Analysis of High-Purity Germanium Dioxide by Inductively Coupled Plasma Atomic Emission Spectrometry with Reaction Distillation of the Matrix

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Analysis of High-Purity Germanium Dioxide by Inductively Coupled Plasma Atomic Emission Spectrometry with Reaction Distillation of the Matrix. / Gusel’nikova, T. Ya; Tsygankova, A. R.; Saprykin, A. I.

In: Journal of Analytical Chemistry, Vol. 75, No. 5, 01.05.2020, p. 582-586.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{acac1b644bb248f7acf1b32bb53236f1,

title = "Analysis of High-Purity Germanium Dioxide by Inductively Coupled Plasma Atomic Emission Spectrometry with Reaction Distillation of the Matrix",

abstract = "A combined method of analysis of high-purity germanium dioxide by atomic emission spectrometry with matrix preseparation and trace element preconcentration was developed. The matrix was separated in an autoclave of a MARS 5 microwave system without the contact of samples with an acid solution. The method allows the determination of the following 50 analytes with the limits of detection 10–8–10–5 wt %: Ag, Al, As, Au, B, Ba, Be, Cd, Ce, Co, Cr, Cu, Dy, Er, Eu, Fe, Ga, Gd, Hf, Hg, Ho, In, La, Li, Lu, Mg, Mn, Na, Nb, Nd, Ni, P, Pb, Pr, Re, Sb, Sc, Sm, Sn, Sr, Ta, Tb, Te, Ti, Tm, W, Y, Yb, Zn, and Zr.",

keywords = "atomic emission spectrometry, high-purity germanium dioxide, inductively coupled plasma, limits of detection, matrix separation, multielement analysis",

author = "Gusel{\textquoteright}nikova, {T. Ya} and Tsygankova, {A. R.} and Saprykin, {A. I.}",

year = "2020",

month = may,

day = "1",

doi = "10.1134/S1061934820050056",

language = "English",

volume = "75",

pages = "582--586",

journal = "Journal of Analytical Chemistry",

issn = "1061-9348",

publisher = "PLEIADES PUBLISHING INC",

number = "5",

}

RIS

TY - JOUR

T1 - Analysis of High-Purity Germanium Dioxide by Inductively Coupled Plasma Atomic Emission Spectrometry with Reaction Distillation of the Matrix

AU - Gusel’nikova, T. Ya

AU - Tsygankova, A. R.

AU - Saprykin, A. I.

PY - 2020/5/1

Y1 - 2020/5/1

N2 - A combined method of analysis of high-purity germanium dioxide by atomic emission spectrometry with matrix preseparation and trace element preconcentration was developed. The matrix was separated in an autoclave of a MARS 5 microwave system without the contact of samples with an acid solution. The method allows the determination of the following 50 analytes with the limits of detection 10–8–10–5 wt %: Ag, Al, As, Au, B, Ba, Be, Cd, Ce, Co, Cr, Cu, Dy, Er, Eu, Fe, Ga, Gd, Hf, Hg, Ho, In, La, Li, Lu, Mg, Mn, Na, Nb, Nd, Ni, P, Pb, Pr, Re, Sb, Sc, Sm, Sn, Sr, Ta, Tb, Te, Ti, Tm, W, Y, Yb, Zn, and Zr.

AB - A combined method of analysis of high-purity germanium dioxide by atomic emission spectrometry with matrix preseparation and trace element preconcentration was developed. The matrix was separated in an autoclave of a MARS 5 microwave system without the contact of samples with an acid solution. The method allows the determination of the following 50 analytes with the limits of detection 10–8–10–5 wt %: Ag, Al, As, Au, B, Ba, Be, Cd, Ce, Co, Cr, Cu, Dy, Er, Eu, Fe, Ga, Gd, Hf, Hg, Ho, In, La, Li, Lu, Mg, Mn, Na, Nb, Nd, Ni, P, Pb, Pr, Re, Sb, Sc, Sm, Sn, Sr, Ta, Tb, Te, Ti, Tm, W, Y, Yb, Zn, and Zr.

KW - atomic emission spectrometry

KW - high-purity germanium dioxide

KW - inductively coupled plasma

KW - limits of detection

KW - matrix separation

KW - multielement analysis

UR - http://www.scopus.com/inward/record.url?scp=85084916295&partnerID=8YFLogxK

U2 - 10.1134/S1061934820050056

DO - 10.1134/S1061934820050056

M3 - Article

AN - SCOPUS:85084916295

VL - 75

SP - 582

EP - 586

JO - Journal of Analytical Chemistry

JF - Journal of Analytical Chemistry

SN - 1061-9348

IS - 5

ER -

ID: 24330201