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Syntheses of chiral nopinane-annelated pyridines of C2 and D2-symmetry : X-ray structures of the fused derivatives of 4,5-diazafluorene, 4,5-diaza-9H-fluoren-9-one, and 9,9’-bi-4,5-diazafluorenylidene. / Vasilyev, Eugene S.; Bagryanskaya, Irina Yu; Tkachev, Alexey V.
In:
Mendeleev Communications, Vol. 27, No. 2, 01.03.2017, p. 128-130.
Research output: Contribution to journal › Article › peer-review
Harvard
Vasilyev, ES, Bagryanskaya, IY
& Tkachev, AV 2017, '
Syntheses of chiral nopinane-annelated pyridines of C2 and D2-symmetry: X-ray structures of the fused derivatives of 4,5-diazafluorene, 4,5-diaza-9H-fluoren-9-one, and 9,9’-bi-4,5-diazafluorenylidene',
Mendeleev Communications, vol. 27, no. 2, pp. 128-130.
https://doi.org/10.1016/j.mencom.2017.03.006APA
Vasilyev, E. S., Bagryanskaya, I. Y.
, & Tkachev, A. V. (2017).
Syntheses of chiral nopinane-annelated pyridines of C2 and D2-symmetry: X-ray structures of the fused derivatives of 4,5-diazafluorene, 4,5-diaza-9H-fluoren-9-one, and 9,9’-bi-4,5-diazafluorenylidene.
Mendeleev Communications,
27(2), 128-130.
https://doi.org/10.1016/j.mencom.2017.03.006Vancouver
Author
Vasilyev, Eugene S. ; Bagryanskaya, Irina Yu
; Tkachev, Alexey V. /
Syntheses of chiral nopinane-annelated pyridines of C2 and D2-symmetry : X-ray structures of the fused derivatives of 4,5-diazafluorene, 4,5-diaza-9H-fluoren-9-one, and 9,9’-bi-4,5-diazafluorenylidene. In:
Mendeleev Communications. 2017 ; Vol. 27, No. 2. pp. 128-130.
BibTeX
@article{1de03af98b914dd2ae6321bb4d0c8b78,
title = "Syntheses of chiral nopinane-annelated pyridines of C2 and D2-symmetry: X-ray structures of the fused derivatives of 4,5-diazafluorene, 4,5-diaza-9H-fluoren-9-one, and 9,9{\textquoteright}-bi-4,5-diazafluorenylidene",
abstract = "Reaction of (+)-pinocarvone oxime with 2-morpholinocyclopent-2-enone and FeCl3·6H2O affords chiral C2-symmetric fused derivative of 4,5-diazafluorene, whose oxidation with SeO2 gives nopinane-annelated derivatives of 4,5-diaza-9Hfluoren- 9-one (C2-symmetry) and of 9,9{\textquoteright}-bi-4,5-diazafluorenylidene (D2-symmetry). Structures of the compounds synthesized were proved by X-ray crystallography.",
keywords = "N-OXIDES, ALLYLATION, ALDEHYDES, CHEMISTRY, LIGANDS, FECL3",
author = "Vasilyev, {Eugene S.} and Bagryanskaya, {Irina Yu} and Tkachev, {Alexey V.}",
year = "2017",
month = mar,
day = "1",
doi = "10.1016/j.mencom.2017.03.006",
language = "English",
volume = "27",
pages = "128--130",
journal = "Mendeleev Communications",
issn = "0959-9436",
publisher = "Elsevier",
number = "2",
}
RIS
TY - JOUR
T1 - Syntheses of chiral nopinane-annelated pyridines of C2 and D2-symmetry
T2 - X-ray structures of the fused derivatives of 4,5-diazafluorene, 4,5-diaza-9H-fluoren-9-one, and 9,9’-bi-4,5-diazafluorenylidene
AU - Vasilyev, Eugene S.
AU - Bagryanskaya, Irina Yu
AU - Tkachev, Alexey V.
PY - 2017/3/1
Y1 - 2017/3/1
N2 - Reaction of (+)-pinocarvone oxime with 2-morpholinocyclopent-2-enone and FeCl3·6H2O affords chiral C2-symmetric fused derivative of 4,5-diazafluorene, whose oxidation with SeO2 gives nopinane-annelated derivatives of 4,5-diaza-9Hfluoren- 9-one (C2-symmetry) and of 9,9’-bi-4,5-diazafluorenylidene (D2-symmetry). Structures of the compounds synthesized were proved by X-ray crystallography.
AB - Reaction of (+)-pinocarvone oxime with 2-morpholinocyclopent-2-enone and FeCl3·6H2O affords chiral C2-symmetric fused derivative of 4,5-diazafluorene, whose oxidation with SeO2 gives nopinane-annelated derivatives of 4,5-diaza-9Hfluoren- 9-one (C2-symmetry) and of 9,9’-bi-4,5-diazafluorenylidene (D2-symmetry). Structures of the compounds synthesized were proved by X-ray crystallography.
KW - N-OXIDES
KW - ALLYLATION
KW - ALDEHYDES
KW - CHEMISTRY
KW - LIGANDS
KW - FECL3
UR - http://www.scopus.com/inward/record.url?scp=85016077690&partnerID=8YFLogxK
U2 - 10.1016/j.mencom.2017.03.006
DO - 10.1016/j.mencom.2017.03.006
M3 - Article
AN - SCOPUS:85016077690
VL - 27
SP - 128
EP - 130
JO - Mendeleev Communications
JF - Mendeleev Communications
SN - 0959-9436
IS - 2
ER -
