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Towards high-quality nitrogen-doped diamond single crystals for X-ray optics. / Shevyrtalov, Sergey; Barannikov, Alexander; Palyanov, Yurii et al.

In: Journal of Synchrotron Radiation, Vol. 28, 01.01.2021, p. 104-110.

Research output: Contribution to journal › Article › peer-review

Harvard

Shevyrtalov, S, Barannikov, A, Palyanov, Y, Khokhryakov, A, Borzdov, Y, Sergueev, I, Rashchenko, S & Snigirev, A 2021, 'Towards high-quality nitrogen-doped diamond single crystals for X-ray optics', Journal of Synchrotron Radiation, vol. 28, pp. 104-110. https://doi.org/10.1107/S1600577520014538

APA

Shevyrtalov, S., Barannikov, A., Palyanov, Y., Khokhryakov, A., Borzdov, Y., Sergueev, I., Rashchenko, S., & Snigirev, A. (2021). Towards high-quality nitrogen-doped diamond single crystals for X-ray optics. Journal of Synchrotron Radiation, 28, 104-110. https://doi.org/10.1107/S1600577520014538

Vancouver

Shevyrtalov S, Barannikov A, Palyanov Y, Khokhryakov A, Borzdov Y, Sergueev I et al. Towards high-quality nitrogen-doped diamond single crystals for X-ray optics. Journal of Synchrotron Radiation. 2021 Jan 1;28:104-110. doi: 10.1107/S1600577520014538

Author

Shevyrtalov, Sergey ; Barannikov, Alexander ; Palyanov, Yurii et al. / Towards high-quality nitrogen-doped diamond single crystals for X-ray optics. In: Journal of Synchrotron Radiation. 2021 ; Vol. 28. pp. 104-110.

BibTeX

@article{af26d2360b8d4e68b9e42922c2cdfa60,
title = "Towards high-quality nitrogen-doped diamond single crystals for X-ray optics",
abstract = "In this manuscript, characterization of single-crystalline (111) plates prepared from type-Ib diamonds with a nitrogen content of 100-150 ppm by means of high-resolution rocking-curve imaging (RCI) is reported. Contrary to common opinion regarding the intrinsically poor diffraction quality of type-I diamonds, RCI showed the presence of nearly defect-free areas of several millimetres squared in the central part of the diamond plates. The observed broadening of the rocking curves is a result of the cutting and polishing processes, causing strains around the edges of the plates and rare defects. An improvement of the preparation technique will thus allow single-crystalline diamond plates to be made for Laue and Bragg monochromators and beam splitters from type-Ib material with areas large enough to be used as optical elements at fourth-generation synchrotron facilities. ",
keywords = "diamond single crystal, rocking curve imaging, X-ray optics",
author = "Sergey Shevyrtalov and Alexander Barannikov and Yurii Palyanov and Alexander Khokhryakov and Yurii Borzdov and Ilya Sergueev and Sergey Rashchenko and Anatoly Snigirev",
note = "Funding Information: This research was funded by RFBR (project No. 19-29-12040) and the Ministry of Science and Higher Education of the Russian Foundation on state assignment of IGM SB RAS. Publisher Copyright: {\textcopyright} 2021 International Union of Crystallography. Copyright: Copyright 2021 Elsevier B.V., All rights reserved.",
year = "2021",
month = jan,
day = "1",
doi = "10.1107/S1600577520014538",
language = "English",
volume = "28",
pages = "104--110",
journal = "Journal of Synchrotron Radiation",
issn = "0909-0495",
publisher = "International Union of Crystallography",

}

RIS

TY - JOUR

T1 - Towards high-quality nitrogen-doped diamond single crystals for X-ray optics

AU - Shevyrtalov, Sergey

AU - Barannikov, Alexander

AU - Palyanov, Yurii

AU - Khokhryakov, Alexander

AU - Borzdov, Yurii

AU - Sergueev, Ilya

AU - Rashchenko, Sergey

AU - Snigirev, Anatoly

N1 - Funding Information: This research was funded by RFBR (project No. 19-29-12040) and the Ministry of Science and Higher Education of the Russian Foundation on state assignment of IGM SB RAS. Publisher Copyright: © 2021 International Union of Crystallography. Copyright: Copyright 2021 Elsevier B.V., All rights reserved.

PY - 2021/1/1

Y1 - 2021/1/1

N2 - In this manuscript, characterization of single-crystalline (111) plates prepared from type-Ib diamonds with a nitrogen content of 100-150 ppm by means of high-resolution rocking-curve imaging (RCI) is reported. Contrary to common opinion regarding the intrinsically poor diffraction quality of type-I diamonds, RCI showed the presence of nearly defect-free areas of several millimetres squared in the central part of the diamond plates. The observed broadening of the rocking curves is a result of the cutting and polishing processes, causing strains around the edges of the plates and rare defects. An improvement of the preparation technique will thus allow single-crystalline diamond plates to be made for Laue and Bragg monochromators and beam splitters from type-Ib material with areas large enough to be used as optical elements at fourth-generation synchrotron facilities.

AB - In this manuscript, characterization of single-crystalline (111) plates prepared from type-Ib diamonds with a nitrogen content of 100-150 ppm by means of high-resolution rocking-curve imaging (RCI) is reported. Contrary to common opinion regarding the intrinsically poor diffraction quality of type-I diamonds, RCI showed the presence of nearly defect-free areas of several millimetres squared in the central part of the diamond plates. The observed broadening of the rocking curves is a result of the cutting and polishing processes, causing strains around the edges of the plates and rare defects. An improvement of the preparation technique will thus allow single-crystalline diamond plates to be made for Laue and Bragg monochromators and beam splitters from type-Ib material with areas large enough to be used as optical elements at fourth-generation synchrotron facilities.

KW - diamond single crystal

KW - rocking curve imaging

KW - X-ray optics

UR - http://www.scopus.com/inward/record.url?scp=85099429199&partnerID=8YFLogxK

U2 - 10.1107/S1600577520014538

DO - 10.1107/S1600577520014538

M3 - Article

C2 - 33399558

AN - SCOPUS:85099429199

VL - 28

SP - 104

EP - 110

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

SN - 0909-0495

ER -

ID: 28011437