Standard

Preparation and study of morphology of mesoporous anodic films grown on tin foil. / Vasilieva, T. A.; Uvarov, N. F.; Bokhonov, B. B.

In: Materials Today: Proceedings, Vol. 25, 01.10.2019, p. 401-404.

Research output: Contribution to journal › Conference article › peer-review

Harvard

Vasilieva, TA, Uvarov, NF & Bokhonov, BB 2019, 'Preparation and study of morphology of mesoporous anodic films grown on tin foil', Materials Today: Proceedings, vol. 25, pp. 401-404. https://doi.org/10.1016/j.matpr.2019.12.118

APA

Vasilieva, T. A., Uvarov, N. F., & Bokhonov, B. B. (2019). Preparation and study of morphology of mesoporous anodic films grown on tin foil. Materials Today: Proceedings, 25, 401-404. https://doi.org/10.1016/j.matpr.2019.12.118

Vancouver

Vasilieva TA, Uvarov NF, Bokhonov BB. Preparation and study of morphology of mesoporous anodic films grown on tin foil. Materials Today: Proceedings. 2019 Oct 1;25:401-404. doi: 10.1016/j.matpr.2019.12.118

Author

Vasilieva, T. A. ; Uvarov, N. F. ; Bokhonov, B. B. / Preparation and study of morphology of mesoporous anodic films grown on tin foil. In: Materials Today: Proceedings. 2019 ; Vol. 25. pp. 401-404.

BibTeX

@article{1f6536b0b29c40fa88ba1591e4a8b7bb,
title = "Preparation and study of morphology of mesoporous anodic films grown on tin foil",
abstract = "Mesoporous anodic layers were obtained on high-purity tin foils in electrolyte of two types: 0.3 M oxalic acid and 1 M NaOH in various anodizing modes. It was demonstrated that in both cases at low voltages below 4 V barrier films form. In acidic electrolyte the formation of tin (II) oxalate was observed whereas in basic electrolytes SnO2·nH2O seems to be formed. At intermediate voltage values from 4 to 8 V mesoporous films may be obtained with average size of pores of 20-40 nm, mesopores are rather uniformly distributed along the surface. It was found that in contrast to alumina anode films no linear dependency between pore diameter and voltage was observed at anodizing of tin foil. At voltages above 8 V and/or long-term anodization the film cracks and the film split to separate islands.",
keywords = "Anodic films, Anodizing of tin, Barrier layer tin(II) oxalate, Effect of voltage, Mesoporous layer on the tin surface, OXIDATION, ANODIZATION, OXIDE LAYERS, SNO2",
author = "Vasilieva, {T. A.} and Uvarov, {N. F.} and Bokhonov, {B. B.}",
year = "2019",
month = oct,
day = "1",
doi = "10.1016/j.matpr.2019.12.118",
language = "English",
volume = "25",
pages = "401--404",
journal = "Materials Today: Proceedings",
issn = "2214-7853",
publisher = "Elsevier Science B.V.",
note = "3rd All-Russian Conference, with International Participation Hot Topics of Solid State Chemistry : From New Ideas to New Materials, HTSSC 2019 ; Conference date: 01-10-2019 Through 05-10-2019",

}

RIS

TY - JOUR

T1 - Preparation and study of morphology of mesoporous anodic films grown on tin foil

AU - Vasilieva, T. A.

AU - Uvarov, N. F.

AU - Bokhonov, B. B.

PY - 2019/10/1

Y1 - 2019/10/1

N2 - Mesoporous anodic layers were obtained on high-purity tin foils in electrolyte of two types: 0.3 M oxalic acid and 1 M NaOH in various anodizing modes. It was demonstrated that in both cases at low voltages below 4 V barrier films form. In acidic electrolyte the formation of tin (II) oxalate was observed whereas in basic electrolytes SnO2·nH2O seems to be formed. At intermediate voltage values from 4 to 8 V mesoporous films may be obtained with average size of pores of 20-40 nm, mesopores are rather uniformly distributed along the surface. It was found that in contrast to alumina anode films no linear dependency between pore diameter and voltage was observed at anodizing of tin foil. At voltages above 8 V and/or long-term anodization the film cracks and the film split to separate islands.

AB - Mesoporous anodic layers were obtained on high-purity tin foils in electrolyte of two types: 0.3 M oxalic acid and 1 M NaOH in various anodizing modes. It was demonstrated that in both cases at low voltages below 4 V barrier films form. In acidic electrolyte the formation of tin (II) oxalate was observed whereas in basic electrolytes SnO2·nH2O seems to be formed. At intermediate voltage values from 4 to 8 V mesoporous films may be obtained with average size of pores of 20-40 nm, mesopores are rather uniformly distributed along the surface. It was found that in contrast to alumina anode films no linear dependency between pore diameter and voltage was observed at anodizing of tin foil. At voltages above 8 V and/or long-term anodization the film cracks and the film split to separate islands.

KW - Anodic films

KW - Anodizing of tin

KW - Barrier layer tin(II) oxalate

KW - Effect of voltage

KW - Mesoporous layer on the tin surface

KW - OXIDATION

KW - ANODIZATION

KW - OXIDE LAYERS

KW - SNO2

UR - http://www.scopus.com/inward/record.url?scp=85086941371&partnerID=8YFLogxK

U2 - 10.1016/j.matpr.2019.12.118

DO - 10.1016/j.matpr.2019.12.118

M3 - Conference article

AN - SCOPUS:85086941371

VL - 25

SP - 401

EP - 404

JO - Materials Today: Proceedings

JF - Materials Today: Proceedings

SN - 2214-7853

T2 - 3rd All-Russian Conference, with International Participation Hot Topics of Solid State Chemistry : From New Ideas to New Materials, HTSSC 2019

Y2 - 1 October 2019 through 5 October 2019

ER -

ID: 24613496