Chromatographic and Mass Spectrometric Studies of the Features of Vanillin Desorption during Regeneration of a Highly Basic Anion Exchanger

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Chromatographic and Mass Spectrometric Studies of the Features of Vanillin Desorption during Regeneration of a Highly Basic Anion Exchanger. / Sholokhova, A. Yu; Shashkov, M. V.; Eliseeva, T. V. et al.

In: Protection of Metals and Physical Chemistry of Surfaces, Vol. 56, No. 1, 01.01.2020, p. 44-48.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{e558e4903f3c42b180232cbba46e484e,

title = "Chromatographic and Mass Spectrometric Studies of the Features of Vanillin Desorption during Regeneration of a Highly Basic Anion Exchanger",

abstract = "The occurrence of side chemical reactions during regeneration of the highly basic anion exchanger AB-17-2P with adsorbed vanillin with an alkali solution in the presence of atmospheric oxygen was confirmed by the method of gas chromatography/mass spectrometry. A number of the vanillin transformation products were identified. The method of mass spectrometry with matrix-activated laser desorption/ionization demonstrated the presence of the products of vanillin oxidation and polymerization, as well as benzoin condensation in the studied regeneration solution.",

keywords = "gas chromatography/mass spectrometry, highly basic anion exchanger, matrix-activated laser desorption/ionization mass spectrometry, regeneration, side reactions, vanillin",

author = "Sholokhova, {A. Yu} and Shashkov, {M. V.} and Eliseeva, {T. V.} and Buryak, {A. K.}",

year = "2020",

month = jan,

day = "1",

doi = "10.1134/S2070205119060297",

language = "English",

volume = "56",

pages = "44--48",

journal = "Protection of Metals and Physical Chemistry of Surfaces",

issn = "2070-2051",

publisher = "PLEIADES PUBLISHING INC",

number = "1",

}

RIS

TY - JOUR

T1 - Chromatographic and Mass Spectrometric Studies of the Features of Vanillin Desorption during Regeneration of a Highly Basic Anion Exchanger

AU - Sholokhova, A. Yu

AU - Shashkov, M. V.

AU - Eliseeva, T. V.

AU - Buryak, A. K.

PY - 2020/1/1

Y1 - 2020/1/1

N2 - The occurrence of side chemical reactions during regeneration of the highly basic anion exchanger AB-17-2P with adsorbed vanillin with an alkali solution in the presence of atmospheric oxygen was confirmed by the method of gas chromatography/mass spectrometry. A number of the vanillin transformation products were identified. The method of mass spectrometry with matrix-activated laser desorption/ionization demonstrated the presence of the products of vanillin oxidation and polymerization, as well as benzoin condensation in the studied regeneration solution.

AB - The occurrence of side chemical reactions during regeneration of the highly basic anion exchanger AB-17-2P with adsorbed vanillin with an alkali solution in the presence of atmospheric oxygen was confirmed by the method of gas chromatography/mass spectrometry. A number of the vanillin transformation products were identified. The method of mass spectrometry with matrix-activated laser desorption/ionization demonstrated the presence of the products of vanillin oxidation and polymerization, as well as benzoin condensation in the studied regeneration solution.

KW - gas chromatography/mass spectrometry

KW - highly basic anion exchanger

KW - matrix-activated laser desorption/ionization mass spectrometry

KW - regeneration

KW - side reactions

KW - vanillin

UR - http://www.scopus.com/inward/record.url?scp=85083198976&partnerID=8YFLogxK

U2 - 10.1134/S2070205119060297

DO - 10.1134/S2070205119060297

M3 - Article

AN - SCOPUS:85083198976

VL - 56

SP - 44

EP - 48

JO - Protection of Metals and Physical Chemistry of Surfaces

JF - Protection of Metals and Physical Chemistry of Surfaces

SN - 2070-2051

IS - 1

ER -

ID: 24161140