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L-Cysteine Nitrates. / Giester, G.; Ghazaryan, V. V.; Minkov, V. S. и др.

в: Journal of Structural Chemistry, Том 64, № 5, 05.2023, стр. 917-931.

Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование

Harvard

Giester, G, Ghazaryan, VV, Minkov, VS, Boldyreva, EV & Petrosyan, AM 2023, 'L-Cysteine Nitrates', Journal of Structural Chemistry, Том. 64, № 5, стр. 917-931. https://doi.org/10.1134/S0022476623050104

APA

Giester, G., Ghazaryan, V. V., Minkov, V. S., Boldyreva, E. V., & Petrosyan, A. M. (2023). L-Cysteine Nitrates. Journal of Structural Chemistry, 64(5), 917-931. https://doi.org/10.1134/S0022476623050104

Vancouver

Giester G, Ghazaryan VV, Minkov VS, Boldyreva EV, Petrosyan AM. L-Cysteine Nitrates. Journal of Structural Chemistry. 2023 май;64(5):917-931. doi: 10.1134/S0022476623050104

Author

Giester, G. ; Ghazaryan, V. V. ; Minkov, V. S. и др. / L-Cysteine Nitrates. в: Journal of Structural Chemistry. 2023 ; Том 64, № 5. стр. 917-931.

BibTeX

@article{6aec8d398e7749548fa35854ae7a82f8,
title = "L-Cysteine Nitrates",
abstract = "The formation of salts in the L-cysteine–HNO3–H2O system was studied yielding three representatives as single crystals: anhydrous L-cysteinium nitrate (L-CysH)NO3 (I) and two new salts (L-CysH⋯L-Cys)NO3 (II) and (L-CysH⋯L-Cys)NO3∙0.5H2O (III) with the dimeric (L-CysH⋯L-Cys) cation. (I), (II) and (III) crystallize in space groups P212121, P21 and I2, respectively. Dimeric cations in (II) and (III) were formed by very short O–H⋯O hydrogen bonds with R(O⋯O) distances of 2.440(2) {\AA} and 2.4352(17) {\AA}, respectively. Infrared and Raman spectra of (I–III) were registered and discussed in relation to crystal structures. Characteristics of dimeric cations are compared with those in the previously obtained compounds of L-CysH(L-CysH⋯L-Cys)F(F⋯HF), (L-CysH⋯L-Cys)Cl, (L-CysH⋯L-Cys)Br and (L-CysH⋯L-Cys)I·0.5H2O.",
keywords = "L-cysteine, crystal structure, dimeric cation, nitrates, short hydrogen bonds, vibrational spectra",
author = "G. Giester and Ghazaryan, {V. V.} and Minkov, {V. S.} and Boldyreva, {E. V.} and Petrosyan, {A. M.}",
note = "This work was supported in part by a research grant matsc-3822 from the Armenian National Science and Education Fund (ANSEF) based in New York, USA. This work was supported by the RA MES State Committee of Science and Russian Foundation for Basic Research (RF) in the frames of the joint research projects SCS 15RF-007 and RFBR 15-53-05023. Публикация для корректировки.",
year = "2023",
month = may,
doi = "10.1134/S0022476623050104",
language = "English",
volume = "64",
pages = "917--931",
journal = "Journal of Structural Chemistry",
issn = "0022-4766",
publisher = "Springer GmbH & Co, Auslieferungs-Gesellschaf",
number = "5",

}

RIS

TY - JOUR

T1 - L-Cysteine Nitrates

AU - Giester, G.

AU - Ghazaryan, V. V.

AU - Minkov, V. S.

AU - Boldyreva, E. V.

AU - Petrosyan, A. M.

N1 - This work was supported in part by a research grant matsc-3822 from the Armenian National Science and Education Fund (ANSEF) based in New York, USA. This work was supported by the RA MES State Committee of Science and Russian Foundation for Basic Research (RF) in the frames of the joint research projects SCS 15RF-007 and RFBR 15-53-05023. Публикация для корректировки.

PY - 2023/5

Y1 - 2023/5

N2 - The formation of salts in the L-cysteine–HNO3–H2O system was studied yielding three representatives as single crystals: anhydrous L-cysteinium nitrate (L-CysH)NO3 (I) and two new salts (L-CysH⋯L-Cys)NO3 (II) and (L-CysH⋯L-Cys)NO3∙0.5H2O (III) with the dimeric (L-CysH⋯L-Cys) cation. (I), (II) and (III) crystallize in space groups P212121, P21 and I2, respectively. Dimeric cations in (II) and (III) were formed by very short O–H⋯O hydrogen bonds with R(O⋯O) distances of 2.440(2) Å and 2.4352(17) Å, respectively. Infrared and Raman spectra of (I–III) were registered and discussed in relation to crystal structures. Characteristics of dimeric cations are compared with those in the previously obtained compounds of L-CysH(L-CysH⋯L-Cys)F(F⋯HF), (L-CysH⋯L-Cys)Cl, (L-CysH⋯L-Cys)Br and (L-CysH⋯L-Cys)I·0.5H2O.

AB - The formation of salts in the L-cysteine–HNO3–H2O system was studied yielding three representatives as single crystals: anhydrous L-cysteinium nitrate (L-CysH)NO3 (I) and two new salts (L-CysH⋯L-Cys)NO3 (II) and (L-CysH⋯L-Cys)NO3∙0.5H2O (III) with the dimeric (L-CysH⋯L-Cys) cation. (I), (II) and (III) crystallize in space groups P212121, P21 and I2, respectively. Dimeric cations in (II) and (III) were formed by very short O–H⋯O hydrogen bonds with R(O⋯O) distances of 2.440(2) Å and 2.4352(17) Å, respectively. Infrared and Raman spectra of (I–III) were registered and discussed in relation to crystal structures. Characteristics of dimeric cations are compared with those in the previously obtained compounds of L-CysH(L-CysH⋯L-Cys)F(F⋯HF), (L-CysH⋯L-Cys)Cl, (L-CysH⋯L-Cys)Br and (L-CysH⋯L-Cys)I·0.5H2O.

KW - L-cysteine

KW - crystal structure

KW - dimeric cation

KW - nitrates

KW - short hydrogen bonds

KW - vibrational spectra

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-85160930687&origin=inward&txGid=a177550191c27510d2922fafcee97d6f

UR - https://www.mendeley.com/catalogue/f676ca73-fb09-368e-afe7-106897acba05/

U2 - 10.1134/S0022476623050104

DO - 10.1134/S0022476623050104

M3 - Article

VL - 64

SP - 917

EP - 931

JO - Journal of Structural Chemistry

JF - Journal of Structural Chemistry

SN - 0022-4766

IS - 5

ER -

ID: 59646995