Research output: Contribution to journal › Article › peer-review
Seed-assisted synthesis of hierarchical zeolite ZSM-5 in the absence of organic templates. / Shestakova, Daria O.; Babina, Kseniya A.; Sladkovskiy, Dmitry A. et al.
In: Materials Chemistry and Physics, Vol. 288, 126432, 01.09.2022.Research output: Contribution to journal › Article › peer-review
}
TY - JOUR
T1 - Seed-assisted synthesis of hierarchical zeolite ZSM-5 in the absence of organic templates
AU - Shestakova, Daria O.
AU - Babina, Kseniya A.
AU - Sladkovskiy, Dmitry A.
AU - Parkhomchuk, Ekaterina V.
N1 - Funding Information: Our work was supported by the Ministry of Science and Higher Education of the Russian Federation within the governmental order for Boreskov Institute of Catalysis (project АААА-А21-121011490008-3 ). Publisher Copyright: © 2022 Elsevier B.V.
PY - 2022/9/1
Y1 - 2022/9/1
N2 - Hierarchical zeolite ZSM-5 was synthesized by template-free seed-assisted technique. The influence of different synthesis conditions (such as temperature (120–200 ⁰С) and time (12–72 h) of the hydrothermal treatment, alkali content, the amount (0–20 wt%) and size (100–1000 nm) of seed crystals) on crystallinity and texture of hierarchical zeolite ZSM-5 was studied. Materials have been characterized by X-ray diffraction, scanning electron microscopy, and nitrogen adsorption measurements. The catalytic activity of synthesized samples was tested in the n-hexane cracking process and compared with the one of commercial ZSM-5.
AB - Hierarchical zeolite ZSM-5 was synthesized by template-free seed-assisted technique. The influence of different synthesis conditions (such as temperature (120–200 ⁰С) and time (12–72 h) of the hydrothermal treatment, alkali content, the amount (0–20 wt%) and size (100–1000 nm) of seed crystals) on crystallinity and texture of hierarchical zeolite ZSM-5 was studied. Materials have been characterized by X-ray diffraction, scanning electron microscopy, and nitrogen adsorption measurements. The catalytic activity of synthesized samples was tested in the n-hexane cracking process and compared with the one of commercial ZSM-5.
KW - Hierarchical structure
KW - n-Hexane cracking
KW - Seed-assisted
KW - Template-free
KW - Zeolite
UR - http://www.scopus.com/inward/record.url?scp=85133440940&partnerID=8YFLogxK
U2 - 10.1016/j.matchemphys.2022.126432
DO - 10.1016/j.matchemphys.2022.126432
M3 - Article
AN - SCOPUS:85133440940
VL - 288
JO - Materials Chemistry and Physics
JF - Materials Chemistry and Physics
SN - 0254-0584
M1 - 126432
ER -
ID: 36571370