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A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC. / Patrushev, Yu V.; Sotnikova, Yu S.; Sidel’nikov, V. N.

In: Protection of Metals and Physical Chemistry of Surfaces, Vol. 56, No. 1, 01.2020, p. 49-53.

Research output: Contribution to journal › Article › peer-review

Harvard

Patrushev, YV, Sotnikova, YS & Sidel’nikov, VN 2020, 'A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC', Protection of Metals and Physical Chemistry of Surfaces, vol. 56, no. 1, pp. 49-53. https://doi.org/10.1134/S2070205119060248

APA

Patrushev, Y. V., Sotnikova, Y. S., & Sidel’nikov, V. N. (2020). A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC. Protection of Metals and Physical Chemistry of Surfaces, 56(1), 49-53. https://doi.org/10.1134/S2070205119060248

Vancouver

Patrushev YV, Sotnikova YS, Sidel’nikov VN. A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC. Protection of Metals and Physical Chemistry of Surfaces. 2020 Jan;56(1):49-53. doi: 10.1134/S2070205119060248

Author

Patrushev, Yu V. ; Sotnikova, Yu S. ; Sidel’nikov, V. N. / A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC. In: Protection of Metals and Physical Chemistry of Surfaces. 2020 ; Vol. 56, No. 1. pp. 49-53.

BibTeX

@article{c87bbabd7a8643b5ad9f1db58aa0ad3f,
title = "A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC",
abstract = "Abstract: A monolithic chromatographic column for HPLC with a sorbent based on 1-vinyl-1,2,4-triazole has been prepared for the first time. It has been shown that, depending on the composition of the mobile phase (acetonitrile/water ratio), this column is able to operate in the modes of both reverse phase chromatography and hydrophilic chromatography. The dependences of the retention factor on the volume fraction of acetonitrile in the mobile phase have been studied for substances of acidic and basic nature. An example of the separation of the components of the pharmaceutical product Askofen-P on the prepared column has been provided.",
keywords = "1-vinyl-1,2,4-triazole, HPLC, hydrophilic interaction chromatography, monolithic columns, porous polymers, ROD COLUMNS, 4-triazole, ACID, CAPILLARY COLUMNS, 2, 1-vinyl-1, POLYMER, SEPARATION, SELECTIVITY, INTERACTION CHROMATOGRAPHY",
author = "Patrushev, {Yu V.} and Sotnikova, {Yu S.} and Sidel{\textquoteright}nikov, {V. N.}",
year = "2020",
month = jan,
doi = "10.1134/S2070205119060248",
language = "English",
volume = "56",
pages = "49--53",
journal = "Protection of Metals and Physical Chemistry of Surfaces",
issn = "2070-2051",
publisher = "PLEIADES PUBLISHING INC",
number = "1",

}

RIS

TY - JOUR

T1 - A Monolithic Column with a Sorbent Based on 1-Vinyl-1,2,4-Triazole for Hydrophilic HPLC

AU - Patrushev, Yu V.

AU - Sotnikova, Yu S.

AU - Sidel’nikov, V. N.

PY - 2020/1

Y1 - 2020/1

N2 - Abstract: A monolithic chromatographic column for HPLC with a sorbent based on 1-vinyl-1,2,4-triazole has been prepared for the first time. It has been shown that, depending on the composition of the mobile phase (acetonitrile/water ratio), this column is able to operate in the modes of both reverse phase chromatography and hydrophilic chromatography. The dependences of the retention factor on the volume fraction of acetonitrile in the mobile phase have been studied for substances of acidic and basic nature. An example of the separation of the components of the pharmaceutical product Askofen-P on the prepared column has been provided.

AB - Abstract: A monolithic chromatographic column for HPLC with a sorbent based on 1-vinyl-1,2,4-triazole has been prepared for the first time. It has been shown that, depending on the composition of the mobile phase (acetonitrile/water ratio), this column is able to operate in the modes of both reverse phase chromatography and hydrophilic chromatography. The dependences of the retention factor on the volume fraction of acetonitrile in the mobile phase have been studied for substances of acidic and basic nature. An example of the separation of the components of the pharmaceutical product Askofen-P on the prepared column has been provided.

KW - 1-vinyl-1,2,4-triazole

KW - HPLC

KW - hydrophilic interaction chromatography

KW - monolithic columns

KW - porous polymers

KW - ROD COLUMNS

KW - 4-triazole

KW - ACID

KW - CAPILLARY COLUMNS

KW - 2

KW - 1-vinyl-1

KW - POLYMER

KW - SEPARATION

KW - SELECTIVITY

KW - INTERACTION CHROMATOGRAPHY

UR - http://www.scopus.com/inward/record.url?scp=85083177067&partnerID=8YFLogxK

U2 - 10.1134/S2070205119060248

DO - 10.1134/S2070205119060248

M3 - Article

AN - SCOPUS:85083177067

VL - 56

SP - 49

EP - 53

JO - Protection of Metals and Physical Chemistry of Surfaces

JF - Protection of Metals and Physical Chemistry of Surfaces

SN - 2070-2051

IS - 1

ER -

ID: 24093841