Standard

Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing. / Fedoseeva, Yu V.; Okotrub, A. V.; Koroteev, V. O. et al.

In: Carbon, Vol. 141, 01.01.2019, p. 323-330.

Research output: Contribution to journal › Article › peer-review

Harvard

Fedoseeva, YV, Okotrub, AV, Koroteev, VO, Borzdov, YM, Palyanov, YN, Shubin, YV, Maksimovskiy, EA, Makarova, AA, Münchgesang, W, Bulusheva, LG & Vyalikh, A 2019, 'Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing', Carbon, vol. 141, pp. 323-330. https://doi.org/10.1016/j.carbon.2018.09.065

APA

Fedoseeva, Y. V., Okotrub, A. V., Koroteev, V. O., Borzdov, Y. M., Palyanov, Y. N., Shubin, Y. V., Maksimovskiy, E. A., Makarova, A. A., Münchgesang, W., Bulusheva, L. G., & Vyalikh, A. (2019). Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing. Carbon, 141, 323-330. https://doi.org/10.1016/j.carbon.2018.09.065

Vancouver

Fedoseeva YV, Okotrub AV, Koroteev VO, Borzdov YM, Palyanov YN, Shubin YV et al. Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing. Carbon. 2019 Jan 1;141:323-330. doi: 10.1016/j.carbon.2018.09.065

Author

Fedoseeva, Yu V. ; Okotrub, A. V. ; Koroteev, V. O. et al. / Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing. In: Carbon. 2019 ; Vol. 141. pp. 323-330.

BibTeX

@article{cd9e36af91eb4452b1283ffff0903f80,
title = "Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing",
abstract = "Hot pressing is one of the promising routes for graphitization of carbon materials. In the present work, high-pressure high-temperature behaviour of 13C-enriched fine-grained graphitic material has been studied by using a set of experimental tools such as scanning electron microscopy, Raman scattering, X-ray diffraction, X-ray photoelectron and near-edge X-ray absorption fine structure spectroscopies, and solid-state nuclear magnetic resonance (NMR) spectroscopy. The material has been annealed at a temperature of 1200 or 1500 °C using a stabilizing pressure of 5 GPa. It shown, that addition of small amount of water during the annealing at 1200 °C results in a better local atomic ordering of carbon material and increases the hydrocarbon fraction. Well-ordered graphite crystals enriched with 13C isotope are formed on the surface of nickel ampule at 1500 °C. An increase in processing time from 2 to 15 h decreases the defect density and improves the graphitization level of the material.",
keywords = "DIAMOND CRYSTAL-GROWTH, RAMAN-SPECTROSCOPY, CARBON, TEMPERATURE, CRYSTALLIZATION, DISORDER, METHANE, FILMS, WATER",
author = "Fedoseeva, {Yu V.} and Okotrub, {A. V.} and Koroteev, {V. O.} and Borzdov, {Yu M.} and Palyanov, {Yu N.} and Shubin, {Yu V.} and Maksimovskiy, {E. A.} and Makarova, {A. A.} and W. M{\"u}nchgesang and Bulusheva, {L. G.} and A. Vyalikh",
note = "Publisher Copyright: {\textcopyright} 2018 Elsevier Ltd",
year = "2019",
month = jan,
day = "1",
doi = "10.1016/j.carbon.2018.09.065",
language = "English",
volume = "141",
pages = "323--330",
journal = "Carbon",
issn = "0008-6223",
publisher = "Elsevier Ltd",

}

RIS

TY - JOUR

T1 - Graphitization of 13C enriched fine-grained graphitic material under high-pressure annealing

AU - Fedoseeva, Yu V.

AU - Okotrub, A. V.

AU - Koroteev, V. O.

AU - Borzdov, Yu M.

AU - Palyanov, Yu N.

AU - Shubin, Yu V.

AU - Maksimovskiy, E. A.

AU - Makarova, A. A.

AU - Münchgesang, W.

AU - Bulusheva, L. G.

AU - Vyalikh, A.

N1 - Publisher Copyright: © 2018 Elsevier Ltd

PY - 2019/1/1

Y1 - 2019/1/1

N2 - Hot pressing is one of the promising routes for graphitization of carbon materials. In the present work, high-pressure high-temperature behaviour of 13C-enriched fine-grained graphitic material has been studied by using a set of experimental tools such as scanning electron microscopy, Raman scattering, X-ray diffraction, X-ray photoelectron and near-edge X-ray absorption fine structure spectroscopies, and solid-state nuclear magnetic resonance (NMR) spectroscopy. The material has been annealed at a temperature of 1200 or 1500 °C using a stabilizing pressure of 5 GPa. It shown, that addition of small amount of water during the annealing at 1200 °C results in a better local atomic ordering of carbon material and increases the hydrocarbon fraction. Well-ordered graphite crystals enriched with 13C isotope are formed on the surface of nickel ampule at 1500 °C. An increase in processing time from 2 to 15 h decreases the defect density and improves the graphitization level of the material.

AB - Hot pressing is one of the promising routes for graphitization of carbon materials. In the present work, high-pressure high-temperature behaviour of 13C-enriched fine-grained graphitic material has been studied by using a set of experimental tools such as scanning electron microscopy, Raman scattering, X-ray diffraction, X-ray photoelectron and near-edge X-ray absorption fine structure spectroscopies, and solid-state nuclear magnetic resonance (NMR) spectroscopy. The material has been annealed at a temperature of 1200 or 1500 °C using a stabilizing pressure of 5 GPa. It shown, that addition of small amount of water during the annealing at 1200 °C results in a better local atomic ordering of carbon material and increases the hydrocarbon fraction. Well-ordered graphite crystals enriched with 13C isotope are formed on the surface of nickel ampule at 1500 °C. An increase in processing time from 2 to 15 h decreases the defect density and improves the graphitization level of the material.

KW - DIAMOND CRYSTAL-GROWTH

KW - RAMAN-SPECTROSCOPY

KW - CARBON

KW - TEMPERATURE

KW - CRYSTALLIZATION

KW - DISORDER

KW - METHANE

KW - FILMS

KW - WATER

UR - http://www.scopus.com/inward/record.url?scp=85054324044&partnerID=8YFLogxK

U2 - 10.1016/j.carbon.2018.09.065

DO - 10.1016/j.carbon.2018.09.065

M3 - Article

AN - SCOPUS:85054324044

VL - 141

SP - 323

EP - 330

JO - Carbon

JF - Carbon

SN - 0008-6223

ER -

ID: 17035348