Elemental Analysis with Sorption Preconcentration by Graphene Oxide for Mineral Water by Inductively Coupled Plasma–Optical Emission and Mass Spectrometries (ICP-OES and ICP-MS)

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Elemental Analysis with Sorption Preconcentration by Graphene Oxide for Mineral Water by Inductively Coupled Plasma–Optical Emission and Mass Spectrometries (ICP-OES and ICP-MS). / Medvedev, Nickolay S.; Kurbatova, Valeriya D.; Frolova, Alexandra O. et al.

In: Analytical Letters, 06.06.2024.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{7465b9f6e9c545749e07ecc6831cddfb,

title = "Elemental Analysis with Sorption Preconcentration by Graphene Oxide for Mineral Water by Inductively Coupled Plasma–Optical Emission and Mass Spectrometries (ICP-OES and ICP-MS)",

abstract = "The paper discusses using sorption preconcentration of elements from mineral waters by graphene oxide. The procedure aims to extract heavy metals such as Cd, Cr, Cu, Pb, Zn and other analytes from solution. Inductively coupled plasma–mass spectrometry (ICP-MS) and inductively coupled plasma–optical emission spectrometry (ICP-OES) were used to determine the analyte content. Graphene oxide was obtained by microwave exfoliation of graphite oxide. The sorption of analytes on the graphene oxide at different pH values and coexisting ion effect were studied in detail. Preliminary preconcentration of analytes provides good extraction recoveries using the optimal conditions. The limits of detection (LODs) of 27 analytes for the developed procedure ranged 0.1 to 200 ng L−1 for ICP-MS and from 5 to 1000 ng L−1 for ICP-OES. Sorption concentration provides recoveries of analytes from 80 to 110%. Graphene oxide was successfully employed for the sorption preconcentration of analytes from mineral and tap water.",

keywords = "Graphene oxide, heavy metals, inductively coupled plasma–mass spectrometry (ICP-MS), inductively coupled plasma–optical emission spectrometry (ICP-OES), sorption preconcentration",

author = "Medvedev, {Nickolay S.} and Kurbatova, {Valeriya D.} and Frolova, {Alexandra O.} and Guselnikova, {Tatiana Ya} and Troitskii, {Dmitry Yu} and Makotchenko, {Victor G.} and Saprykin, {Anatoly I.}",

note = "The study was funded by the Russian Science Foundation, project № 23-23-00058.",

year = "2024",

month = jun,

day = "6",

doi = "10.1080/00032719.2024.2356759",

language = "English",

journal = "Analytical Letters",

issn = "0003-2719",

publisher = "Taylor and Francis Ltd.",

}

RIS

TY - JOUR

T1 - Elemental Analysis with Sorption Preconcentration by Graphene Oxide for Mineral Water by Inductively Coupled Plasma–Optical Emission and Mass Spectrometries (ICP-OES and ICP-MS)

AU - Medvedev, Nickolay S.

AU - Kurbatova, Valeriya D.

AU - Frolova, Alexandra O.

AU - Guselnikova, Tatiana Ya

AU - Troitskii, Dmitry Yu

AU - Makotchenko, Victor G.

AU - Saprykin, Anatoly I.

N1 - The study was funded by the Russian Science Foundation, project № 23-23-00058.

PY - 2024/6/6

Y1 - 2024/6/6

N2 - The paper discusses using sorption preconcentration of elements from mineral waters by graphene oxide. The procedure aims to extract heavy metals such as Cd, Cr, Cu, Pb, Zn and other analytes from solution. Inductively coupled plasma–mass spectrometry (ICP-MS) and inductively coupled plasma–optical emission spectrometry (ICP-OES) were used to determine the analyte content. Graphene oxide was obtained by microwave exfoliation of graphite oxide. The sorption of analytes on the graphene oxide at different pH values and coexisting ion effect were studied in detail. Preliminary preconcentration of analytes provides good extraction recoveries using the optimal conditions. The limits of detection (LODs) of 27 analytes for the developed procedure ranged 0.1 to 200 ng L−1 for ICP-MS and from 5 to 1000 ng L−1 for ICP-OES. Sorption concentration provides recoveries of analytes from 80 to 110%. Graphene oxide was successfully employed for the sorption preconcentration of analytes from mineral and tap water.

AB - The paper discusses using sorption preconcentration of elements from mineral waters by graphene oxide. The procedure aims to extract heavy metals such as Cd, Cr, Cu, Pb, Zn and other analytes from solution. Inductively coupled plasma–mass spectrometry (ICP-MS) and inductively coupled plasma–optical emission spectrometry (ICP-OES) were used to determine the analyte content. Graphene oxide was obtained by microwave exfoliation of graphite oxide. The sorption of analytes on the graphene oxide at different pH values and coexisting ion effect were studied in detail. Preliminary preconcentration of analytes provides good extraction recoveries using the optimal conditions. The limits of detection (LODs) of 27 analytes for the developed procedure ranged 0.1 to 200 ng L−1 for ICP-MS and from 5 to 1000 ng L−1 for ICP-OES. Sorption concentration provides recoveries of analytes from 80 to 110%. Graphene oxide was successfully employed for the sorption preconcentration of analytes from mineral and tap water.

KW - Graphene oxide

KW - heavy metals

KW - inductively coupled plasma–mass spectrometry (ICP-MS)

KW - inductively coupled plasma–optical emission spectrometry (ICP-OES)

KW - sorption preconcentration

UR - https://www.scopus.com/record/display.uri?eid=2-s2.0-85194697666&origin=inward&txGid=19f1080af5b8b0a939159723ee3dc3b7

UR - https://www.webofscience.com/wos/woscc/full-record/WOS:001235404200001

UR - https://www.mendeley.com/catalogue/5cbc7430-ac2a-3d30-a69c-4d205ed3075a/

U2 - 10.1080/00032719.2024.2356759

DO - 10.1080/00032719.2024.2356759

M3 - Article

JO - Analytical Letters

JF - Analytical Letters

SN - 0003-2719

ER -

ID: 61171042