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Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium. / Tiuliukova, I. A.; Rudina, N. A.; Lysikov, A. I. et al.

In: Materials Letters, Vol. 228, 01.10.2018, p. 61-64.

Research output: Contribution to journal › Article › peer-review

Harvard

Tiuliukova, IA, Rudina, NA, Lysikov, AI, Cherepanova, SV & Parkhomchuk, EV 2018, 'Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium', Materials Letters, vol. 228, pp. 61-64. https://doi.org/10.1016/j.matlet.2018.05.118

APA

Tiuliukova, I. A., Rudina, N. A., Lysikov, A. I., Cherepanova, S. V., & Parkhomchuk, E. V. (2018). Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium. Materials Letters, 228, 61-64. https://doi.org/10.1016/j.matlet.2018.05.118

Vancouver

Tiuliukova IA, Rudina NA, Lysikov AI, Cherepanova SV, Parkhomchuk EV. Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium. Materials Letters. 2018 Oct 1;228:61-64. doi: 10.1016/j.matlet.2018.05.118

Author

Tiuliukova, I. A. ; Rudina, N. A. ; Lysikov, A. I. et al. / Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium. In: Materials Letters. 2018 ; Vol. 228. pp. 61-64.

BibTeX

@article{e5fefa5fd6f34fd4b133c3be5f86bddb,
title = "Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium",
abstract = "Silicoaluminophosphate-11 (SAPO-11) crystals were synthesized in different media – water and ethanol – by the two-stage hydrothermal method using ultrasonic pretreatment of precursor mixture. Changing of the synthesis medium from water to ethanol leads to transformation of SAPO-11 morphology: from pseudo-spherical aggregative crystals to novel screw-like morphology. SAPO-11 crystals, synthesized in ethanol medium (Et-SAPO-11), have remarkable textural properties: the greater values of BET surface area and micropore/mesopores volume, compared with crystals, obtained in the water medium (W-SAPO-11). Besides, the acidity of Et-SAPO-11 is lower than that of W-SAPO-11 due to hindered incorporation of silicon into aluminophosphate lattice in ethanol medium.",
keywords = "Crystal morphology, Ethanol medium, Porous materials, SAPO-11, Silicoaluminophosphate, Texture, SILICON, HYDROISOMERIZATION, MOLECULAR-SIEVES, NONAQUEOUS MEDIA, PT/SAPO-11, ALKENES, CATALYTIC-PROPERTIES, IMPROVEMENT",
author = "Tiuliukova, {I. A.} and Rudina, {N. A.} and Lysikov, {A. I.} and Cherepanova, {S. V.} and Parkhomchuk, {E. V.}",
note = "Publisher Copyright: {\textcopyright} 2018 Elsevier B.V.",
year = "2018",
month = oct,
day = "1",
doi = "10.1016/j.matlet.2018.05.118",
language = "English",
volume = "228",
pages = "61--64",
journal = "Materials Letters",
issn = "0167-577X",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Screw-like morphology of silicoaluminophosphate-11 (SAPO-11) crystallized in ethanol medium

AU - Tiuliukova, I. A.

AU - Rudina, N. A.

AU - Lysikov, A. I.

AU - Cherepanova, S. V.

AU - Parkhomchuk, E. V.

N1 - Publisher Copyright: © 2018 Elsevier B.V.

PY - 2018/10/1

Y1 - 2018/10/1

N2 - Silicoaluminophosphate-11 (SAPO-11) crystals were synthesized in different media – water and ethanol – by the two-stage hydrothermal method using ultrasonic pretreatment of precursor mixture. Changing of the synthesis medium from water to ethanol leads to transformation of SAPO-11 morphology: from pseudo-spherical aggregative crystals to novel screw-like morphology. SAPO-11 crystals, synthesized in ethanol medium (Et-SAPO-11), have remarkable textural properties: the greater values of BET surface area and micropore/mesopores volume, compared with crystals, obtained in the water medium (W-SAPO-11). Besides, the acidity of Et-SAPO-11 is lower than that of W-SAPO-11 due to hindered incorporation of silicon into aluminophosphate lattice in ethanol medium.

AB - Silicoaluminophosphate-11 (SAPO-11) crystals were synthesized in different media – water and ethanol – by the two-stage hydrothermal method using ultrasonic pretreatment of precursor mixture. Changing of the synthesis medium from water to ethanol leads to transformation of SAPO-11 morphology: from pseudo-spherical aggregative crystals to novel screw-like morphology. SAPO-11 crystals, synthesized in ethanol medium (Et-SAPO-11), have remarkable textural properties: the greater values of BET surface area and micropore/mesopores volume, compared with crystals, obtained in the water medium (W-SAPO-11). Besides, the acidity of Et-SAPO-11 is lower than that of W-SAPO-11 due to hindered incorporation of silicon into aluminophosphate lattice in ethanol medium.

KW - Crystal morphology

KW - Ethanol medium

KW - Porous materials

KW - SAPO-11

KW - Silicoaluminophosphate

KW - Texture

KW - SILICON

KW - HYDROISOMERIZATION

KW - MOLECULAR-SIEVES

KW - NONAQUEOUS MEDIA

KW - PT/SAPO-11

KW - ALKENES

KW - CATALYTIC-PROPERTIES

KW - IMPROVEMENT

UR - http://www.scopus.com/inward/record.url?scp=85048465497&partnerID=8YFLogxK

U2 - 10.1016/j.matlet.2018.05.118

DO - 10.1016/j.matlet.2018.05.118

M3 - Article

AN - SCOPUS:85048465497

VL - 228

SP - 61

EP - 64

JO - Materials Letters

JF - Materials Letters

SN - 0167-577X

ER -

ID: 14048024