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Influence of Alumina Preparation Method on the Specific Features of Its Local Structure. / Moroz, E. M.; Shefer, K. I.

In: Theoretical and Experimental Chemistry, Vol. 56, No. 6, 01.2021, p. 417-423.

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Moroz EM, Shefer KI. Influence of Alumina Preparation Method on the Specific Features of Its Local Structure. Theoretical and Experimental Chemistry. 2021 Jan;56(6):417-423. doi: 10.1007/s11237-021-09671-9

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Moroz, E. M. ; Shefer, K. I. / Influence of Alumina Preparation Method on the Specific Features of Its Local Structure. In: Theoretical and Experimental Chemistry. 2021 ; Vol. 56, No. 6. pp. 417-423.

BibTeX

@article{cb8d5e2d83514740abcd28e8183d48a6,
title = "Influence of Alumina Preparation Method on the Specific Features of Its Local Structure",
abstract = "It is shown that analysis of X-ray scattering using the atomic pair distribution function makes it possible to reveal the differences in the fine structure of alumina samples, which have similar powder diffraction patterns. Such differences consist in different populations of tetrahedral and octahedral sites in the spinel structure of alumina or the existence of nuclei of a certain phase. The approach applied made it possible to explain the formation of different phases, baerite and pseudoboehmite, upon the rehydration of alumina obtained from gibbsite by thermal activation on a rotating metal plate or in a hot gas flow, respectively.",
keywords = "alumina, aluminum hydroxide, atomic pair distribution function, structure, X-ray diffraction, X-ray scattering",
author = "Moroz, {E. M.} and Shefer, {K. I.}",
note = "Funding Information: This work was supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental order for Boreskov Institute of Catalysis(project No. AAAA-A17-117041710079-8) and by the Russian Foundation for Basic Research (project No. 19-03-00595). Publisher Copyright: {\textcopyright} 2021, Springer Science+Business Media, LLC, part of Springer Nature. Copyright: Copyright 2021 Elsevier B.V., All rights reserved.",
year = "2021",
month = jan,
doi = "10.1007/s11237-021-09671-9",
language = "English",
volume = "56",
pages = "417--423",
journal = "Theoretical and Experimental Chemistry",
issn = "0040-5760",
publisher = "Springer New York",
number = "6",

}

RIS

TY - JOUR

T1 - Influence of Alumina Preparation Method on the Specific Features of Its Local Structure

AU - Moroz, E. M.

AU - Shefer, K. I.

N1 - Funding Information: This work was supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental order for Boreskov Institute of Catalysis(project No. AAAA-A17-117041710079-8) and by the Russian Foundation for Basic Research (project No. 19-03-00595). Publisher Copyright: © 2021, Springer Science+Business Media, LLC, part of Springer Nature. Copyright: Copyright 2021 Elsevier B.V., All rights reserved.

PY - 2021/1

Y1 - 2021/1

N2 - It is shown that analysis of X-ray scattering using the atomic pair distribution function makes it possible to reveal the differences in the fine structure of alumina samples, which have similar powder diffraction patterns. Such differences consist in different populations of tetrahedral and octahedral sites in the spinel structure of alumina or the existence of nuclei of a certain phase. The approach applied made it possible to explain the formation of different phases, baerite and pseudoboehmite, upon the rehydration of alumina obtained from gibbsite by thermal activation on a rotating metal plate or in a hot gas flow, respectively.

AB - It is shown that analysis of X-ray scattering using the atomic pair distribution function makes it possible to reveal the differences in the fine structure of alumina samples, which have similar powder diffraction patterns. Such differences consist in different populations of tetrahedral and octahedral sites in the spinel structure of alumina or the existence of nuclei of a certain phase. The approach applied made it possible to explain the formation of different phases, baerite and pseudoboehmite, upon the rehydration of alumina obtained from gibbsite by thermal activation on a rotating metal plate or in a hot gas flow, respectively.

KW - alumina

KW - aluminum hydroxide

KW - atomic pair distribution function

KW - structure

KW - X-ray diffraction

KW - X-ray scattering

UR - http://www.scopus.com/inward/record.url?scp=85101209457&partnerID=8YFLogxK

U2 - 10.1007/s11237-021-09671-9

DO - 10.1007/s11237-021-09671-9

M3 - Article

AN - SCOPUS:85101209457

VL - 56

SP - 417

EP - 423

JO - Theoretical and Experimental Chemistry

JF - Theoretical and Experimental Chemistry

SN - 0040-5760

IS - 6

ER -

ID: 27965871