Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
Approach to the study of the dynamics of unit cell parameters of single crystal in a wide temperature range on the example of Ag0.39Li0.61GaSe2. / Panchenko, A. V.; Sukhikh, A. S.; Isaenko, L. I. и др.
в: Journal of Structural Chemistry, Том 63, № 10, 10.2022, стр. 1662-1669.Результаты исследований: Научные публикации в периодических изданиях › статья › Рецензирование
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TY - JOUR
T1 - Approach to the study of the dynamics of unit cell parameters of single crystal in a wide temperature range on the example of Ag0.39Li0.61GaSe2
AU - Panchenko, A. V.
AU - Sukhikh, A. S.
AU - Isaenko, L. I.
AU - Gromilov, S. A.
N1 - Funding Information: The LiAgGaSe crystals were grown with the support of the Russian Science Foundation (project No. 19-12-00085). The composition of the grown crystals was analyzed within the State Task for IGM SB RAS. x 1–x 2 Funding Information: This work was funded by the Ministry of Science and Higher Education of the Russian Federation, project No. 121031700313-8. Publisher Copyright: © 2022, Pleiades Publishing, Ltd.
PY - 2022/10
Y1 - 2022/10
N2 - We report a technique for the refinement of unit cell parameters by using external referencing for goniometer calibration, processing the 2D profile of diffraction reflection, and introducing corrections. The changes of unit cell parameters of the Ag0.39Li0.61GaSe2 single crystal is studied in the temperature range from 100 K to 480 K. As the volume of the tetragonal unit cell increases by 1%, parameter a increases by 0.6% and parameter c decreases by 0.3%.
AB - We report a technique for the refinement of unit cell parameters by using external referencing for goniometer calibration, processing the 2D profile of diffraction reflection, and introducing corrections. The changes of unit cell parameters of the Ag0.39Li0.61GaSe2 single crystal is studied in the temperature range from 100 K to 480 K. As the volume of the tetragonal unit cell increases by 1%, parameter a increases by 0.6% and parameter c decreases by 0.3%.
KW - single-crystal XRD
KW - temperature dependence
KW - unit cell parameters
UR - http://www.scopus.com/inward/record.url?scp=85141209878&partnerID=8YFLogxK
UR - https://www.mendeley.com/catalogue/d3125eee-6e84-34b7-90f8-b303208ef62f/
U2 - 10.1134/S0022476622100122
DO - 10.1134/S0022476622100122
M3 - Article
AN - SCOPUS:85141209878
VL - 63
SP - 1662
EP - 1669
JO - Journal of Structural Chemistry
JF - Journal of Structural Chemistry
SN - 0022-4766
IS - 10
ER -
ID: 39125944