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Concomitant cocrystal and salt : no interconversion in the solid state. / Losev, Evgeniy A.; Boldyreva, Elena.

In: Acta Crystallographica Section C: Structural Chemistry, Vol. 75, 03.2019, p. 313-319.

Research output: Contribution to journal › Article › peer-review

Harvard

Losev, EA & Boldyreva, E 2019, 'Concomitant cocrystal and salt: no interconversion in the solid state', Acta Crystallographica Section C: Structural Chemistry, vol. 75, pp. 313-319. https://doi.org/10.1107/S2053229619001372

APA

Losev, E. A., & Boldyreva, E. (2019). Concomitant cocrystal and salt: no interconversion in the solid state. Acta Crystallographica Section C: Structural Chemistry, 75, 313-319. https://doi.org/10.1107/S2053229619001372

Vancouver

Losev EA, Boldyreva E. Concomitant cocrystal and salt: no interconversion in the solid state. Acta Crystallographica Section C: Structural Chemistry. 2019 Mar;75:313-319. doi: 10.1107/S2053229619001372

Author

Losev, Evgeniy A. ; Boldyreva, Elena. / Concomitant cocrystal and salt : no interconversion in the solid state. In: Acta Crystallographica Section C: Structural Chemistry. 2019 ; Vol. 75. pp. 313-319.

BibTeX

@article{bfb405cf6dda45069b895f3df9adbe68,
title = "Concomitant cocrystal and salt: no interconversion in the solid state",
abstract = " A cocrystal and a molecular salt of β-alanine and dl-tartaric acid, C 3 H 8 NO 2 + ·C 4 H 4 O 6 − , of the same chemical composition, were studied over a wide temperature range by single-crystal and powder X-ray diffraction. Neither the interconversion between the two phases nor any polymorphic transitions were observed in the temperature range from 100 K to the melting points. This contrasts with the solvent-mediated phase transition from the salt to the cocrystal in a slurry that has been documented earlier. ",
keywords = "cocrystal, crystal structure, dl-tartaric acid, molecular salt, solvent-mediated phase transformation, X-ray diffraction, β-alanine, β-Alanine, DL-tartaric acid, Cocrystal, Molecular salt, Crystal structure, Solvent-mediated phase transformation, CRYSTALLIZATION, GLYCINE, RAMAN-SPECTROSCOPY, X-RAY-DIFFRACTION, POLYMORPHISM, LOW-TEMPERATURES, ACID CO-CRYSTALS, PHASE, beta-alanine, KINETICS",
author = "Losev, {Evgeniy A.} and Elena Boldyreva",
note = "Publisher Copyright: {\textcopyright} 2019 International Union of Crystallography.",
year = "2019",
month = mar,
doi = "10.1107/S2053229619001372",
language = "English",
volume = "75",
pages = "313--319",
journal = "Acta Crystallographica Section C: Structural Chemistry",
issn = "2053-2296",
publisher = "John Wiley and Sons Inc.",

}

RIS

TY - JOUR

T1 - Concomitant cocrystal and salt

T2 - no interconversion in the solid state

AU - Losev, Evgeniy A.

AU - Boldyreva, Elena

N1 - Publisher Copyright: © 2019 International Union of Crystallography.

PY - 2019/3

Y1 - 2019/3

N2 - A cocrystal and a molecular salt of β-alanine and dl-tartaric acid, C 3 H 8 NO 2 + ·C 4 H 4 O 6 − , of the same chemical composition, were studied over a wide temperature range by single-crystal and powder X-ray diffraction. Neither the interconversion between the two phases nor any polymorphic transitions were observed in the temperature range from 100 K to the melting points. This contrasts with the solvent-mediated phase transition from the salt to the cocrystal in a slurry that has been documented earlier.

AB - A cocrystal and a molecular salt of β-alanine and dl-tartaric acid, C 3 H 8 NO 2 + ·C 4 H 4 O 6 − , of the same chemical composition, were studied over a wide temperature range by single-crystal and powder X-ray diffraction. Neither the interconversion between the two phases nor any polymorphic transitions were observed in the temperature range from 100 K to the melting points. This contrasts with the solvent-mediated phase transition from the salt to the cocrystal in a slurry that has been documented earlier.

KW - cocrystal

KW - crystal structure

KW - dl-tartaric acid

KW - molecular salt

KW - solvent-mediated phase transformation

KW - X-ray diffraction

KW - β-alanine

KW - β-Alanine

KW - DL-tartaric acid

KW - Cocrystal

KW - Molecular salt

KW - Crystal structure

KW - Solvent-mediated phase transformation

KW - CRYSTALLIZATION

KW - GLYCINE

KW - RAMAN-SPECTROSCOPY

KW - X-RAY-DIFFRACTION

KW - POLYMORPHISM

KW - LOW-TEMPERATURES

KW - ACID CO-CRYSTALS

KW - PHASE

KW - beta-alanine

KW - KINETICS

UR - http://www.scopus.com/inward/record.url?scp=85061487052&partnerID=8YFLogxK

U2 - 10.1107/S2053229619001372

DO - 10.1107/S2053229619001372

M3 - Article

C2 - 30833526

AN - SCOPUS:85061487052

VL - 75

SP - 313

EP - 319

JO - Acta Crystallographica Section C: Structural Chemistry

JF - Acta Crystallographica Section C: Structural Chemistry

SN - 2053-2296

ER -

ID: 18562028