The Synthesis of Monodisperse MFI Nanozeolites

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The Synthesis of Monodisperse MFI Nanozeolites : Controlling the Crystallization Process. / Sashkina, K. A.; Shestakova, D. O.; Parkhomchuk, E. V.

In: Petroleum Chemistry, Vol. 60, No. 8, 01.08.2020, p. 881-889.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{fbaa60a7265242e6aac31c9175e52031,

title = "The Synthesis of Monodisperse MFI Nanozeolites: Controlling the Crystallization Process",

abstract = "The sinthesis conditions of a series of monodisperse crystals of ZSM-5 zeolite, silicalite-1, and Fe-silicalite-1 with an average particle size in the range of 30 to 450 nm have been determined. The kinetic features of the silicalite-1 crystallization at low temperatures (60−90°C) and atmospheric pressure have been studied. The effective activation energies of silicalite-1 nucliation and crystal growth have been determined to be 95 ± 7 and 100 ± 7 kJ/mol, respectively. The influence of the synthesis time and temperature as well as the silicon source concentration on the size of the MFI type nanocrystals has been studied.",

keywords = "crystallization, Fe-silicalite-1, nanozeolites, silicalite-1, ZSM-5, MECHANISM, PARTICLES, SIZE, TPA-SILICALITE-1, IN-SITU OBSERVATION, ZSM-5 ZEOLITES, CRYSTAL-GROWTH, KINETICS, NUCLEATION, CATALYSTS",

author = "Sashkina, {K. A.} and Shestakova, {D. O.} and Parkhomchuk, {E. V.}",

year = "2020",

month = aug,

day = "1",

doi = "10.1134/S0965544120080137",

language = "English",

volume = "60",

pages = "881--889",

journal = "Petroleum Chemistry",

issn = "0965-5441",

publisher = "Maik Nauka-Interperiodica Publishing",

number = "8",

}

RIS

TY - JOUR

T1 - The Synthesis of Monodisperse MFI Nanozeolites

T2 - Controlling the Crystallization Process

AU - Sashkina, K. A.

AU - Shestakova, D. O.

AU - Parkhomchuk, E. V.

PY - 2020/8/1

Y1 - 2020/8/1

N2 - The sinthesis conditions of a series of monodisperse crystals of ZSM-5 zeolite, silicalite-1, and Fe-silicalite-1 with an average particle size in the range of 30 to 450 nm have been determined. The kinetic features of the silicalite-1 crystallization at low temperatures (60−90°C) and atmospheric pressure have been studied. The effective activation energies of silicalite-1 nucliation and crystal growth have been determined to be 95 ± 7 and 100 ± 7 kJ/mol, respectively. The influence of the synthesis time and temperature as well as the silicon source concentration on the size of the MFI type nanocrystals has been studied.

AB - The sinthesis conditions of a series of monodisperse crystals of ZSM-5 zeolite, silicalite-1, and Fe-silicalite-1 with an average particle size in the range of 30 to 450 nm have been determined. The kinetic features of the silicalite-1 crystallization at low temperatures (60−90°C) and atmospheric pressure have been studied. The effective activation energies of silicalite-1 nucliation and crystal growth have been determined to be 95 ± 7 and 100 ± 7 kJ/mol, respectively. The influence of the synthesis time and temperature as well as the silicon source concentration on the size of the MFI type nanocrystals has been studied.

KW - crystallization

KW - Fe-silicalite-1

KW - nanozeolites

KW - silicalite-1

KW - ZSM-5

KW - MECHANISM

KW - PARTICLES

KW - SIZE

KW - TPA-SILICALITE-1

KW - IN-SITU OBSERVATION

KW - ZSM-5 ZEOLITES

KW - CRYSTAL-GROWTH

KW - KINETICS

KW - NUCLEATION

KW - CATALYSTS

UR - http://www.scopus.com/inward/record.url?scp=85089969256&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/b19f57ce-6856-3c61-9a3c-8733145b5b74/

U2 - 10.1134/S0965544120080137

DO - 10.1134/S0965544120080137

M3 - Article

AN - SCOPUS:85089969256

VL - 60

SP - 881

EP - 889

JO - Petroleum Chemistry

JF - Petroleum Chemistry

SN - 0965-5441

IS - 8

ER -

ID: 25291212

The Synthesis of Monodisperse MFI Nanozeolites: Controlling the Crystallization Process

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