: 10.1016/j.nanoso.2020.100647

Author

Larichev, Yu V. / Small angle X-ray scattering study for supported catalysts: From solids to sols. In: Nano-Structures and Nano-Objects. 2021 ; Vol. 25.

BibTeX

@article{ed3b7716cb2a499fbcef4698854aaa74,

title = "Small angle X-ray scattering study for supported catalysts: From solids to sols",

abstract = "New STS (from solids to sols) technique for studying supported metal catalysts by small angle X-ray scattering without parasitic scattering signal from porous support has been proposed. Due to selective dissolution of support, this parasitic scattering disappears. Efficiency of STS technique was demonstrated on three different supported catalysts. A good agreement between transmission electron microscopy data for initial supported catalysts and small angle X-ray scattering data for sols prepared from them was found. STS technique can be an expansion of small angle X-ray scattering application for analysis of wider range of solid functional materials with poly-phase composition. The main limitation of such technique is possibility of selective dissolution of different phases in complex material.",

keywords = "SAXS, Selective dissolution, Sols, Supported catalysts",

author = "Larichev, {Yu V.}",

year = "2021",

month = feb,

doi = "10.1016/j.nanoso.2020.100647",

language = "English",

volume = "25",

journal = "Nano-Structures and Nano-Objects",

issn = "2352-507X",

publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Small angle X-ray scattering study for supported catalysts: From solids to sols

AU - Larichev, Yu V.

PY - 2021/2

Y1 - 2021/2

N2 - New STS (from solids to sols) technique for studying supported metal catalysts by small angle X-ray scattering without parasitic scattering signal from porous support has been proposed. Due to selective dissolution of support, this parasitic scattering disappears. Efficiency of STS technique was demonstrated on three different supported catalysts. A good agreement between transmission electron microscopy data for initial supported catalysts and small angle X-ray scattering data for sols prepared from them was found. STS technique can be an expansion of small angle X-ray scattering application for analysis of wider range of solid functional materials with poly-phase composition. The main limitation of such technique is possibility of selective dissolution of different phases in complex material.

AB - New STS (from solids to sols) technique for studying supported metal catalysts by small angle X-ray scattering without parasitic scattering signal from porous support has been proposed. Due to selective dissolution of support, this parasitic scattering disappears. Efficiency of STS technique was demonstrated on three different supported catalysts. A good agreement between transmission electron microscopy data for initial supported catalysts and small angle X-ray scattering data for sols prepared from them was found. STS technique can be an expansion of small angle X-ray scattering application for analysis of wider range of solid functional materials with poly-phase composition. The main limitation of such technique is possibility of selective dissolution of different phases in complex material.

KW - SAXS

KW - Selective dissolution

KW - Sols

KW - Supported catalysts

UR - http://www.scopus.com/inward/record.url?scp=85097792646&partnerID=8YFLogxK

U2 - 10.1016/j.nanoso.2020.100647

DO - 10.1016/j.nanoso.2020.100647

M3 - Article

AN - SCOPUS:85097792646

VL - 25

JO - Nano-Structures and Nano-Objects

JF - Nano-Structures and Nano-Objects

SN - 2352-507X

M1 - 100647

ER -

ID: 27119559