To touch or not to touch? Fingerprint-assisted grinding of carbamazepine form III

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To touch or not to touch? Fingerprint-assisted grinding of carbamazepine form III. / Zheltikova, Daria; Losev, Evgeniy ; Boldyreva, Elena.

In: CrystEngComm, Vol. 25, No. 34, 21.07.2023, p. 4879-4888.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{38acc120eebf434fabbb6f48db684d3b,

title = "To touch or not to touch? Fingerprint-assisted grinding of carbamazepine form III",

abstract = "Mechanically induced polymorphic transformation of polymorph III of carbamazepine into form IV was accelerated and brought to completion by contaminating deliberately a milling jar and ball by touching them with fingers. In model experiments with additives of water and fatty acids (important components of fingerprints), carbamazepine dihydrate and carbamazepine form II, respectively, were obtained, without any evidence of form IV, as a result of mechanical treatment under otherwise the same milling conditions. A possible interpretation was suggested.",

author = "Daria Zheltikova and Evgeniy Losev and Elena Boldyreva",

note = "This work was funded by the Russian Foundation of Basic Research (Project 19-29-12026-mk) at the Boreskov Institute of Catalysis SB RAS (EL and EB) and by the Strategic Academic Leadership Program “Priority 2030” from Russian Ministry of Education and Science at the Novosibirsk State University (DZ). The equipment of the Chair of Solid-State Chemistry and Laboratory MDEST of the REC INChT, Novosibirsk State University was used.",

year = "2023",

month = jul,

day = "21",

doi = "10.1039/d3ce00544e",

language = "English",

volume = "25",

pages = "4879--4888",

journal = "CrystEngComm",

issn = "1466-8033",

publisher = "Royal Society of Chemistry",

number = "34",

}

RIS

TY - JOUR

T1 - To touch or not to touch? Fingerprint-assisted grinding of carbamazepine form III

AU - Zheltikova, Daria

AU - Losev, Evgeniy

AU - Boldyreva, Elena

N1 - This work was funded by the Russian Foundation of Basic Research (Project 19-29-12026-mk) at the Boreskov Institute of Catalysis SB RAS (EL and EB) and by the Strategic Academic Leadership Program “Priority 2030” from Russian Ministry of Education and Science at the Novosibirsk State University (DZ). The equipment of the Chair of Solid-State Chemistry and Laboratory MDEST of the REC INChT, Novosibirsk State University was used.

PY - 2023/7/21

Y1 - 2023/7/21

N2 - Mechanically induced polymorphic transformation of polymorph III of carbamazepine into form IV was accelerated and brought to completion by contaminating deliberately a milling jar and ball by touching them with fingers. In model experiments with additives of water and fatty acids (important components of fingerprints), carbamazepine dihydrate and carbamazepine form II, respectively, were obtained, without any evidence of form IV, as a result of mechanical treatment under otherwise the same milling conditions. A possible interpretation was suggested.

AB - Mechanically induced polymorphic transformation of polymorph III of carbamazepine into form IV was accelerated and brought to completion by contaminating deliberately a milling jar and ball by touching them with fingers. In model experiments with additives of water and fatty acids (important components of fingerprints), carbamazepine dihydrate and carbamazepine form II, respectively, were obtained, without any evidence of form IV, as a result of mechanical treatment under otherwise the same milling conditions. A possible interpretation was suggested.

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-85168615968&origin=inward&txGid=73b3ed28074b4be4bf7f5cb105e8fc56

UR - https://www.mendeley.com/catalogue/ee7cc897-310d-39d3-9e34-fe70d43ce703/

U2 - 10.1039/d3ce00544e

DO - 10.1039/d3ce00544e

M3 - Article

VL - 25

SP - 4879

EP - 4888

JO - CrystEngComm

JF - CrystEngComm

SN - 1466-8033

IS - 34

ER -

ID: 59263215