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Influence of synthesis conditions on the crystal and local structures of WO3 powders. / Popov, V. V.; Menushenkov, A. P.; Pisarev, A. A. et al.

In: Journal of Physics: Conference Series, Vol. 1238, No. 1, 012009, 2019.

Research output: Contribution to journal › Conference article › peer-review

Harvard

Popov, VV, Menushenkov, AP, Pisarev, AA, Berdnikova, MM, Zubavichus, YV, Svetogorov, RD, Shchetinin, IV, Zheleznyi, MV, Tsarenko, NA, Arzhatkina, LA, Yastrebtsev, AA, Gaynanov, BR & Ponkratov, KV 2019, 'Influence of synthesis conditions on the crystal and local structures of WO3 powders', Journal of Physics: Conference Series, vol. 1238, no. 1, 012009. https://doi.org/10.1088/1742-6596/1238/1/012009

APA

Popov, V. V., Menushenkov, A. P., Pisarev, A. A., Berdnikova, M. M., Zubavichus, Y. V., Svetogorov, R. D., Shchetinin, I. V., Zheleznyi, M. V., Tsarenko, N. A., Arzhatkina, L. A., Yastrebtsev, A. A., Gaynanov, B. R., & Ponkratov, K. V. (2019). Influence of synthesis conditions on the crystal and local structures of WO3 powders. Journal of Physics: Conference Series, 1238(1), [012009]. https://doi.org/10.1088/1742-6596/1238/1/012009

Vancouver

Popov VV, Menushenkov AP, Pisarev AA, Berdnikova MM, Zubavichus YV, Svetogorov RD et al. Influence of synthesis conditions on the crystal and local structures of WO3 powders. Journal of Physics: Conference Series. 2019;1238(1):012009. doi: 10.1088/1742-6596/1238/1/012009

Author

Popov, V. V. ; Menushenkov, A. P. ; Pisarev, A. A. et al. / Influence of synthesis conditions on the crystal and local structures of WO3 powders. In: Journal of Physics: Conference Series. 2019 ; Vol. 1238, No. 1.

BibTeX

@article{d711c5048b99442481b44de73930d410,
title = "Influence of synthesis conditions on the crystal and local structures of WO3 powders",
abstract = "Influence of synthesis conditions on the crystal and local structures of WO3 powders prepared by thermal decomposition of ammonium paratungstate and precipitation of tungstates aqueous solutions in strong acid conditions has been investigated. Combination of X-ray powder diffraction, X-ray absorption fine structure spectroscopy, IR- and Raman-spectroscopy, and scanning electron microscopy was used. The calcination of all initial compounds at temperatures ≥ 500C led to formation of the monoclinic γ-WO3 single phase. It was concluded that the neutral octahedral complex [W=0(0H)4(H20)] can be a structural unit of the precursors prepared in acidic suspensions. The local structure of synthesized tungsten oxides consists of edge-shared and corner-shared distorted octahedral WO6 species linked together.",
author = "Popov, {V. V.} and Menushenkov, {A. P.} and Pisarev, {A. A.} and Berdnikova, {M. M.} and Zubavichus, {Ya V.} and Svetogorov, {R. D.} and Shchetinin, {I. V.} and Zheleznyi, {M. V.} and Tsarenko, {N. A.} and Arzhatkina, {L. A.} and Yastrebtsev, {A. A.} and Gaynanov, {B. R.} and Ponkratov, {K. V.}",
note = "Publisher Copyright: {\textcopyright} Published under licence by IOP Publishing Ltd.; 4th International Conference on Laser and Plasma Research and Technologies, LaPlas 2018 ; Conference date: 30-01-2018 Through 01-02-2018",
year = "2019",
doi = "10.1088/1742-6596/1238/1/012009",
language = "English",
volume = "1238",
journal = "Journal of Physics: Conference Series",
issn = "1742-6588",
publisher = "IOP Publishing Ltd.",
number = "1",

}

RIS

TY - JOUR

T1 - Influence of synthesis conditions on the crystal and local structures of WO3 powders

AU - Popov, V. V.

AU - Menushenkov, A. P.

AU - Pisarev, A. A.

AU - Berdnikova, M. M.

AU - Zubavichus, Ya V.

AU - Svetogorov, R. D.

AU - Shchetinin, I. V.

AU - Zheleznyi, M. V.

AU - Tsarenko, N. A.

AU - Arzhatkina, L. A.

AU - Yastrebtsev, A. A.

AU - Gaynanov, B. R.

AU - Ponkratov, K. V.

N1 - Publisher Copyright: © Published under licence by IOP Publishing Ltd.

PY - 2019

Y1 - 2019

N2 - Influence of synthesis conditions on the crystal and local structures of WO3 powders prepared by thermal decomposition of ammonium paratungstate and precipitation of tungstates aqueous solutions in strong acid conditions has been investigated. Combination of X-ray powder diffraction, X-ray absorption fine structure spectroscopy, IR- and Raman-spectroscopy, and scanning electron microscopy was used. The calcination of all initial compounds at temperatures ≥ 500C led to formation of the monoclinic γ-WO3 single phase. It was concluded that the neutral octahedral complex [W=0(0H)4(H20)] can be a structural unit of the precursors prepared in acidic suspensions. The local structure of synthesized tungsten oxides consists of edge-shared and corner-shared distorted octahedral WO6 species linked together.

AB - Influence of synthesis conditions on the crystal and local structures of WO3 powders prepared by thermal decomposition of ammonium paratungstate and precipitation of tungstates aqueous solutions in strong acid conditions has been investigated. Combination of X-ray powder diffraction, X-ray absorption fine structure spectroscopy, IR- and Raman-spectroscopy, and scanning electron microscopy was used. The calcination of all initial compounds at temperatures ≥ 500C led to formation of the monoclinic γ-WO3 single phase. It was concluded that the neutral octahedral complex [W=0(0H)4(H20)] can be a structural unit of the precursors prepared in acidic suspensions. The local structure of synthesized tungsten oxides consists of edge-shared and corner-shared distorted octahedral WO6 species linked together.

UR - http://www.scopus.com/inward/record.url?scp=85069964990&partnerID=8YFLogxK

U2 - 10.1088/1742-6596/1238/1/012009

DO - 10.1088/1742-6596/1238/1/012009

M3 - Conference article

AN - SCOPUS:85069964990

VL - 1238

JO - Journal of Physics: Conference Series

JF - Journal of Physics: Conference Series

SN - 1742-6588

IS - 1

M1 - 012009

T2 - 4th International Conference on Laser and Plasma Research and Technologies, LaPlas 2018

Y2 - 30 January 2018 through 1 February 2018

ER -

ID: 25464637