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SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE. / VINOGRADOV, Artem S.; S.B., KALASHNIKOV; V.E., PLATONOV et al.

In: Chemistry for Sustainable Development, Vol. 31, No. 6, 2023, p. 614-618.

Research output: Contribution to journal › Article › peer-review

Harvard

VINOGRADOV, AS, S.B., KALASHNIKOV, V.E., PLATONOV & T.V., MEZHENKOVA 2023, 'SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE', Chemistry for Sustainable Development, vol. 31, no. 6, pp. 614-618. https://doi.org/10.15372/csd2023508

APA

VINOGRADOV, A. S., S.B., KALASHNIKOV., V.E., PLATONOV., & T.V., MEZHENKOVA. (2023). SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE. Chemistry for Sustainable Development, 31(6), 614-618. https://doi.org/10.15372/csd2023508

Vancouver

VINOGRADOV AS, S.B. KALASHNIKOV, V.E. PLATONOV, T.V. MEZHENKOVA. SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE. Chemistry for Sustainable Development. 2023;31(6):614-618. doi: 10.15372/csd2023508

Author

VINOGRADOV, Artem S. ; S.B., KALASHNIKOV ; V.E., PLATONOV et al. / SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE. In: Chemistry for Sustainable Development. 2023 ; Vol. 31, No. 6. pp. 614-618.

BibTeX

@article{f9d27c04d64e4b11b30af4194791f164,
title = "SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE",
abstract = "1-(Pentafluorophenyl)propan-1-one reacts with zinc in the presence of catalytic amounts of SnCl2 under heating in dimethyl formamide to give (2,3,5,6-tetrafluoro-4-propionylphenyl)zinc chloride and bis(2,3,5,6-tetrafluoro-4-propionylphenyl)zinc. 1,1¢-(2,3,5,6-Tetrafluoro-1,4-phenylene)dipropan-1-one was synthesized from these organozinc compounds and propionyl chloride in the presence of CuI. The reaction of organozinc compounds obtained from 3-bromo-1,2,4,5-tetrafluorobenzene leads to the formation of 1-(2,3,5,6-tetrafluorophenyl)propan-1-one",
keywords = "KETONE, ZINC, ORGANOZINC COMPOUNDS, PROPIONYL CHLORIDE",
author = "VINOGRADOV, {Artem S.} and KALASHNIKOV S.B. and PLATONOV V.E. and MEZHENKOVA T.V.",
note = "The work was supported by the Russian Science Foundation (grant No. 23-23-00547). 1. ПОЛИФТОРИРОВАННЫЕ АРОМАТИЧЕСКИЕ ТЕТРАКАРБОНОВЫЕ КИСЛОТЫ – ПЕРСПЕКТИВНЫЕ СТРУКТУРНЫЕ БЛОКИ ДЛЯ СОВРЕМЕННЫХ ФУНКЦИОНАЛЬНЫХ МАТЕРИАЛОВ. СИНТЕЗ И ИЗУЧЕНИЕ ФИЗИКО-ХИМИЧЕСКИХ СВОЙСТВ Виноградов А.С. Synthesis of 1,1′-(2,3,5,6-Tetrafluoro-1,4-phenylene)dipropan-1-one / A. S. Vinogradov, S. B. Kalashnikov, V. E. Platonov, T. V. Mezhenkova // Chemistry for Sustainable Development. – 2023. – Vol. 31, No. 6. – P. 614-618. – DOI 10.15372/CSD2023508. ",
year = "2023",
doi = "10.15372/csd2023508",
language = "English",
volume = "31",
pages = "614--618",
journal = "Chemistry for Sustainable Development",
issn = "1817-1818",
publisher = "ФГУП {"}Издательство СО РАН{"}",
number = "6",

}

RIS

TY - JOUR

T1 - SYNTHESIS OF 1,1′-(2,3,5,6-TETRAFLUORO-1,4-PHENYLENE)DIPROPAN-1-ONE

AU - VINOGRADOV, Artem S.

AU - S.B., KALASHNIKOV

AU - V.E., PLATONOV

AU - T.V., MEZHENKOVA

N1 - The work was supported by the Russian Science Foundation (grant No. 23-23-00547). 1. ПОЛИФТОРИРОВАННЫЕ АРОМАТИЧЕСКИЕ ТЕТРАКАРБОНОВЫЕ КИСЛОТЫ – ПЕРСПЕКТИВНЫЕ СТРУКТУРНЫЕ БЛОКИ ДЛЯ СОВРЕМЕННЫХ ФУНКЦИОНАЛЬНЫХ МАТЕРИАЛОВ. СИНТЕЗ И ИЗУЧЕНИЕ ФИЗИКО-ХИМИЧЕСКИХ СВОЙСТВ Виноградов А.С. Synthesis of 1,1′-(2,3,5,6-Tetrafluoro-1,4-phenylene)dipropan-1-one / A. S. Vinogradov, S. B. Kalashnikov, V. E. Platonov, T. V. Mezhenkova // Chemistry for Sustainable Development. – 2023. – Vol. 31, No. 6. – P. 614-618. – DOI 10.15372/CSD2023508.

PY - 2023

Y1 - 2023

N2 - 1-(Pentafluorophenyl)propan-1-one reacts with zinc in the presence of catalytic amounts of SnCl2 under heating in dimethyl formamide to give (2,3,5,6-tetrafluoro-4-propionylphenyl)zinc chloride and bis(2,3,5,6-tetrafluoro-4-propionylphenyl)zinc. 1,1¢-(2,3,5,6-Tetrafluoro-1,4-phenylene)dipropan-1-one was synthesized from these organozinc compounds and propionyl chloride in the presence of CuI. The reaction of organozinc compounds obtained from 3-bromo-1,2,4,5-tetrafluorobenzene leads to the formation of 1-(2,3,5,6-tetrafluorophenyl)propan-1-one

AB - 1-(Pentafluorophenyl)propan-1-one reacts with zinc in the presence of catalytic amounts of SnCl2 under heating in dimethyl formamide to give (2,3,5,6-tetrafluoro-4-propionylphenyl)zinc chloride and bis(2,3,5,6-tetrafluoro-4-propionylphenyl)zinc. 1,1¢-(2,3,5,6-Tetrafluoro-1,4-phenylene)dipropan-1-one was synthesized from these organozinc compounds and propionyl chloride in the presence of CuI. The reaction of organozinc compounds obtained from 3-bromo-1,2,4,5-tetrafluorobenzene leads to the formation of 1-(2,3,5,6-tetrafluorophenyl)propan-1-one

KW - KETONE

KW - ZINC

KW - ORGANOZINC COMPOUNDS

KW - PROPIONYL CHLORIDE

UR - https://www.mendeley.com/catalogue/1abad61b-2c90-39a7-a432-e2afdcf01988/

UR - https://www.elibrary.ru/item.asp?id=59461425

U2 - 10.15372/csd2023508

DO - 10.15372/csd2023508

M3 - Article

VL - 31

SP - 614

EP - 618

JO - Chemistry for Sustainable Development

JF - Chemistry for Sustainable Development

SN - 1817-1818

IS - 6

ER -

ID: 68316979