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Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-. / Sukhikh, Taisiya S.; Vostrikova, Kira E.

In: Journal of Solid State Chemistry, Vol. 258, 01.02.2018, p. 485-487.

Research output: Contribution to journal › Article › peer-review

Harvard

Sukhikh, TS & Vostrikova, KE 2018, 'Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-', Journal of Solid State Chemistry, vol. 258, pp. 485-487. https://doi.org/10.1016/j.jssc.2017.11.016

APA

Sukhikh, T. S., & Vostrikova, K. E. (2018). Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-. Journal of Solid State Chemistry, 258, 485-487. https://doi.org/10.1016/j.jssc.2017.11.016

Vancouver

Sukhikh TS, Vostrikova KE. Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-. Journal of Solid State Chemistry. 2018 Feb 1;258:485-487. doi: 10.1016/j.jssc.2017.11.016

Author

Sukhikh, Taisiya S. ; Vostrikova, Kira E. / Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-. In: Journal of Solid State Chemistry. 2018 ; Vol. 258. pp. 485-487.

BibTeX

@article{1cfae05388ef40bca76e928f242b1f71,
title = "Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-",
abstract = "A new XRD experiment and crystal structure refinement was performed for the earlier published compound in the paper “Heterobimetallic coordination polymers involving 3d metal complexes and heavier transition metals cyanometallates” by Peresypkina et al. (2015) [1]. A choice of a crystal cell taking in consideration the superstructural reflections allowed to obtain more reliable data about the symmetry and bond distances in the heterometallic 2D framework {[Ni(cyclam)]2[ReO(OH)0.5(MeOH)0.5(CN)4]}2.5+. Additionally, doubling of the parameter c permitted to get more details about interlayer space. As a result, disordered perchlorate anions and solvate molecules were located.",
keywords = "2D coordination polymer, Crystal structure, Cyclam, Heptacyanorhenate, Nickel(II), Rhenium",
author = "Sukhikh, {Taisiya S.} and Vostrikova, {Kira E.}",
year = "2018",
month = feb,
day = "1",
doi = "10.1016/j.jssc.2017.11.016",
language = "English",
volume = "258",
pages = "485--487",
journal = "Journal of Solid State Chemistry",
issn = "0022-4596",
publisher = "Academic Press Inc.",

}

RIS

TY - JOUR

T1 - Redetermination of the crystal structure of the 2D heterometallic framework prepared from [Ni(cyclam)]2+ and [Re(CN)7]3-

AU - Sukhikh, Taisiya S.

AU - Vostrikova, Kira E.

PY - 2018/2/1

Y1 - 2018/2/1

N2 - A new XRD experiment and crystal structure refinement was performed for the earlier published compound in the paper “Heterobimetallic coordination polymers involving 3d metal complexes and heavier transition metals cyanometallates” by Peresypkina et al. (2015) [1]. A choice of a crystal cell taking in consideration the superstructural reflections allowed to obtain more reliable data about the symmetry and bond distances in the heterometallic 2D framework {[Ni(cyclam)]2[ReO(OH)0.5(MeOH)0.5(CN)4]}2.5+. Additionally, doubling of the parameter c permitted to get more details about interlayer space. As a result, disordered perchlorate anions and solvate molecules were located.

AB - A new XRD experiment and crystal structure refinement was performed for the earlier published compound in the paper “Heterobimetallic coordination polymers involving 3d metal complexes and heavier transition metals cyanometallates” by Peresypkina et al. (2015) [1]. A choice of a crystal cell taking in consideration the superstructural reflections allowed to obtain more reliable data about the symmetry and bond distances in the heterometallic 2D framework {[Ni(cyclam)]2[ReO(OH)0.5(MeOH)0.5(CN)4]}2.5+. Additionally, doubling of the parameter c permitted to get more details about interlayer space. As a result, disordered perchlorate anions and solvate molecules were located.

KW - 2D coordination polymer

KW - Crystal structure

KW - Cyclam

KW - Heptacyanorhenate

KW - Nickel(II)

KW - Rhenium

UR - http://www.scopus.com/inward/record.url?scp=85034743681&partnerID=8YFLogxK

U2 - 10.1016/j.jssc.2017.11.016

DO - 10.1016/j.jssc.2017.11.016

M3 - Article

AN - SCOPUS:85034743681

VL - 258

SP - 485

EP - 487

JO - Journal of Solid State Chemistry

JF - Journal of Solid State Chemistry

SN - 0022-4596

ER -

ID: 9161037