Standard

Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis. / Polyakova, E. V.; Shuvaeva, O. V.; Borisov, A. S.

In: Journal of Analytical Chemistry, Vol. 73, No. 9, 01.09.2018, p. 906-909.

Research output: Contribution to journal › Article › peer-review

Harvard

Polyakova, EV, Shuvaeva, OV & Borisov, AS 2018, 'Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis', Journal of Analytical Chemistry, vol. 73, no. 9, pp. 906-909. https://doi.org/10.1134/S1061934818090113

APA

Polyakova, E. V., Shuvaeva, O. V., & Borisov, A. S. (2018). Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis. Journal of Analytical Chemistry, 73(9), 906-909. https://doi.org/10.1134/S1061934818090113

Vancouver

Polyakova EV, Shuvaeva OV, Borisov AS. Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis. Journal of Analytical Chemistry. 2018 Sept 1;73(9):906-909. doi: 10.1134/S1061934818090113

Author

Polyakova, E. V. ; Shuvaeva, O. V. ; Borisov, A. S. / Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis. In: Journal of Analytical Chemistry. 2018 ; Vol. 73, No. 9. pp. 906-909.

BibTeX

@article{12b042db91694221a530c02a84c1d2df,
title = "Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis",
abstract = "Abstract: A procedure is developed for the determination of citrate ions in blood plasma by capillary zone electrophoresis at a level of 20‒800 mg/L. The background electrolyte (BGE) was a solution containing 10 mM chromate ions and 40 mM diethanolamine. Sample preparation included protein precipitation with acetonitrile, followed by dilution with a solution containing an internal standard (fluoride ion), and centrifugation. It is shown that the use of the internal standard ensures the account of the change in the migration time of the analyte in the analysis of biological samples. The relative standard deviation of analysis does not exceed 10% for two replicate determinations. The systematic error of the developed procedure was evaluated by the added–found method.",
keywords = "blood plasma, capillary electrophoresis, citrate ion, hemodialysis, OXALATE, ORGANIC-ACIDS",
author = "Polyakova, {E. V.} and Shuvaeva, {O. V.} and Borisov, {A. S.}",
note = "Publisher Copyright: {\textcopyright} 2018, Pleiades Publishing, Ltd.",
year = "2018",
month = sep,
day = "1",
doi = "10.1134/S1061934818090113",
language = "English",
volume = "73",
pages = "906--909",
journal = "Journal of Analytical Chemistry",
issn = "1061-9348",
publisher = "PLEIADES PUBLISHING INC",
number = "9",

}

RIS

TY - JOUR

T1 - Determination of Citrate Ions in Blood Plasma by Capillary Zone Electrophoresis

AU - Polyakova, E. V.

AU - Shuvaeva, O. V.

AU - Borisov, A. S.

N1 - Publisher Copyright: © 2018, Pleiades Publishing, Ltd.

PY - 2018/9/1

Y1 - 2018/9/1

N2 - Abstract: A procedure is developed for the determination of citrate ions in blood plasma by capillary zone electrophoresis at a level of 20‒800 mg/L. The background electrolyte (BGE) was a solution containing 10 mM chromate ions and 40 mM diethanolamine. Sample preparation included protein precipitation with acetonitrile, followed by dilution with a solution containing an internal standard (fluoride ion), and centrifugation. It is shown that the use of the internal standard ensures the account of the change in the migration time of the analyte in the analysis of biological samples. The relative standard deviation of analysis does not exceed 10% for two replicate determinations. The systematic error of the developed procedure was evaluated by the added–found method.

AB - Abstract: A procedure is developed for the determination of citrate ions in blood plasma by capillary zone electrophoresis at a level of 20‒800 mg/L. The background electrolyte (BGE) was a solution containing 10 mM chromate ions and 40 mM diethanolamine. Sample preparation included protein precipitation with acetonitrile, followed by dilution with a solution containing an internal standard (fluoride ion), and centrifugation. It is shown that the use of the internal standard ensures the account of the change in the migration time of the analyte in the analysis of biological samples. The relative standard deviation of analysis does not exceed 10% for two replicate determinations. The systematic error of the developed procedure was evaluated by the added–found method.

KW - blood plasma

KW - capillary electrophoresis

KW - citrate ion

KW - hemodialysis

KW - OXALATE

KW - ORGANIC-ACIDS

UR - http://www.scopus.com/inward/record.url?scp=85052907080&partnerID=8YFLogxK

U2 - 10.1134/S1061934818090113

DO - 10.1134/S1061934818090113

M3 - Article

AN - SCOPUS:85052907080

VL - 73

SP - 906

EP - 909

JO - Journal of Analytical Chemistry

JF - Journal of Analytical Chemistry

SN - 1061-9348

IS - 9

ER -

ID: 16485338