Research output: Contribution to journal › Article › peer-review
Synthesis of Stoichiometric and Substituted ss-Tricalciumphosphate Using Mechanochemistry. / Chaikina, M.; Bulina, N.; Vinokurova, O. B. et al.
In: Chemistry for Sustainable Development, Vol. 28, No. 1, 2020, p. 71-76.Research output: Contribution to journal › Article › peer-review
}
TY - JOUR
T1 - Synthesis of Stoichiometric and Substituted ss-Tricalciumphosphate Using Mechanochemistry
AU - Chaikina, M.
AU - Bulina, N.
AU - Vinokurova, O. B.
AU - Prosanov, I. Yu
PY - 2020
Y1 - 2020
N2 - A solid-phase method was developed for the synthesis of ss-tricalciumphosphate (ss-TCP) with the stoichiometric composition and with partial substitution of calcium ions for copper, zinc and silver ions. The method involves preliminary preparation of precursors by means of mechanical activation of reaction mixtures. The start of ss-TCP formation was detected directly during the activation of reaction mixtures in the mill. The optimal conditions for activation, the temperature and the duration of annealing were determined.
AB - A solid-phase method was developed for the synthesis of ss-tricalciumphosphate (ss-TCP) with the stoichiometric composition and with partial substitution of calcium ions for copper, zinc and silver ions. The method involves preliminary preparation of precursors by means of mechanical activation of reaction mixtures. The start of ss-TCP formation was detected directly during the activation of reaction mixtures in the mill. The optimal conditions for activation, the temperature and the duration of annealing were determined.
KW - ss-tricalciumphosphate
KW - synthesis
KW - mechanical activation
KW - precursor
KW - PHOSPHATE
U2 - 10.15372/CSD2020205
DO - 10.15372/CSD2020205
M3 - Article
VL - 28
SP - 71
EP - 76
JO - Chemistry for Sustainable Development
JF - Chemistry for Sustainable Development
SN - 1817-1818
IS - 1
ER -
ID: 26077152