Multi-analytical approach (SEM-EDS, FTIR, Py-GC/MS) to characterize the lacquer objects from Xiongnu burial complex (Noin-Ula, Mongolia)

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Multi-analytical approach (SEM-EDS, FTIR, Py-GC/MS) to characterize the lacquer objects from Xiongnu burial complex (Noin-Ula, Mongolia). / Karpova, Elena; Nefedov, Andrey; Mamatyuk, Victor et al.

In: Microchemical Journal, Vol. 130, 01.01.2017, p. 336-344.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{34230909634f4b2581f07a565aa1559c,

title = "Multi-analytical approach (SEM-EDS, FTIR, Py-GC/MS) to characterize the lacquer objects from Xiongnu burial complex (Noin-Ula, Mongolia)",

abstract = "A multi-analytical investigation was carried out to study lacquer objects from Noin-Ula burial complex (Mongolia, the first century AD). This complex is a unique source of information about Xiongnu - one of the most ancient nomadic empires, due to the variety of findings of different origin. This study was undertaken to characterize the materials used for manufacturing and decoration of lacquer everyday life objects and works of art from the 22nd and 31st Noin-Ula barrows. Scanning electron microscopy coupled with X-ray microanalysis (SEM-EDS), FT-IR spectroscopy and pyrolysis coupled with gas chromatography/mass spectrometry (Py-GS/MS) and derivatisation in situ with tetramethylammonium hydroxide were used to study both organic and inorganic components of ancient lacquer wares. The components of the drying oil and urushiol were identified in the lacquer coating compositions. Diterpenoid resin and polycyclic aromatic hydrocarbons (charcoal components) were found in some samples. Inorganic pigments of the lacquer wares were umber, iron oxides, cinnabar, orpiment and charcoal.",

keywords = "Colophony, Drying oil, Noin-Ula, Oriental lacquer, Urushiol, GAS CHROMATOGRAPHY/MASS SPECTROMETRY, ORIENTAL LACQUER, MASS-SPECTROMETRY",

author = "Elena Karpova and Andrey Nefedov and Victor Mamatyuk and Natalia Polosmak and Lyudmila Kundo",

year = "2017",

month = jan,

day = "1",

doi = "10.1016/j.microc.2016.10.013",

language = "English",

volume = "130",

pages = "336--344",

journal = "Microchemical Journal",

issn = "0026-265X",

publisher = "Elsevier Science Inc.",

}

RIS

TY - JOUR

T1 - Multi-analytical approach (SEM-EDS, FTIR, Py-GC/MS) to characterize the lacquer objects from Xiongnu burial complex (Noin-Ula, Mongolia)

AU - Karpova, Elena

AU - Nefedov, Andrey

AU - Mamatyuk, Victor

AU - Polosmak, Natalia

AU - Kundo, Lyudmila

PY - 2017/1/1

Y1 - 2017/1/1

N2 - A multi-analytical investigation was carried out to study lacquer objects from Noin-Ula burial complex (Mongolia, the first century AD). This complex is a unique source of information about Xiongnu - one of the most ancient nomadic empires, due to the variety of findings of different origin. This study was undertaken to characterize the materials used for manufacturing and decoration of lacquer everyday life objects and works of art from the 22nd and 31st Noin-Ula barrows. Scanning electron microscopy coupled with X-ray microanalysis (SEM-EDS), FT-IR spectroscopy and pyrolysis coupled with gas chromatography/mass spectrometry (Py-GS/MS) and derivatisation in situ with tetramethylammonium hydroxide were used to study both organic and inorganic components of ancient lacquer wares. The components of the drying oil and urushiol were identified in the lacquer coating compositions. Diterpenoid resin and polycyclic aromatic hydrocarbons (charcoal components) were found in some samples. Inorganic pigments of the lacquer wares were umber, iron oxides, cinnabar, orpiment and charcoal.

AB - A multi-analytical investigation was carried out to study lacquer objects from Noin-Ula burial complex (Mongolia, the first century AD). This complex is a unique source of information about Xiongnu - one of the most ancient nomadic empires, due to the variety of findings of different origin. This study was undertaken to characterize the materials used for manufacturing and decoration of lacquer everyday life objects and works of art from the 22nd and 31st Noin-Ula barrows. Scanning electron microscopy coupled with X-ray microanalysis (SEM-EDS), FT-IR spectroscopy and pyrolysis coupled with gas chromatography/mass spectrometry (Py-GS/MS) and derivatisation in situ with tetramethylammonium hydroxide were used to study both organic and inorganic components of ancient lacquer wares. The components of the drying oil and urushiol were identified in the lacquer coating compositions. Diterpenoid resin and polycyclic aromatic hydrocarbons (charcoal components) were found in some samples. Inorganic pigments of the lacquer wares were umber, iron oxides, cinnabar, orpiment and charcoal.

KW - Colophony

KW - Drying oil

KW - Noin-Ula

KW - Oriental lacquer

KW - Urushiol

KW - GAS CHROMATOGRAPHY/MASS SPECTROMETRY

KW - ORIENTAL LACQUER

KW - MASS-SPECTROMETRY

UR - http://www.scopus.com/inward/record.url?scp=84991669517&partnerID=8YFLogxK

U2 - 10.1016/j.microc.2016.10.013

DO - 10.1016/j.microc.2016.10.013

M3 - Article

AN - SCOPUS:84991669517

VL - 130

SP - 336

EP - 344

JO - Microchemical Journal

JF - Microchemical Journal

SN - 0026-265X

ER -

ID: 10320803