Standard

Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine. / Okotrub, A. V.; Kanygin, M. A.; Koroteev, V. O. et al.

In: Synthetic Metals, Vol. 248, 01.02.2019, p. 53-58.

Research output: Contribution to journal › Article › peer-review

Harvard

Okotrub, AV, Kanygin, MA, Koroteev, VO, Stolyarova, SG, Gorodetskiy, DV, Fedoseeva, YV, Asanov, IP, Bulusheva, LG & Vyalikh, A 2019, 'Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine', Synthetic Metals, vol. 248, pp. 53-58. https://doi.org/10.1016/j.synthmet.2019.01.005

APA

Okotrub, A. V., Kanygin, M. A., Koroteev, V. O., Stolyarova, S. G., Gorodetskiy, D. V., Fedoseeva, Y. V., Asanov, I. P., Bulusheva, L. G., & Vyalikh, A. (2019). Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine. Synthetic Metals, 248, 53-58. https://doi.org/10.1016/j.synthmet.2019.01.005

Vancouver

Okotrub AV, Kanygin MA, Koroteev VO, Stolyarova SG, Gorodetskiy DV, Fedoseeva YV et al. Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine. Synthetic Metals. 2019 Feb 1;248:53-58. doi: 10.1016/j.synthmet.2019.01.005

Author

Okotrub, A. V. ; Kanygin, M. A. ; Koroteev, V. O. et al. / Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine. In: Synthetic Metals. 2019 ; Vol. 248. pp. 53-58.

BibTeX

@article{66ce4c23ff9848e3936d5ace81dd26a6,
title = "Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine",
abstract = "It was shown, that the treatment of graphite oxide (GO) at a temperature of 1000 °C and a static pressure of 500 bar recovers the graphene layers. Addition of triphenylphosphine to GO helps in removal of oxygen during the treatment and allows introducing ca. 0.7 at% of phosphorus in the product. Most phosphorus atoms are bonded with oxygen as the 31P nuclear magnetic resonance spectrum showed. An analysis of the X-ray photoelectron P 2p spectrum additionally found the components corresponding to C–P and P–P bonding. Assembling of phosphorus atoms into nanometer clusters was confirmed by transmission electron microscopy. Raman spectroscopy and electrical conductivity measurements revealed the n-type doping of graphitic material through the incorporation of phosphorus.",
keywords = "Graphite oxide, Hot pressing, NMR, Phosphorus doping, Triphenylphosphine, XPS, OXIDATION, SOLID-STATE NMR, REDUCTION, DOPED GRAPHENE NANOSHEETS, FUNCTIONALIZED GRAPHENE",
author = "Okotrub, {A. V.} and Kanygin, {M. A.} and Koroteev, {V. O.} and Stolyarova, {S. G.} and Gorodetskiy, {D. V.} and Fedoseeva, {Yu V.} and Asanov, {I. P.} and Bulusheva, {L. G.} and A. Vyalikh",
year = "2019",
month = feb,
day = "1",
doi = "10.1016/j.synthmet.2019.01.005",
language = "English",
volume = "248",
pages = "53--58",
journal = "Synthetic Metals",
issn = "0379-6779",
publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Phosphorus incorporation into graphitic material via hot pressing of graphite oxide and triphenylphosphine

AU - Okotrub, A. V.

AU - Kanygin, M. A.

AU - Koroteev, V. O.

AU - Stolyarova, S. G.

AU - Gorodetskiy, D. V.

AU - Fedoseeva, Yu V.

AU - Asanov, I. P.

AU - Bulusheva, L. G.

AU - Vyalikh, A.

PY - 2019/2/1

Y1 - 2019/2/1

N2 - It was shown, that the treatment of graphite oxide (GO) at a temperature of 1000 °C and a static pressure of 500 bar recovers the graphene layers. Addition of triphenylphosphine to GO helps in removal of oxygen during the treatment and allows introducing ca. 0.7 at% of phosphorus in the product. Most phosphorus atoms are bonded with oxygen as the 31P nuclear magnetic resonance spectrum showed. An analysis of the X-ray photoelectron P 2p spectrum additionally found the components corresponding to C–P and P–P bonding. Assembling of phosphorus atoms into nanometer clusters was confirmed by transmission electron microscopy. Raman spectroscopy and electrical conductivity measurements revealed the n-type doping of graphitic material through the incorporation of phosphorus.

AB - It was shown, that the treatment of graphite oxide (GO) at a temperature of 1000 °C and a static pressure of 500 bar recovers the graphene layers. Addition of triphenylphosphine to GO helps in removal of oxygen during the treatment and allows introducing ca. 0.7 at% of phosphorus in the product. Most phosphorus atoms are bonded with oxygen as the 31P nuclear magnetic resonance spectrum showed. An analysis of the X-ray photoelectron P 2p spectrum additionally found the components corresponding to C–P and P–P bonding. Assembling of phosphorus atoms into nanometer clusters was confirmed by transmission electron microscopy. Raman spectroscopy and electrical conductivity measurements revealed the n-type doping of graphitic material through the incorporation of phosphorus.

KW - Graphite oxide

KW - Hot pressing

KW - NMR

KW - Phosphorus doping

KW - Triphenylphosphine

KW - XPS

KW - OXIDATION

KW - SOLID-STATE NMR

KW - REDUCTION

KW - DOPED GRAPHENE NANOSHEETS

KW - FUNCTIONALIZED GRAPHENE

UR - http://www.scopus.com/inward/record.url?scp=85059571774&partnerID=8YFLogxK

U2 - 10.1016/j.synthmet.2019.01.005

DO - 10.1016/j.synthmet.2019.01.005

M3 - Article

AN - SCOPUS:85059571774

VL - 248

SP - 53

EP - 58

JO - Synthetic Metals

JF - Synthetic Metals

SN - 0379-6779

ER -

ID: 18066370