Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
Purification of Single-Walled Carbon Nanotubes Using Acid Treatment and Magnetic Separation. / Gurova, Olga A.; Arhipov, Vyacheslav E.; Koroteev, Viktor O. и др.
в: Physica Status Solidi (B) Basic Research, Том 256, № 9, 1800742, 01.09.2019.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - Purification of Single-Walled Carbon Nanotubes Using Acid Treatment and Magnetic Separation
AU - Gurova, Olga A.
AU - Arhipov, Vyacheslav E.
AU - Koroteev, Viktor O.
AU - Guselnikova, Tatiana Ya
AU - Asanov, Igor P.
AU - Sedelnikova, Olga V.
AU - Okotrub, Alexander V.
PY - 2019/9/1
Y1 - 2019/9/1
N2 - A detailed analysis of TUBALL single-walled carbon nanotubes (SWCNTs) after two-step purification involving acid purification treatment with concentrated HCl, HNO3, H2SO4 and solution of HNO3:H2SO4 followed by magnetic processing is presented. The purity degree from iron higher than 99% is achieved, and the yield obtained by the above process is about 75 wt.%. Such high purity of the resultant sample is achieved by removing of the external iron nanoparticles by acid treatment and following extraction of nanotubes containing encapsulated nanoparticles under applied magnetic field. A comprehensive characterization of SWCNTs by Raman, optical absorption, and X-ray photoelectron spectroscopies reveals purification-induced changes in the integrity, composition, and electronic properties of SWCNT.
AB - A detailed analysis of TUBALL single-walled carbon nanotubes (SWCNTs) after two-step purification involving acid purification treatment with concentrated HCl, HNO3, H2SO4 and solution of HNO3:H2SO4 followed by magnetic processing is presented. The purity degree from iron higher than 99% is achieved, and the yield obtained by the above process is about 75 wt.%. Such high purity of the resultant sample is achieved by removing of the external iron nanoparticles by acid treatment and following extraction of nanotubes containing encapsulated nanoparticles under applied magnetic field. A comprehensive characterization of SWCNTs by Raman, optical absorption, and X-ray photoelectron spectroscopies reveals purification-induced changes in the integrity, composition, and electronic properties of SWCNT.
KW - acid treatment
KW - magnetic separation
KW - purification
KW - single-walled carbon nanotubes
KW - FILMS
KW - MICROWAVE
KW - DISPERSION
KW - RAMAN
KW - COMPOSITES
KW - G(-)
KW - G(+)
UR - http://www.scopus.com/inward/record.url?scp=85067859932&partnerID=8YFLogxK
U2 - 10.1002/pssb.201800742
DO - 10.1002/pssb.201800742
M3 - Article
AN - SCOPUS:85067859932
VL - 256
JO - Physica Status Solidi (B): Basic Research
JF - Physica Status Solidi (B): Basic Research
SN - 0370-1972
IS - 9
M1 - 1800742
ER -
ID: 20708383