Standard

Sol–gel synthesis of 2D and 3D nanostructured YSZ : Yb3+ ceramics. / Krivoruchko, O. P.; Larina, T. V.; Ishchenko, A. V. et al.

In: Inorganic Materials, Vol. 53, No. 5, 01.05.2017, p. 540-547.

Research output: Contribution to journal › Article › peer-review

Harvard

Krivoruchko, OP, Larina, TV, Ishchenko, AV, Pestryakov, EV & Merzliakov, MA 2017, 'Sol–gel synthesis of 2D and 3D nanostructured YSZ: Yb3+ ceramics', Inorganic Materials, vol. 53, no. 5, pp. 540-547. https://doi.org/10.1134/S0020168517050144

APA

Krivoruchko, O. P., Larina, T. V., Ishchenko, A. V., Pestryakov, E. V., & Merzliakov, M. A. (2017). Sol–gel synthesis of 2D and 3D nanostructured YSZ: Yb3+ ceramics. Inorganic Materials, 53(5), 540-547. https://doi.org/10.1134/S0020168517050144

Vancouver

Krivoruchko OP, Larina TV, Ishchenko AV, Pestryakov EV, Merzliakov MA. Sol–gel synthesis of 2D and 3D nanostructured YSZ: Yb3+ ceramics. Inorganic Materials. 2017 May 1;53(5):540-547. doi: 10.1134/S0020168517050144

Author

Krivoruchko, O. P. ; Larina, T. V. ; Ishchenko, A. V. et al. / Sol–gel synthesis of 2D and 3D nanostructured YSZ : Yb3+ ceramics. In: Inorganic Materials. 2017 ; Vol. 53, No. 5. pp. 540-547.

BibTeX

@article{db98f42bdeb44f91b71b29fbbc4d84c6,
title = "Sol–gel synthesis of 2D and 3D nanostructured YSZ: Yb3+ ceramics",
abstract = "This paper presents results of a detailed study of fundamental aspects of the formation of 2D and 3D nanostructured YSZ:Yb3+ ceramics with a cubic structure through a key synthesis step in aqueous solutions of zirconium-containing hydroxy nanoparticles (1–2 nm) modified by Y3+ and Yb3+ ions, with the use of a sol–gel method and subsequent calcination of the resultant xerogels at temperatures above 350°C. As starting chemicals for the synthesis of ceramic powders, we used zirconyl, yttrium, and ytterbium nitrates and chlorides and aqueous ammonia. Using mixed solutions of these salts and a procedure developed by us, we synthesized sols, gels, and xerogels. To examine the effect of temperature on solid-state transformations, the xerogels were calcined according to a predetermined program in a muffle furnace at temperatures in the range from 350 to 1350°C (rarely, up to 1650°C). We focused primarily on ceramic powders close in composition to 0.86ZrO2 · 0.10Y2O3 · 0.04Yb2O3. The ceramics were characterized by high-resolution transmission electron microscopy, electron microdiffraction, electronic diffuse reflectance spectroscopy, energy dispersive X-ray microanalysis, and X-ray fluorescence analysis.",
keywords = "2D and 3D nanostructures, optically transparent ceramics, sol–gel method, DEFECTS, ZIRCONIA, sol-gel method",
author = "Krivoruchko, {O. P.} and Larina, {T. V.} and Ishchenko, {A. V.} and Pestryakov, {E. V.} and Merzliakov, {M. A.}",
year = "2017",
month = may,
day = "1",
doi = "10.1134/S0020168517050144",
language = "English",
volume = "53",
pages = "540--547",
journal = "Inorganic Materials",
issn = "0020-1685",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "5",

}

RIS

TY - JOUR

T1 - Sol–gel synthesis of 2D and 3D nanostructured YSZ

T2 - Yb3+ ceramics

AU - Krivoruchko, O. P.

AU - Larina, T. V.

AU - Ishchenko, A. V.

AU - Pestryakov, E. V.

AU - Merzliakov, M. A.

PY - 2017/5/1

Y1 - 2017/5/1

N2 - This paper presents results of a detailed study of fundamental aspects of the formation of 2D and 3D nanostructured YSZ:Yb3+ ceramics with a cubic structure through a key synthesis step in aqueous solutions of zirconium-containing hydroxy nanoparticles (1–2 nm) modified by Y3+ and Yb3+ ions, with the use of a sol–gel method and subsequent calcination of the resultant xerogels at temperatures above 350°C. As starting chemicals for the synthesis of ceramic powders, we used zirconyl, yttrium, and ytterbium nitrates and chlorides and aqueous ammonia. Using mixed solutions of these salts and a procedure developed by us, we synthesized sols, gels, and xerogels. To examine the effect of temperature on solid-state transformations, the xerogels were calcined according to a predetermined program in a muffle furnace at temperatures in the range from 350 to 1350°C (rarely, up to 1650°C). We focused primarily on ceramic powders close in composition to 0.86ZrO2 · 0.10Y2O3 · 0.04Yb2O3. The ceramics were characterized by high-resolution transmission electron microscopy, electron microdiffraction, electronic diffuse reflectance spectroscopy, energy dispersive X-ray microanalysis, and X-ray fluorescence analysis.

AB - This paper presents results of a detailed study of fundamental aspects of the formation of 2D and 3D nanostructured YSZ:Yb3+ ceramics with a cubic structure through a key synthesis step in aqueous solutions of zirconium-containing hydroxy nanoparticles (1–2 nm) modified by Y3+ and Yb3+ ions, with the use of a sol–gel method and subsequent calcination of the resultant xerogels at temperatures above 350°C. As starting chemicals for the synthesis of ceramic powders, we used zirconyl, yttrium, and ytterbium nitrates and chlorides and aqueous ammonia. Using mixed solutions of these salts and a procedure developed by us, we synthesized sols, gels, and xerogels. To examine the effect of temperature on solid-state transformations, the xerogels were calcined according to a predetermined program in a muffle furnace at temperatures in the range from 350 to 1350°C (rarely, up to 1650°C). We focused primarily on ceramic powders close in composition to 0.86ZrO2 · 0.10Y2O3 · 0.04Yb2O3. The ceramics were characterized by high-resolution transmission electron microscopy, electron microdiffraction, electronic diffuse reflectance spectroscopy, energy dispersive X-ray microanalysis, and X-ray fluorescence analysis.

KW - 2D and 3D nanostructures

KW - optically transparent ceramics

KW - sol–gel method

KW - DEFECTS

KW - ZIRCONIA

KW - sol-gel method

UR - http://www.scopus.com/inward/record.url?scp=85018505886&partnerID=8YFLogxK

U2 - 10.1134/S0020168517050144

DO - 10.1134/S0020168517050144

M3 - Article

AN - SCOPUS:85018505886

VL - 53

SP - 540

EP - 547

JO - Inorganic Materials

JF - Inorganic Materials

SN - 0020-1685

IS - 5

ER -

ID: 10260578