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Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series. / Baidina, I. A.; Belyaev, A. V.; Korolkov, I. V. и др.

в: Journal of Structural Chemistry, Том 60, № 9, 01.09.2019, стр. 1482-1488.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Baidina, IA, Belyaev, AV, Korolkov, IV, Smolentsev, AI & Vorobieva, SN 2019, 'Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series', Journal of Structural Chemistry, Том. 60, № 9, стр. 1482-1488. https://doi.org/10.1134/S0022476619090130

APA

Baidina, I. A., Belyaev, A. V., Korolkov, I. V., Smolentsev, A. I., & Vorobieva, S. N. (2019). Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series. Journal of Structural Chemistry, 60(9), 1482-1488. https://doi.org/10.1134/S0022476619090130

Vancouver

Baidina IA, Belyaev AV, Korolkov IV, Smolentsev AI, Vorobieva SN. Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series. Journal of Structural Chemistry. 2019 сент. 1;60(9):1482-1488. doi: 10.1134/S0022476619090130

Author

Baidina, I. A. ; Belyaev, A. V. ; Korolkov, I. V. и др. / Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series. в: Journal of Structural Chemistry. 2019 ; Том 60, № 9. стр. 1482-1488.

BibTeX

@article{8a6f42c728fc43dfa5dcbe5fac96ae33,
title = "Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series",
abstract = "Complex compounds cis-K[Rh(NH3)2Cl4]·KCl (I), cis-K[Rh(NH3)2Cl3(NO2)] (II), and K2[Rh(NH3)Cl5] (III) are synthesized. The single crystal X-ray diffraction analysis of the compounds obtained is performed at T = 296 K. Crystallographic data for I are: a = 11.822(5) {\AA}, b = 11.608(5) {\AA}, c = 8.196(4) {\AA}, β = 107.56(2)°, space group C2/m, Z = 4, dcalc = 2.431 g/cm3. For II: a = 8.946(3) {\AA}, b = 5.941(2) {\AA}, c = 8.182(3) {\AA}, space group Pmn21, Z = 2, dcalc= 2.509 g/cm3. For III: a = 13.464(6) {\AA}, b = 9.989(4) {\AA}, c = 6.932(3) {\AA}, space group Pnma, Z = 4, dcalc = 2.675 g/cm3. The compounds are characterized by IR spectroscopy, powder X-ray diffraction, and chemical analysis.",
keywords = "chloro complexes, coordination compounds, crystal structure, diammines, monoammines, nitro complexes, rhodium, RHODIUM(III), IRIDIUM(III), SALTS",
author = "Baidina, {I. A.} and Belyaev, {A. V.} and Korolkov, {I. V.} and Smolentsev, {A. I.} and Vorobieva, {S. N.}",
year = "2019",
month = sep,
day = "1",
doi = "10.1134/S0022476619090130",
language = "English",
volume = "60",
pages = "1482--1488",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "9",

}

RIS

TY - JOUR

T1 - Synthesis and Crystal Structure of Chloride complexes of Rh(III) Diammino- and Monoammino Series

AU - Baidina, I. A.

AU - Belyaev, A. V.

AU - Korolkov, I. V.

AU - Smolentsev, A. I.

AU - Vorobieva, S. N.

PY - 2019/9/1

Y1 - 2019/9/1

N2 - Complex compounds cis-K[Rh(NH3)2Cl4]·KCl (I), cis-K[Rh(NH3)2Cl3(NO2)] (II), and K2[Rh(NH3)Cl5] (III) are synthesized. The single crystal X-ray diffraction analysis of the compounds obtained is performed at T = 296 K. Crystallographic data for I are: a = 11.822(5) Å, b = 11.608(5) Å, c = 8.196(4) Å, β = 107.56(2)°, space group C2/m, Z = 4, dcalc = 2.431 g/cm3. For II: a = 8.946(3) Å, b = 5.941(2) Å, c = 8.182(3) Å, space group Pmn21, Z = 2, dcalc= 2.509 g/cm3. For III: a = 13.464(6) Å, b = 9.989(4) Å, c = 6.932(3) Å, space group Pnma, Z = 4, dcalc = 2.675 g/cm3. The compounds are characterized by IR spectroscopy, powder X-ray diffraction, and chemical analysis.

AB - Complex compounds cis-K[Rh(NH3)2Cl4]·KCl (I), cis-K[Rh(NH3)2Cl3(NO2)] (II), and K2[Rh(NH3)Cl5] (III) are synthesized. The single crystal X-ray diffraction analysis of the compounds obtained is performed at T = 296 K. Crystallographic data for I are: a = 11.822(5) Å, b = 11.608(5) Å, c = 8.196(4) Å, β = 107.56(2)°, space group C2/m, Z = 4, dcalc = 2.431 g/cm3. For II: a = 8.946(3) Å, b = 5.941(2) Å, c = 8.182(3) Å, space group Pmn21, Z = 2, dcalc= 2.509 g/cm3. For III: a = 13.464(6) Å, b = 9.989(4) Å, c = 6.932(3) Å, space group Pnma, Z = 4, dcalc = 2.675 g/cm3. The compounds are characterized by IR spectroscopy, powder X-ray diffraction, and chemical analysis.

KW - chloro complexes

KW - coordination compounds

KW - crystal structure

KW - diammines

KW - monoammines

KW - nitro complexes

KW - rhodium

KW - RHODIUM(III)

KW - IRIDIUM(III)

KW - SALTS

UR - http://www.scopus.com/inward/record.url?scp=85073186749&partnerID=8YFLogxK

U2 - 10.1134/S0022476619090130

DO - 10.1134/S0022476619090130

M3 - Article

AN - SCOPUS:85073186749

VL - 60

SP - 1482

EP - 1488

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 9

ER -

ID: 21855845