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Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine. / Fedoseeva, Yuliya V.; Dubois, Marc; Flahaut, Emmanuel et al.

In: Physica Status Solidi (B) Basic Research, Vol. 255, No. 1, 1700261, 01.01.2018.

Research output: Contribution to journal › Article › peer-review

Harvard

Fedoseeva, YV, Dubois, M, Flahaut, E, Vilkov, OY, Chuvilin, A, Asanov, IP, Okotrub, AV & Bulusheva, LG 2018, 'Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine', Physica Status Solidi (B) Basic Research, vol. 255, no. 1, 1700261. https://doi.org/10.1002/pssb.201700261

APA

Fedoseeva, Y. V., Dubois, M., Flahaut, E., Vilkov, O. Y., Chuvilin, A., Asanov, I. P., Okotrub, A. V., & Bulusheva, L. G. (2018). Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine. Physica Status Solidi (B) Basic Research, 255(1), [1700261]. https://doi.org/10.1002/pssb.201700261

Vancouver

Fedoseeva YV, Dubois M, Flahaut E, Vilkov OY, Chuvilin A, Asanov IP et al. Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine. Physica Status Solidi (B) Basic Research. 2018 Jan 1;255(1):1700261. doi: 10.1002/pssb.201700261

Author

Fedoseeva, Yuliya V. ; Dubois, Marc ; Flahaut, Emmanuel et al. / Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine. In: Physica Status Solidi (B) Basic Research. 2018 ; Vol. 255, No. 1.

BibTeX

@article{191cb621f71a49668b045a041d5f950a,
title = "Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine",
abstract = "Double-walled carbon nanotubes (DWCNTs) have been fluorinated by pure molecular fluorine (F2) at room temperature or 200 °C and a mixture of F2 with hydrogen fluoride (HF) at 200 °C that resulted in products with compositions of CF0.12, CF0.39, and CF0.53 as determined by X-ray photoelectron spectroscopy. The differences in the structures of three kinds of fluorinated DWCNTs were revealed using transmission electron microscopy, Raman scattering, and near-edge X-ray absorption fine structure (NEXAFS) spectroscopy. Quantum-chemical modeling of the NEXAFS F K-edge spectra detected a change in the fluorine pattern with the increase of the F2 treatment temperature. The presence of HF in fluorine gas was found to accelerate the fluorination process and cause a partial destruction of outer shells of the DWCNTs.",
keywords = "double-walled carbon nanotubes, fluorination, HF, NEXAFS, X-ray photoelectron spectroscopy, DENSITY, ENERGY, RAMAN-SPECTROSCOPY, GRAPHITE",
author = "Fedoseeva, {Yuliya V.} and Marc Dubois and Emmanuel Flahaut and Vilkov, {Oleg Yu} and Andrey Chuvilin and Asanov, {Igor P.} and Okotrub, {Alexander V.} and Bulusheva, {Lyubov G.}",
year = "2018",
month = jan,
day = "1",
doi = "10.1002/pssb.201700261",
language = "English",
volume = "255",
journal = "Physica Status Solidi (B): Basic Research",
issn = "0370-1972",
publisher = "Wiley-VCH Verlag",
number = "1",

}

RIS

TY - JOUR

T1 - Effect of Hydrogen Fluoride Addition and Synthesis Temperature on the Structure of Double-Walled Carbon Nanotubes Fluorinated by Molecular Fluorine

AU - Fedoseeva, Yuliya V.

AU - Dubois, Marc

AU - Flahaut, Emmanuel

AU - Vilkov, Oleg Yu

AU - Chuvilin, Andrey

AU - Asanov, Igor P.

AU - Okotrub, Alexander V.

AU - Bulusheva, Lyubov G.

PY - 2018/1/1

Y1 - 2018/1/1

N2 - Double-walled carbon nanotubes (DWCNTs) have been fluorinated by pure molecular fluorine (F2) at room temperature or 200 °C and a mixture of F2 with hydrogen fluoride (HF) at 200 °C that resulted in products with compositions of CF0.12, CF0.39, and CF0.53 as determined by X-ray photoelectron spectroscopy. The differences in the structures of three kinds of fluorinated DWCNTs were revealed using transmission electron microscopy, Raman scattering, and near-edge X-ray absorption fine structure (NEXAFS) spectroscopy. Quantum-chemical modeling of the NEXAFS F K-edge spectra detected a change in the fluorine pattern with the increase of the F2 treatment temperature. The presence of HF in fluorine gas was found to accelerate the fluorination process and cause a partial destruction of outer shells of the DWCNTs.

AB - Double-walled carbon nanotubes (DWCNTs) have been fluorinated by pure molecular fluorine (F2) at room temperature or 200 °C and a mixture of F2 with hydrogen fluoride (HF) at 200 °C that resulted in products with compositions of CF0.12, CF0.39, and CF0.53 as determined by X-ray photoelectron spectroscopy. The differences in the structures of three kinds of fluorinated DWCNTs were revealed using transmission electron microscopy, Raman scattering, and near-edge X-ray absorption fine structure (NEXAFS) spectroscopy. Quantum-chemical modeling of the NEXAFS F K-edge spectra detected a change in the fluorine pattern with the increase of the F2 treatment temperature. The presence of HF in fluorine gas was found to accelerate the fluorination process and cause a partial destruction of outer shells of the DWCNTs.

KW - double-walled carbon nanotubes

KW - fluorination

KW - HF

KW - NEXAFS

KW - X-ray photoelectron spectroscopy

KW - DENSITY

KW - ENERGY

KW - RAMAN-SPECTROSCOPY

KW - GRAPHITE

UR - http://www.scopus.com/inward/record.url?scp=85040788788&partnerID=8YFLogxK

U2 - 10.1002/pssb.201700261

DO - 10.1002/pssb.201700261

M3 - Article

AN - SCOPUS:85040788788

VL - 255

JO - Physica Status Solidi (B): Basic Research

JF - Physica Status Solidi (B): Basic Research

SN - 0370-1972

IS - 1

M1 - 1700261

ER -

ID: 12102014