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Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support. / Chikunova, Yu O.; Vorobieva, E. E.; Moseenkov, S. I. и др.

в: Journal of Structural Chemistry, Том 66, № 2, 10.03.2025, стр. 369-385.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Chikunova, YO, Vorobieva, EE, Moseenkov, SI, Parkhomchuk, EV, Gribov, EN, Shaparenko, NO & Kozlov, DV 2025, 'Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support', Journal of Structural Chemistry, Том. 66, № 2, стр. 369-385. https://doi.org/10.1134/S0022476625020143

APA

Chikunova, Y. O., Vorobieva, E. E., Moseenkov, S. I., Parkhomchuk, E. V., Gribov, E. N., Shaparenko, N. O., & Kozlov, D. V. (2025). Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support. Journal of Structural Chemistry, 66(2), 369-385. https://doi.org/10.1134/S0022476625020143

Vancouver

Chikunova YO, Vorobieva EE, Moseenkov SI, Parkhomchuk EV, Gribov EN, Shaparenko NO и др. Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support. Journal of Structural Chemistry. 2025 март 10;66(2):369-385. doi: 10.1134/S0022476625020143

Author

Chikunova, Yu O. ; Vorobieva, E. E. ; Moseenkov, S. I. и др. / Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support. в: Journal of Structural Chemistry. 2025 ; Том 66, № 2. стр. 369-385.

BibTeX

@article{ead9f229e6ee42638120e87923c93c01,
title = "Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support",
abstract = "Abstract: Owing to its semiconductor properties, tin(IV) oxide is widely used in gas sensors, photo- and electrocatalysis, fuel cells, electrolyzers etc. In this work, macroporous SnO2 samples are synthesized by impregnating polystyrene (PS) microspheres with sols containing SnCl4 and alcohol (96% ethanol, isopropanol, or n-butanol). After impregnation, the composites undergo drying and annealing. After drying, the same samples are washed with water for more complete hydrolysis followed by annealing. The resulting SnO2 samples are studied by powder X-ray diffraction, X-ray photoelectron spectroscopy, X-ray fluorescence analysis, low-temperature N2 adsorption (77 K), mercury porosimetry, and scanning electron microscopy. The effect of washing with alcohol and water on the porous characteristics and electrical conductivity of the materials is studied.",
keywords = "SnO2, electrical conductivity, polystyrene microspheres, template synthesis",
author = "Chikunova, {Yu O.} and Vorobieva, {E. E.} and Moseenkov, {S. I.} and Parkhomchuk, {E. V.} and Gribov, {E. N.} and Shaparenko, {N. O.} and Kozlov, {D. V.}",
note = "The work was supported by the Ministry of Science and Higher Education of the Russian Federation within the State Task for the Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences (project FWUR-2024-0036). Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support / Yu. O. Chikunova, E. E. Vorobieva, S. I. Moseenkov [et al.] // Journal of Structural Chemistry. – 2025. – Vol. 66, No. 2. – P. 369-385. – DOI 10.1134/S0022476625020143.",
year = "2025",
month = mar,
day = "10",
doi = "10.1134/S0022476625020143",
language = "English",
volume = "66",
pages = "369--385",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer",
number = "2",

}

RIS

TY - JOUR

T1 - Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support

AU - Chikunova, Yu O.

AU - Vorobieva, E. E.

AU - Moseenkov, S. I.

AU - Parkhomchuk, E. V.

AU - Gribov, E. N.

AU - Shaparenko, N. O.

AU - Kozlov, D. V.

N1 - The work was supported by the Ministry of Science and Higher Education of the Russian Federation within the State Task for the Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences (project FWUR-2024-0036). Template Synthesis of Macroporous Tin(IV) Oxide for its Use as an Electrocatalyst Support / Yu. O. Chikunova, E. E. Vorobieva, S. I. Moseenkov [et al.] // Journal of Structural Chemistry. – 2025. – Vol. 66, No. 2. – P. 369-385. – DOI 10.1134/S0022476625020143.

PY - 2025/3/10

Y1 - 2025/3/10

N2 - Abstract: Owing to its semiconductor properties, tin(IV) oxide is widely used in gas sensors, photo- and electrocatalysis, fuel cells, electrolyzers etc. In this work, macroporous SnO2 samples are synthesized by impregnating polystyrene (PS) microspheres with sols containing SnCl4 and alcohol (96% ethanol, isopropanol, or n-butanol). After impregnation, the composites undergo drying and annealing. After drying, the same samples are washed with water for more complete hydrolysis followed by annealing. The resulting SnO2 samples are studied by powder X-ray diffraction, X-ray photoelectron spectroscopy, X-ray fluorescence analysis, low-temperature N2 adsorption (77 K), mercury porosimetry, and scanning electron microscopy. The effect of washing with alcohol and water on the porous characteristics and electrical conductivity of the materials is studied.

AB - Abstract: Owing to its semiconductor properties, tin(IV) oxide is widely used in gas sensors, photo- and electrocatalysis, fuel cells, electrolyzers etc. In this work, macroporous SnO2 samples are synthesized by impregnating polystyrene (PS) microspheres with sols containing SnCl4 and alcohol (96% ethanol, isopropanol, or n-butanol). After impregnation, the composites undergo drying and annealing. After drying, the same samples are washed with water for more complete hydrolysis followed by annealing. The resulting SnO2 samples are studied by powder X-ray diffraction, X-ray photoelectron spectroscopy, X-ray fluorescence analysis, low-temperature N2 adsorption (77 K), mercury porosimetry, and scanning electron microscopy. The effect of washing with alcohol and water on the porous characteristics and electrical conductivity of the materials is studied.

KW - SnO2

KW - electrical conductivity

KW - polystyrene microspheres

KW - template synthesis

UR - https://www.mendeley.com/catalogue/775fe07d-66d1-3b18-98ce-7a9b0a7c42da/

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-86000773269&origin=inward&txGid=6e90fe1f4bee8aba82dd4dd855790ecc

UR - https://www.elibrary.ru/item.asp?id=80438838

U2 - 10.1134/S0022476625020143

DO - 10.1134/S0022476625020143

M3 - Article

VL - 66

SP - 369

EP - 385

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 2

ER -

ID: 65066821