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Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials. / Vasilyeva, Inga; Logvinenko, Vladimir.

Solid Compounds of Transition Elements. Vol. 257 Trans Tech Publications Ltd, 2017. p. 237-240 (Solid State Phenomena; Vol. 257).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Research › peer-review

Harvard

Vasilyeva, I & Logvinenko, V 2017, Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials. in Solid Compounds of Transition Elements. vol. 257, Solid State Phenomena, vol. 257, Trans Tech Publications Ltd, pp. 237-240, 20th International Conference on Solid Compounds of Transition Elements, SCTE2016, Zaragoza, Spain, 10.04.2016. https://doi.org/10.4028/www.scientific.net/SSP.257.237

APA

Vasilyeva, I., & Logvinenko, V. (2017). Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials. In Solid Compounds of Transition Elements (Vol. 257, pp. 237-240). (Solid State Phenomena; Vol. 257). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/SSP.257.237

Vancouver

Vasilyeva I, Logvinenko V. Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials. In Solid Compounds of Transition Elements. Vol. 257. Trans Tech Publications Ltd. 2017. p. 237-240. (Solid State Phenomena). doi: 10.4028/www.scientific.net/SSP.257.237

Author

Vasilyeva, Inga ; Logvinenko, Vladimir. / Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials. Solid Compounds of Transition Elements. Vol. 257 Trans Tech Publications Ltd, 2017. pp. 237-240 (Solid State Phenomena).

BibTeX

@inproceedings{8516faa3d69b41a092f49802bea40714,
title = "Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials",
abstract = "Controlling the hydrolysis conditions of the solution TiOSO4•xH2SO4•yH2O, the η-TiO2 and A-TiO2 single phases were prepared in amorphous/crystalline state. With scanty structural and electron microscopy data, the unique capability of differential dissolution method was used to perform quantitative phase analysis of the samples and identify phases where two from them (TiO)(HSO4)0.4(OH) and TiO(OH)2 were found to be amorphous. New results were obtained that the amorphous TiO(OH)2 is transformed to ~ 5-nm crystallites TiO2-x•0.95H2O which then turned into ~ 3-nm crystallites TiO2•0.25H2O when drying the gels at 90°C. New structural models for the crystallites were proposed explaining differences in their chemical and thermal characteristics.",
keywords = "Chemical and structural variety, TiO, η-nanoparticles",
author = "Inga Vasilyeva and Vladimir Logvinenko",
year = "2017",
doi = "10.4028/www.scientific.net/SSP.257.237",
language = "English",
isbn = "9783038355861",
volume = "257",
series = "Solid State Phenomena",
publisher = "Trans Tech Publications Ltd",
pages = "237--240",
booktitle = "Solid Compounds of Transition Elements",
note = "20th International Conference on Solid Compounds of Transition Elements, SCTE2016 ; Conference date: 10-04-2016 Through 14-04-2016",

}

RIS

TY - GEN

T1 - Contribution of chemical methods to the study of nanostructure of ultrafine and amorphous materials

AU - Vasilyeva, Inga

AU - Logvinenko, Vladimir

PY - 2017

Y1 - 2017

N2 - Controlling the hydrolysis conditions of the solution TiOSO4•xH2SO4•yH2O, the η-TiO2 and A-TiO2 single phases were prepared in amorphous/crystalline state. With scanty structural and electron microscopy data, the unique capability of differential dissolution method was used to perform quantitative phase analysis of the samples and identify phases where two from them (TiO)(HSO4)0.4(OH) and TiO(OH)2 were found to be amorphous. New results were obtained that the amorphous TiO(OH)2 is transformed to ~ 5-nm crystallites TiO2-x•0.95H2O which then turned into ~ 3-nm crystallites TiO2•0.25H2O when drying the gels at 90°C. New structural models for the crystallites were proposed explaining differences in their chemical and thermal characteristics.

AB - Controlling the hydrolysis conditions of the solution TiOSO4•xH2SO4•yH2O, the η-TiO2 and A-TiO2 single phases were prepared in amorphous/crystalline state. With scanty structural and electron microscopy data, the unique capability of differential dissolution method was used to perform quantitative phase analysis of the samples and identify phases where two from them (TiO)(HSO4)0.4(OH) and TiO(OH)2 were found to be amorphous. New results were obtained that the amorphous TiO(OH)2 is transformed to ~ 5-nm crystallites TiO2-x•0.95H2O which then turned into ~ 3-nm crystallites TiO2•0.25H2O when drying the gels at 90°C. New structural models for the crystallites were proposed explaining differences in their chemical and thermal characteristics.

KW - Chemical and structural variety

KW - TiO

KW - η-nanoparticles

UR - http://www.scopus.com/inward/record.url?scp=84994187798&partnerID=8YFLogxK

U2 - 10.4028/www.scientific.net/SSP.257.237

DO - 10.4028/www.scientific.net/SSP.257.237

M3 - Conference contribution

AN - SCOPUS:84994187798

SN - 9783038355861

VL - 257

T3 - Solid State Phenomena

SP - 237

EP - 240

BT - Solid Compounds of Transition Elements

PB - Trans Tech Publications Ltd

T2 - 20th International Conference on Solid Compounds of Transition Elements, SCTE2016

Y2 - 10 April 2016 through 14 April 2016

ER -

ID: 9444684