Результаты исследований: Публикации в книгах, отчётах, сборниках, трудах конференций › статья в сборнике материалов конференции › научная › Рецензирование
Simple synthesis of pyrazole-derived dithioethers. / Chernova, Nina P.; Pirmanova, Nurgul A.; Dzhienalyev, Tolebi и др.
16TH INTERNATIONAL SCIENTIFIC CONFERENCE CHEMISTRY AND CHEMICAL ENGINEERING IN XXI CENTURY DEDICATED TO PROFESSOR L.P. KULYOV (CCE 2015). ред. / E Korotkova. Elsevier Science B.V., 2015. стр. 277-281 (Procedia Chemistry; Том 15).Результаты исследований: Публикации в книгах, отчётах, сборниках, трудах конференций › статья в сборнике материалов конференции › научная › Рецензирование
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TY - GEN
T1 - Simple synthesis of pyrazole-derived dithioethers
AU - Chernova, Nina P.
AU - Pirmanova, Nurgul A.
AU - Dzhienalyev, Tolebi
AU - Potapov, Andrei S.
PY - 2015
Y1 - 2015
N2 - A number of pyrazole-derived dithioethers were prepared by the reaction of diisothiuronium salts and 2-(3,5-dimethylpyrazol-1-yl)ethanol tosylate in a basic aqueous solution. Diisothiuronium salts were prepared by the reaction of thiourea with alpha,omega-dibromoalkanes containing from two to nine methylene groups. The use of these salts allowed in situ generation ions dithiolate, thus eliminating the need to use hazardous dimercaptans. (c) 2015 Published by Elsevier B.V.
AB - A number of pyrazole-derived dithioethers were prepared by the reaction of diisothiuronium salts and 2-(3,5-dimethylpyrazol-1-yl)ethanol tosylate in a basic aqueous solution. Diisothiuronium salts were prepared by the reaction of thiourea with alpha,omega-dibromoalkanes containing from two to nine methylene groups. The use of these salts allowed in situ generation ions dithiolate, thus eliminating the need to use hazardous dimercaptans. (c) 2015 Published by Elsevier B.V.
KW - pyrazole
KW - thioether ligands
KW - thiourea
KW - thiuronium salts
KW - hybrid ligands
KW - CRYSTAL-STRUCTURES
KW - STRUCTURAL-ANALYSIS
KW - NMR-SPECTROSCOPY
KW - LIGANDS
KW - COMPLEXES
KW - THIOETHER
KW - 1,8-BIS(3,5-DIMETHYL-1-PYRAZOLYL)-3,6-DITHIAOCTANE
KW - DERIVATIVES
KW - SYSTEMS
KW - H-1
U2 - 10.1016/j.proche.2015.10.044
DO - 10.1016/j.proche.2015.10.044
M3 - Conference contribution
T3 - Procedia Chemistry
SP - 277
EP - 281
BT - 16TH INTERNATIONAL SCIENTIFIC CONFERENCE CHEMISTRY AND CHEMICAL ENGINEERING IN XXI CENTURY DEDICATED TO PROFESSOR L.P. KULYOV (CCE 2015)
A2 - Korotkova, E
PB - Elsevier Science B.V.
T2 - 16th International Scientific Conference on Chemistry and Chemical Engineering in XXI century (CCE2015)
Y2 - 25 May 2015 through 29 May 2015
ER -
ID: 25398964