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[NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K. / Khranenko, S. P.; Sukhikh, A. S.; Pishchur, D. P. и др.

в: Journal of Structural Chemistry, Том 59, № 8, 01.12.2018, стр. 1897-1902.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Khranenko, SP, Sukhikh, AS, Pishchur, DP, Buneeva, PS, Komarov, VY & Gromilov, SA 2018, '[NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K', Journal of Structural Chemistry, Том. 59, № 8, стр. 1897-1902. https://doi.org/10.1134/S0022476618080188

APA

Khranenko, S. P., Sukhikh, A. S., Pishchur, D. P., Buneeva, P. S., Komarov, V. Y., & Gromilov, S. A. (2018). [NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K. Journal of Structural Chemistry, 59(8), 1897-1902. https://doi.org/10.1134/S0022476618080188

Vancouver

Khranenko SP, Sukhikh AS, Pishchur DP, Buneeva PS, Komarov VY, Gromilov SA. [NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K. Journal of Structural Chemistry. 2018 дек. 1;59(8):1897-1902. doi: 10.1134/S0022476618080188

Author

Khranenko, S. P. ; Sukhikh, A. S. ; Pishchur, D. P. и др. / [NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K. в: Journal of Structural Chemistry. 2018 ; Том 59, № 8. стр. 1897-1902.

BibTeX

@article{236b4ee1c4404282b9343432d7024228,
title = "[NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K",
abstract = "The synthesis method for [NiEn3]WO4 complex salt is described. Data of single crystal X-ray diffraction at 115 K are: space group p3 ¯ , a = 15.9633(5) {\AA}, c = 9.9446(4) {\AA}, V = 2194.6(1) {\AA}3, Z = 6, dx = 2.210 g/cm3, Ni–N is 2.120(2)-2.149(2) {\AA}, ∠N–Ni–N is 80.69(7)-82.28(7)°. From the differential scanning calorimetry data it is found that a phase transition occurs at 269 K. The crystal structural characteristics at 298 K are as follows: space group p3 ¯ 1 c, a = 9.2641(3) {\AA}, c = 9.9817(3) {\AA}, V = 741.89(4) {\AA}3, Z = 2, dx = 2.179 g/cm3, Ni–N is 2.128(2) {\AA}, ∠N–Ni–N is 81.05(12)°. The phase transition is shown to correspond to the disordering of tungstate anions over three positions. The comparative analysis of N–H…O and C–H…O interionic contacts is performed.",
keywords = "bimetallic complex salt, crystal chemistry, differential scanning calorimetry, single crystal X-ray diffraction analysis, tris(ethylenediamine)nickel, tungstate anion, IR",
author = "Khranenko, {S. P.} and Sukhikh, {A. S.} and Pishchur, {D. P.} and Buneeva, {P. S.} and Komarov, {V. Yu} and Gromilov, {S. A.}",
year = "2018",
month = dec,
day = "1",
doi = "10.1134/S0022476618080188",
language = "English",
volume = "59",
pages = "1897--1902",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "8",

}

RIS

TY - JOUR

T1 - [NiEn 3]WO4. Crystal Structural Features Of The Phase Transition At 269 K

AU - Khranenko, S. P.

AU - Sukhikh, A. S.

AU - Pishchur, D. P.

AU - Buneeva, P. S.

AU - Komarov, V. Yu

AU - Gromilov, S. A.

PY - 2018/12/1

Y1 - 2018/12/1

N2 - The synthesis method for [NiEn3]WO4 complex salt is described. Data of single crystal X-ray diffraction at 115 K are: space group p3 ¯ , a = 15.9633(5) Å, c = 9.9446(4) Å, V = 2194.6(1) Å3, Z = 6, dx = 2.210 g/cm3, Ni–N is 2.120(2)-2.149(2) Å, ∠N–Ni–N is 80.69(7)-82.28(7)°. From the differential scanning calorimetry data it is found that a phase transition occurs at 269 K. The crystal structural characteristics at 298 K are as follows: space group p3 ¯ 1 c, a = 9.2641(3) Å, c = 9.9817(3) Å, V = 741.89(4) Å3, Z = 2, dx = 2.179 g/cm3, Ni–N is 2.128(2) Å, ∠N–Ni–N is 81.05(12)°. The phase transition is shown to correspond to the disordering of tungstate anions over three positions. The comparative analysis of N–H…O and C–H…O interionic contacts is performed.

AB - The synthesis method for [NiEn3]WO4 complex salt is described. Data of single crystal X-ray diffraction at 115 K are: space group p3 ¯ , a = 15.9633(5) Å, c = 9.9446(4) Å, V = 2194.6(1) Å3, Z = 6, dx = 2.210 g/cm3, Ni–N is 2.120(2)-2.149(2) Å, ∠N–Ni–N is 80.69(7)-82.28(7)°. From the differential scanning calorimetry data it is found that a phase transition occurs at 269 K. The crystal structural characteristics at 298 K are as follows: space group p3 ¯ 1 c, a = 9.2641(3) Å, c = 9.9817(3) Å, V = 741.89(4) Å3, Z = 2, dx = 2.179 g/cm3, Ni–N is 2.128(2) Å, ∠N–Ni–N is 81.05(12)°. The phase transition is shown to correspond to the disordering of tungstate anions over three positions. The comparative analysis of N–H…O and C–H…O interionic contacts is performed.

KW - bimetallic complex salt

KW - crystal chemistry

KW - differential scanning calorimetry

KW - single crystal X-ray diffraction analysis

KW - tris(ethylenediamine)nickel

KW - tungstate anion

KW - IR

UR - http://www.scopus.com/inward/record.url?scp=85059734739&partnerID=8YFLogxK

U2 - 10.1134/S0022476618080188

DO - 10.1134/S0022476618080188

M3 - Article

AN - SCOPUS:85059734739

VL - 59

SP - 1897

EP - 1902

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 8

ER -

ID: 18108625