Zeolite/silica aerogel composite monoliths and microspheres

Standard

Zeolite/silica aerogel composite monoliths and microspheres. / Sashkina, Kseniya A.; Gurikov, Pavel A.; Ayupov, Artem B. et al.

In: Microporous and Mesoporous Materials, Vol. 263, 01.06.2018, p. 106-112.

Research output: Contribution to journal › Article › peer-review

Harvard

Sashkina, KA, Gurikov, PA, Ayupov, AB, Smirnova, I & Parkhomchuk, EV 2018, 'Zeolite/silica aerogel composite monoliths and microspheres', Microporous and Mesoporous Materials, vol. 263, pp. 106-112. https://doi.org/10.1016/j.micromeso.2017.12.010

APA

Sashkina, K. A., Gurikov, P. A., Ayupov, A. B., Smirnova, I., & Parkhomchuk, E. V. (2018). Zeolite/silica aerogel composite monoliths and microspheres. Microporous and Mesoporous Materials, 263, 106-112. https://doi.org/10.1016/j.micromeso.2017.12.010

Vancouver

Sashkina KA, Gurikov PA, Ayupov AB, Smirnova I, Parkhomchuk EV. Zeolite/silica aerogel composite monoliths and microspheres. Microporous and Mesoporous Materials. 2018 Jun 1;263:106-112. doi: 10.1016/j.micromeso.2017.12.010

Author

Sashkina, Kseniya A. ; Gurikov, Pavel A. ; Ayupov, Artem B. et al. / Zeolite/silica aerogel composite monoliths and microspheres. In: Microporous and Mesoporous Materials. 2018 ; Vol. 263. pp. 106-112.

BibTeX

@article{cbf840ff1d0b441ba9c078f42b5e82f9,

title = "Zeolite/silica aerogel composite monoliths and microspheres",

abstract = "A series of silica aerogels and composite materials based on Fe-silicalite-1 nanocrystals embedded into silica aerogel matrix in the form of monoliths and microspheres have been synthesized by drying with supercritical CO2. Using equivolume water/ethanol mixture as a medium for the aging of monoliths enabled to produce monoliths of silica aerogel and composite without cracks. The synthesis of the composite and silica aerogel microspheres by the emulsion/gelation technique has been designed. The different effects of the stirring rate during the emulsification on the particle size and texture of composites and silica aerogels has been observed. The synthesized samples were characterized by X-ray diffraction, scanning electron microscopy and nitrogen adsorption measurements.",

keywords = "Composite, Emulsion/gelation, Fe-silicalite-1, Monolith, Silica aerogel, Supercritical CO, Zeolite",

author = "Sashkina, {Kseniya A.} and Gurikov, {Pavel A.} and Ayupov, {Artem B.} and Irina Smirnova and Parkhomchuk, {Ekaterina V.}",

note = "This work was performed within the framework of budget project No. 0303-2016-0010 for Boreskov Institute of Catalysis. Publisher Copyright: {\textcopyright} 2017 Elsevier Inc.",

year = "2018",

month = jun,

day = "1",

doi = "10.1016/j.micromeso.2017.12.010",

language = "English",

volume = "263",

pages = "106--112",

journal = "Microporous and Mesoporous Materials",

issn = "1387-1811",

publisher = "Elsevier",

}

RIS

TY - JOUR

T1 - Zeolite/silica aerogel composite monoliths and microspheres

AU - Sashkina, Kseniya A.

AU - Gurikov, Pavel A.

AU - Ayupov, Artem B.

AU - Smirnova, Irina

AU - Parkhomchuk, Ekaterina V.

PY - 2018/6/1

Y1 - 2018/6/1

N2 - A series of silica aerogels and composite materials based on Fe-silicalite-1 nanocrystals embedded into silica aerogel matrix in the form of monoliths and microspheres have been synthesized by drying with supercritical CO2. Using equivolume water/ethanol mixture as a medium for the aging of monoliths enabled to produce monoliths of silica aerogel and composite without cracks. The synthesis of the composite and silica aerogel microspheres by the emulsion/gelation technique has been designed. The different effects of the stirring rate during the emulsification on the particle size and texture of composites and silica aerogels has been observed. The synthesized samples were characterized by X-ray diffraction, scanning electron microscopy and nitrogen adsorption measurements.

AB - A series of silica aerogels and composite materials based on Fe-silicalite-1 nanocrystals embedded into silica aerogel matrix in the form of monoliths and microspheres have been synthesized by drying with supercritical CO2. Using equivolume water/ethanol mixture as a medium for the aging of monoliths enabled to produce monoliths of silica aerogel and composite without cracks. The synthesis of the composite and silica aerogel microspheres by the emulsion/gelation technique has been designed. The different effects of the stirring rate during the emulsification on the particle size and texture of composites and silica aerogels has been observed. The synthesized samples were characterized by X-ray diffraction, scanning electron microscopy and nitrogen adsorption measurements.

KW - Composite

KW - Emulsion/gelation

KW - Fe-silicalite-1

KW - Monolith

KW - Silica aerogel

KW - Supercritical CO

KW - Zeolite

UR - http://www.scopus.com/inward/record.url?scp=85038034147&partnerID=8YFLogxK

U2 - 10.1016/j.micromeso.2017.12.010

DO - 10.1016/j.micromeso.2017.12.010

M3 - Article

AN - SCOPUS:85038034147

VL - 263

SP - 106

EP - 112

JO - Microporous and Mesoporous Materials

JF - Microporous and Mesoporous Materials

SN - 1387-1811

ER -

ID: 9154343