Application of Synchrotron Radiation for Phase Analysis of Metal-Ceramic Materials Obtained by Laser Additive Manufacturing

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Application of Synchrotron Radiation for Phase Analysis of Metal-Ceramic Materials Obtained by Laser Additive Manufacturing. / Golyshev, A. A.; Gertsel, I. S.; Zavjalov, A. P. et al.

In: Journal of Surface Investigation, Vol. 19, No. 5, 10.2025, p. 1141-1147.

Research output: Contribution to journal › Article › peer-review

BibTeX

@article{c044ca19eebe46388906f8b567510a30,

title = "Application of Synchrotron Radiation for Phase Analysis of Metal-Ceramic Materials Obtained by Laser Additive Manufacturing",

abstract = "The evolution of the phase composition of a metal-ceramic material formed by direct laser deposition using synchrotron radiation has been studied. Electron microscopy and X-ray phase analysis demonstrate that active formation of secondary phases of compounds occurs during repeated remelting in the process of multilayer deposition. Insignificant formation of secondary phases occurs during single-track deposition due to the short lifetime of the molten pool. It is established that an increase in the concentration of secondary phases leads to an increase in the material microhardness.",

keywords = "Rietveld method, additive technologies, boron carbide, in situ, metal ceramics, microhardness, secondary phases transformations, synchrotron radiation, titanium alloy, АДДИТИВНЫЕ ТЕХНОЛОГИИ, ТИТАНОВЫЙ СПЛАВ, КАРБИД БОРА, МЕТАЛЛОКЕРАМИКА, СИНХРОТРОННОЕ ИЗЛУЧЕНИЕ, IN SITU, ВТОРИЧНЫЕ ФАЗЫ ПРЕВРАЩЕНИЯ, ИКРОТВЕРДОСТЬ, МЕТОД РИТВЕЛЬДА",

author = "Golyshev, {A. A.} and Gertsel, {I. S.} and Zavjalov, {A. P.} and Mamutov, {R. S.} and Malikov, {A. G.}",

note = "Golyshev, A.A., Gertsel, I.S., Zavjalov, A.P. et al. Application of Synchrotron Radiation for Phase Analysis of Metal-Ceramic Materials Obtained by Laser Additive Manufacturing. J. Surf. Investig. 19, 1141–1147 (2025). https://doi.org/10.1134/S1027451025701629 The work was carried out within the budget themes of the Khristianovich Institute of Theoretical and Applied Mechanics, Siberian Branch of the Russian Academy of Sciences 124021500015-1.",

year = "2025",

month = oct,

doi = "10.1134/S1027451025701629",

language = "English",

volume = "19",

pages = "1141--1147",

journal = "Journal of Surface Investigation",

issn = "1027-4510",

publisher = "ФГБУ {"}Издательство {"}Наука{"}",

number = "5",

}

RIS

TY - JOUR

T1 - Application of Synchrotron Radiation for Phase Analysis of Metal-Ceramic Materials Obtained by Laser Additive Manufacturing

AU - Golyshev, A. A.

AU - Gertsel, I. S.

AU - Zavjalov, A. P.

AU - Mamutov, R. S.

AU - Malikov, A. G.

N1 - Golyshev, A.A., Gertsel, I.S., Zavjalov, A.P. et al. Application of Synchrotron Radiation for Phase Analysis of Metal-Ceramic Materials Obtained by Laser Additive Manufacturing. J. Surf. Investig. 19, 1141–1147 (2025). https://doi.org/10.1134/S1027451025701629 The work was carried out within the budget themes of the Khristianovich Institute of Theoretical and Applied Mechanics, Siberian Branch of the Russian Academy of Sciences 124021500015-1.

PY - 2025/10

Y1 - 2025/10

N2 - The evolution of the phase composition of a metal-ceramic material formed by direct laser deposition using synchrotron radiation has been studied. Electron microscopy and X-ray phase analysis demonstrate that active formation of secondary phases of compounds occurs during repeated remelting in the process of multilayer deposition. Insignificant formation of secondary phases occurs during single-track deposition due to the short lifetime of the molten pool. It is established that an increase in the concentration of secondary phases leads to an increase in the material microhardness.

AB - The evolution of the phase composition of a metal-ceramic material formed by direct laser deposition using synchrotron radiation has been studied. Electron microscopy and X-ray phase analysis demonstrate that active formation of secondary phases of compounds occurs during repeated remelting in the process of multilayer deposition. Insignificant formation of secondary phases occurs during single-track deposition due to the short lifetime of the molten pool. It is established that an increase in the concentration of secondary phases leads to an increase in the material microhardness.

KW - Rietveld method

KW - additive technologies

KW - boron carbide

KW - in situ

KW - metal ceramics

KW - microhardness

KW - secondary phases transformations

KW - synchrotron radiation

KW - titanium alloy

KW - АДДИТИВНЫЕ ТЕХНОЛОГИИ

KW - ТИТАНОВЫЙ СПЛАВ

KW - КАРБИД БОРА

KW - МЕТАЛЛОКЕРАМИКА

KW - СИНХРОТРОННОЕ ИЗЛУЧЕНИЕ

KW - IN SITU

KW - ВТОРИЧНЫЕ ФАЗЫ ПРЕВРАЩЕНИЯ

KW - ИКРОТВЕРДОСТЬ

KW - МЕТОД РИТВЕЛЬДА

UR - https://www.scopus.com/pages/publications/105028414410

UR - https://www.elibrary.ru/item.asp?id=88906062

UR - https://www.mendeley.com/catalogue/f34beb46-dbfd-389e-86e6-000e3c1016af/

U2 - 10.1134/S1027451025701629

DO - 10.1134/S1027451025701629

M3 - Article

VL - 19

SP - 1141

EP - 1147

JO - Journal of Surface Investigation

JF - Journal of Surface Investigation

SN - 1027-4510

IS - 5

ER -

ID: 74616725