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Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent. / Trakhinina, S. Yu; Taratayko, A. I.; Glazachev, Yu I. et al.

In: Russian Chemical Bulletin, Vol. 72, No. 7, 07.2023, p. 1569-1575.

Research output: Contribution to journal › Article › peer-review

Harvard

Trakhinina, SY, Taratayko, AI, Glazachev, YI & Kirilyuk, IA 2023, 'Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent', Russian Chemical Bulletin, vol. 72, no. 7, pp. 1569-1575. https://doi.org/10.1007/s11172-023-3935-6

APA

Trakhinina, S. Y., Taratayko, A. I., Glazachev, Y. I., & Kirilyuk, I. A. (2023). Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent. Russian Chemical Bulletin, 72(7), 1569-1575. https://doi.org/10.1007/s11172-023-3935-6

Vancouver

Trakhinina SY, Taratayko AI, Glazachev YI, Kirilyuk IA. Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent. Russian Chemical Bulletin. 2023 Jul;72(7):1569-1575. doi: 10.1007/s11172-023-3935-6

Author

Trakhinina, S. Yu ; Taratayko, A. I. ; Glazachev, Yu I. et al. / Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent. In: Russian Chemical Bulletin. 2023 ; Vol. 72, No. 7. pp. 1569-1575.

BibTeX

@article{07869ae212284a5c8c9a531a5ce530bc,
title = "Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent",
abstract = "Water-soluble spin probes were obtained from reduction-resistant sterically shielded pyrrolidine nitroxides by forming a 4,5-dicarboxy-1H-1,2,3-triazole fragment in the side chain by the Huisgen reaction of the azido group with acetylenedicarboxylic acid ester followed by hydrolysis. For the synthesized radicals, the reduction rate constants by ascorbate and the partition coefficient in an octanol—water system were determined.",
keywords = "Grignard reagents, nitrones, nitroxides, pyrrolidine, reduction kinetics",
author = "Trakhinina, {S. Yu} and Taratayko, {A. I.} and Glazachev, {Yu I.} and Kirilyuk, {I. A.}",
note = "This work was financially supported by the Russian Science Foundation (Project No. 21-73-00281). Публикация для корректировки.",
year = "2023",
month = jul,
doi = "10.1007/s11172-023-3935-6",
language = "English",
volume = "72",
pages = "1569--1575",
journal = "Russian Chemical Bulletin",
issn = "1066-5285",
publisher = "Springer Nature",
number = "7",

}

RIS

TY - JOUR

T1 - Sterically shielded pyrrolidine nitroxides with 3-(4,5-dicarboxy-1H-1,2,3-triazol-1-yl)propyl substituent

AU - Trakhinina, S. Yu

AU - Taratayko, A. I.

AU - Glazachev, Yu I.

AU - Kirilyuk, I. A.

N1 - This work was financially supported by the Russian Science Foundation (Project No. 21-73-00281). Публикация для корректировки.

PY - 2023/7

Y1 - 2023/7

N2 - Water-soluble spin probes were obtained from reduction-resistant sterically shielded pyrrolidine nitroxides by forming a 4,5-dicarboxy-1H-1,2,3-triazole fragment in the side chain by the Huisgen reaction of the azido group with acetylenedicarboxylic acid ester followed by hydrolysis. For the synthesized radicals, the reduction rate constants by ascorbate and the partition coefficient in an octanol—water system were determined.

AB - Water-soluble spin probes were obtained from reduction-resistant sterically shielded pyrrolidine nitroxides by forming a 4,5-dicarboxy-1H-1,2,3-triazole fragment in the side chain by the Huisgen reaction of the azido group with acetylenedicarboxylic acid ester followed by hydrolysis. For the synthesized radicals, the reduction rate constants by ascorbate and the partition coefficient in an octanol—water system were determined.

KW - Grignard reagents

KW - nitrones

KW - nitroxides

KW - pyrrolidine

KW - reduction kinetics

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-85167404747&origin=inward&txGid=c34816d23d1a11da13ef2c35a2880f88

UR - https://www.mendeley.com/catalogue/1e7985c3-25a3-3981-95c5-19cbdd707f10/

U2 - 10.1007/s11172-023-3935-6

DO - 10.1007/s11172-023-3935-6

M3 - Article

VL - 72

SP - 1569

EP - 1575

JO - Russian Chemical Bulletin

JF - Russian Chemical Bulletin

SN - 1066-5285

IS - 7

ER -

ID: 59582960