Research output: Contribution to journal › Article › peer-review
Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity. / Adonin, Nicolay Yu; Prikhod’ko, Sergey A.; Shabalin, Anton Yu et al.
In: Silicon, Vol. 7, No. 2, 18.04.2015, p. 79-87.Research output: Contribution to journal › Article › peer-review
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TY - JOUR
T1 - Synthesis and Structural Features of Nanostructured Cuprous Chloride with High Catalytic Activity
AU - Adonin, Nicolay Yu
AU - Prikhod’ko, Sergey A.
AU - Shabalin, Anton Yu
AU - Prosvirin, Igor P.
AU - Zaikovskii, Vladimir I.
AU - Kochubey, Dmitry I.
AU - Zyuzin, Dmitry A.
AU - Parmon, Valentin N.
AU - Monin, Evgeny A.
AU - Bykova, Irina A.
AU - Martynov, Petr O.
AU - Rusakov, Sergey L.
AU - Storozhenko, Pavel A.
PY - 2015/4/18
Y1 - 2015/4/18
N2 - A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl2⋅2H2O and Cu(OH)2 mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.
AB - A method for nanostructured cuprous chloride preparation by reductive thermolysis of a CuCl2⋅2H2O and Cu(OH)2 mixture in glycerol has been developed. The resultant CuCl was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, EXAFS spectroscopy, X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The prepared samples of CuCl demonstrated high catalytic activity in the “direct synthesis” of triethoxysilane.
KW - Copper catalyst
KW - Cuprous chloride
KW - Direct synthesis
KW - Nanoparticles
KW - Nanostructured
KW - Silicon
KW - Trialkoxysilanes
KW - Triethoxysilane
UR - http://www.scopus.com/inward/record.url?scp=84941743113&partnerID=8YFLogxK
U2 - 10.1007/s12633-014-9272-5
DO - 10.1007/s12633-014-9272-5
M3 - Article
AN - SCOPUS:84941743113
VL - 7
SP - 79
EP - 87
JO - Silicon
JF - Silicon
SN - 1876-990X
IS - 2
ER -
ID: 25413274