Evolution of Aggregate-Like ZSM-5 Crystals

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Evolution of Aggregate-Like ZSM-5 Crystals. / Babina, K. A.; Shestakova, D. O.; Gerasimov, E. Yu et al.

In: Petroleum Chemistry, Vol. 62, No. 8, 08.2022, p. 820-826.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{285bd2399e9847a4b14ca4d1207494d7,

title = "Evolution of Aggregate-Like ZSM-5 Crystals",

abstract = "A series of zeolites ZSM-5 has been synthesized in hydrothermal conditions at160°C by varying the time of HT treatment with the following molar compositionsof the precursor gel: 1.0 SiO2 : 0.01Al2O3 : 0.2 ТPAОН : 0.05Na2O : 50 H2O : 4.0 EtOH.Materials have been characterized by X-ray diffraction, transmission electronmicroscopy and nitrogen adsorption measurements. We have succeeded to synthesizeZSM-5 crystals with metastable aggregate-like morphology reproducibly and tofollow their evolution during HT treatment.",

keywords = "crystallization, morphology, zeolite, ZSM-5",

author = "Babina, {K. A.} and Shestakova, {D. O.} and Gerasimov, {E. Yu} and I. Shamanaeva and Parkhomchuk, {E. V.}",

note = "Funding Information: Authors thank T.Ya. Efimenko for nitrogen adsorption measurements and N.A. Alekseeva for recording X-ray diffraction (XRD) patterns. The reported study was funded by RFBR, project number 20-33-90254. Publisher Copyright: {\textcopyright} 2022, Pleiades Publishing, Ltd.",

year = "2022",

month = aug,

doi = "10.1134/S0965544122070015",

language = "English",

volume = "62",

pages = "820--826",

journal = "Petroleum Chemistry",

issn = "0965-5441",

publisher = "Maik Nauka-Interperiodica Publishing",

number = "8",

}

RIS

TY - JOUR

T1 - Evolution of Aggregate-Like ZSM-5 Crystals

AU - Babina, K. A.

AU - Shestakova, D. O.

AU - Gerasimov, E. Yu

AU - Shamanaeva, I.

AU - Parkhomchuk, E. V.

N1 - Funding Information: Authors thank T.Ya. Efimenko for nitrogen adsorption measurements and N.A. Alekseeva for recording X-ray diffraction (XRD) patterns. The reported study was funded by RFBR, project number 20-33-90254. Publisher Copyright: © 2022, Pleiades Publishing, Ltd.

PY - 2022/8

Y1 - 2022/8

N2 - A series of zeolites ZSM-5 has been synthesized in hydrothermal conditions at160°C by varying the time of HT treatment with the following molar compositionsof the precursor gel: 1.0 SiO2 : 0.01Al2O3 : 0.2 ТPAОН : 0.05Na2O : 50 H2O : 4.0 EtOH.Materials have been characterized by X-ray diffraction, transmission electronmicroscopy and nitrogen adsorption measurements. We have succeeded to synthesizeZSM-5 crystals with metastable aggregate-like morphology reproducibly and tofollow their evolution during HT treatment.

AB - A series of zeolites ZSM-5 has been synthesized in hydrothermal conditions at160°C by varying the time of HT treatment with the following molar compositionsof the precursor gel: 1.0 SiO2 : 0.01Al2O3 : 0.2 ТPAОН : 0.05Na2O : 50 H2O : 4.0 EtOH.Materials have been characterized by X-ray diffraction, transmission electronmicroscopy and nitrogen adsorption measurements. We have succeeded to synthesizeZSM-5 crystals with metastable aggregate-like morphology reproducibly and tofollow their evolution during HT treatment.

KW - crystallization

KW - morphology

KW - zeolite

KW - ZSM-5

UR - http://www.scopus.com/inward/record.url?scp=85133570525&partnerID=8YFLogxK

UR - https://www.elibrary.ru/item.asp?id=49152559

UR - https://www.mendeley.com/catalogue/e7f769ce-c0a2-38bb-bf2d-80cd5a0d2ac5/

U2 - 10.1134/S0965544122070015

DO - 10.1134/S0965544122070015

M3 - Article

AN - SCOPUS:85133570525

VL - 62

SP - 820

EP - 826

JO - Petroleum Chemistry

JF - Petroleum Chemistry

SN - 0965-5441

IS - 8

ER -

ID: 36715924